Method for producing layer structure and method for patterning
A technology for generating layers and patterns, which is applied in the photoengraving process of the pattern surface, photosensitive materials and instruments for opto-mechanical equipment, etc., and can solve the problem of difficulty in providing clear and fine patterns.
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Synthetic example 1
[0175] 16 grams of phenanthrene-9-ol, 16 grams of 1,3-bis(2-methoxyethyl)benzene (1,3-bis(2-methoxyethyl)benzene), 0.46 grams of diethyl sulfate and 61 grams of propylene glycol Propylene glycol monomethyl ether acetate (PGMEA) was put into the flask and then stirred at 100° C. for 2 hours to 15 hours to perform polymerization reaction. The reaction is complete when the weight average molecular weight of the polymer is 2,000 to 3,500. When the polymerization reaction was completed, the reactant was slowly cooled to room temperature and then added to 40 g of distilled water and 400 g of methanol, and the mixture was stirred and allowed to stand. After removing the supernatant therefrom, the precipitate therein was dissolved in 80 g of propylene glycol monomethyl ether acetate (PGMEA), and the solution was stirred by using 320 g of methanol and 320 g of water and allowed to stand (primary process) . Herein, after removing the supernatant obtained therefrom again, the precipita...
Synthetic example 2
[0179] According to the same synthesis as Synthetic Example 1, by using 18 grams of anthracene, 26 grams of 1,4-bis(methoxymethyl)benzene (1,4-bis(methoxymethyl)benzene), 66 grams of propylene glycol monomethyl ether acetic acid Ester (PGMEA) and 0.5 g of diethyl sulfate obtained a polymer (Mw: 3500) including the structural unit represented by Chemical Formula 2a.
[0180] [chemical formula 2a]
[0181]
Synthetic example 3
[0183] According to the same synthesis as in Synthesis Example 1, by using 38 grams of 4,4'-(9H-fluorene-9,9-diyl)diphenol (4,4'-(9H-fluorene-9,9-diyl)diphenol ), 17 grams of 1,4-bis(methoxymethyl)benzene, 82 grams of propylene glycol monomethyl ether acetate (PGMEA) and 0.5 grams of diethyl sulfate to obtain a polymer comprising a structural unit represented by Chemical Formula 3a ( Mw: 3500).
[0184] [chemical formula 3a]
[0185]
PUM
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