High nickel ternary lithium ion battery anode slurry and preparation method thereof
A lithium-ion battery and positive electrode slurry technology, which is applied to battery electrodes, secondary batteries, circuits, etc., can solve the problems of increasing the difficulty of homogenization, achieve the effects of reducing pulping time, reducing usage, and improving dispersion force
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[0040] The preparation method of an embodiment of the high-nickel ternary lithium-ion battery cathode slurry of the present invention may comprise the following steps:
[0041] S1. Weigh each raw material according to parts by weight: 89.5-97.9 parts of high-nickel ternary positive electrode powder, 1-5 parts of conductive agent, 1-5 parts of binder, accounting for 0.1%-0.5% of the weight ratio of all solid powder materials Mixed additives and an appropriate amount of solvent. If the above-mentioned solid raw materials are stored abnormally, they can be baked first, and then pulped after cooling.
[0042] S2. Add the binder and mixed additives in the raw materials into the solvent, stir evenly and vacuum defoam to prepare glue. Control the temperature of the glue solution to be 25-50°C.
[0043] Further, step S2 may include:
[0044]S2.1. Add any one of the binder and mixed additives (dispersive additive or acidic buffer additive) into the solvent, stir evenly, and then add...
Embodiment 1
[0057] Take 97 parts of high-nickel ternary positive electrode powder, 1.3 parts of conductive agent, 1.4 parts of binder, and 0.3 parts of mixed additive. In the mixed additive, the dosage ratio of dispersive additive and acidic buffer additive is 1:2; It is polyvinylidene fluoride, and the solvent is N-methylpyrrolidone, 25 parts. According to the preparation method of the present invention, the above-mentioned raw materials are made into high-nickel ternary lithium-ion battery positive electrode slurry, the temperature of the glue and the slurry is controlled to be 25-50° C. in the whole process, and the viscosity of the final slurry is 5600 mPa.s. The solid content of the slurry is 80%. Among them, the glue preparation time is 2.5h, and the total homogenization time is 5.0h.
Embodiment 2
[0059] Take 96.8 parts of high-nickel ternary positive electrode powder, 1.3 parts of conductive agent, 1.4 parts of binder, and 0.5 parts of mixed additives. In the mixed additives, the dosage ratio of dispersive additives and acidic buffer additives is 2:1; It is polyvinylidene fluoride, and the solvent is N-methylpyrrolidone, 23.5 parts. According to the preparation method of the present invention, the above-mentioned raw materials are made into high-nickel ternary lithium-ion battery positive electrode slurry, the temperature of the glue and the slurry is controlled to be 25-50° C. in the whole process, and the viscosity of the final slurry is 6300 mPa.s. The solid content of the slurry was 81%. Among them, the glue preparation time is 2.5h, and the total homogenization time is 5.0h.
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