Novel vinegar age rapid detecting method
A detection method, the technology of vinegar, is applied in the direction of material analysis by observing the influence of chemical indicators, and analysis by making materials undergo chemical reactions. Gas detection analysis, vinegar marker analysis and other issues, to achieve the effect of maintaining market order and low cost
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[0029] The flowchart of the method of the present invention is as figure 1 As shown, the present invention will be described in detail below in conjunction with various implementations shown in the accompanying drawings.
[0030]Step 1: Fragrant vinegar (taking Zhenjiang fragrant vinegar as an example) screening and analysis of vinegar age markers: firstly, determine the characteristic volatile gases of different vinegar age vinegars by GC-MS. Including the following steps:
[0031] (1.1) Use a pipette to pipette 8 mL of balsamic vinegar sample into a 15 mL extraction bottle, add 2.5 g of solid sodium chloride, and tighten the cap. Wherein the effect of adding sodium chloride is to promote the volatilization of volatile gas in the balsamic vinegar. Then place the extraction bottle in a constant temperature water bath at 45°C and heat it with an oscillation frequency of 250r / min. Insert the SPME extraction head from the rubber pad of the bottle cap into the headspace of the ...
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