Preparation method of yttrium zirconate ceramic glaze material having photocatalytic function

A technology of ceramic glaze and yttrium zirconate, which is applied in the field of preparation of yttrium zirconate ceramic glaze with photocatalytic function, can solve the problems of poor bonding effect between coating and substrate, uneven distribution of photocatalyst, etc., and achieve good visible light Response, good surface decoration effect, and the effect of improving absorption utilization

Active Publication Date: 2017-05-17
广西艾陶新型材料科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The photocatalyst distribution of the above two methods is uneven, and there are shortcomings such as "rainbow effect" or poor bonding effect between the coating and the substrate.

Method used

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  • Preparation method of yttrium zirconate ceramic glaze material having photocatalytic function
  • Preparation method of yttrium zirconate ceramic glaze material having photocatalytic function

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] 1) First, quartz, potassium feldspar, albite, borax, Y 2 o 3 , Suzhou soil, and lithium carbonate are prepared according to the following mass chemical composition ratios. SiO 2 :Al 2 o 3 :B 2 o 3 : Y 2 o 3 : Li 2 O: Na 2 O:K 2 O=57:4:22:4:7:4:3.

[0033] 2) Dry mix and grind the above-mentioned powders, pass through a 60-mesh sieve to obtain the mixture, put it into a crucible, put it into an electric furnace and keep it at 1270°C for 20 minutes, take it out and pour it into water to quench to make a frit. Take out the frit from the water, put it into a ball mill after drying, and grind it finely. The mass ratio of control material (frit): ball: water is 1:1:0.8, pass through a 250-mesh sieve after grinding for 3 hours, and dry for later use. This powder is denoted as A material.

[0034] 3) The above-mentioned material A, Y 2 o 3 , ZrO 2 And Suzhou soil is A material according to the mass ratio: Y 2 o 3 : Suzhou soil = 82:8:7 ratio for batching, and ...

Embodiment 2

[0040] 1) First, quartz, potassium feldspar, albite, borax, Y 2 o 3 , Suzhou soil, and lithium carbonate are prepared according to the following mass chemical composition ratios. SiO 2 :Al 2 o 3 :B 2 o 3 : Y 2 o 3 : Li 2 O: Na 2 O:K 2 O=58:5:23:3:6:3:2.

[0041] 2) Dry mix and grind the above-mentioned powders, pass through a 60-mesh sieve to obtain the mixture, put it into a crucible, put it into an electric furnace and keep it warm at 1280°C for 30 minutes, take it out and pour it into water to quench to make a frit. Take the frit out of the water, put it into a ball mill after drying, and grind it finely. The mass ratio of control material (frit): ball: water is 1:1:0.8, pass through a 250-mesh sieve after grinding for 4 hours, and dry for later use. This powder is denoted as A material.

[0042] 3) The above-mentioned material A, Y 2 o 3 , ZrO 2 And Suzhou soil is A material according to the mass ratio: Y 2 o 3 : Suzhou soil = 84:7:6 ratio for batching, a...

Embodiment 3

[0046] 1) First, quartz, potassium feldspar, albite, borax, Y 2 o 3 , Suzhou soil, and lithium carbonate are prepared according to the following mass chemical composition ratios. SiO 2 :Al 2 o 3 :B 2 o 3 : Y 2 o 3 : Li 2 O: Na 2 O:K 2 O=59:6:24:2:5:2:1.

[0047] 2) Dry mix and grind the above-mentioned powders, pass through a 40-mesh sieve to obtain the mixture, put it into a crucible, put it in an electric furnace at 1290° C. for 40 minutes, take it out and pour it into water to quench to obtain a frit. Take out the frit from the water, put it into a ball mill after drying, and grind it finely. The mass ratio of control material (frit): ball: water is 1:1:0.8, pass through a 250-mesh sieve after grinding for 3 hours, and dry for later use. This powder is denoted as A material.

[0048] 3) The above-mentioned material A, Y 2 o 3 , ZrO 2 And Suzhou soil is A material according to the mass ratio: Y 2 o 3 : Suzhou soil = 86:6:5 ratio for batching, and Y 2 o 3 ...

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Abstract

The invention relates to a preparation method of a yttrium zirconate ceramic glaze material having a photocatalytic function. The preparation method comprises the following steps: preparing quartz, potash feldspar, albite, borax, Y2O3, Suzhou clay and lithium carbonate, keeping the temperature at 1270-1290 DEG C for 20-40 minutes, taking out, pouring into water, quenching to prepare a fusion cake, and grinding the fusion cake to obtain a material A; preparing the material A, Y2O3, ZrO2 and Suzhou clay, and grinding to obtain a material B; adding the material B and dispersing agent into water, and uniformly stirring and mixing to prepare a glaze slip; and applying the glaze slip to the surface of ceramics in a glaze spray manner, and firing to obtain the yttrium zirconate ceramic glaze material having a photocatalytic function. According to the invention, the ceramic glaze is prepared through a firing process and does not need coating, so that the prepared functional ceramic glaze material can be tightly combined with a ceramic matrix; and the photocatalyst yttrium zirconate generated in the sintering process of Y2O3 and ZrO2 is uniformly distributed in the glaze material, thereby avoiding influencing the aesthetic property of the glaze material due to a rainbow effect.

Description

technical field [0001] The invention belongs to the technical field of ceramic glazes. Specifically relates to a preparation method of yttrium zirconate ceramic glaze with photocatalytic function. Background technique [0002] In the 21st century, human society is developing rapidly, and has made great progress in various aspects such as technology and economy. However, the problems of resources and ecology are becoming increasingly prominent, threatening the sustainable development of human society. The birth of photocatalytic technology provides a new way of thinking for us to use solar energy, a clean, cheap and renewable energy. [0003] Photocatalytic technology began in 1972 with the discovery of the Fujishima-Honda effect [Fujishima A., Honda K. Photocatalysis-decomposition of water at the surface of an irradiated semiconductor [J]. Nature, 1972, 238(5385): 37-38.] , which has aroused the great attention of scientific and technological workers on semiconductor phot...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C03C8/20C03C8/02C04B41/86
CPCC03C8/02C03C8/20C04B41/009C04B41/5022C04B41/86C04B41/4539C04B41/4543C04B41/0072
Inventor 曹丽云罗艺佳黄剑锋李嘉胤孔新刚刘一军
Owner 广西艾陶新型材料科技有限公司
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