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Preparation method of chitosan/agarose xerogel particles and application of chitosan/agarose xerogel particles in cigarette filter tip

A technology of xerogel particles and chitosan, applied in the application, tobacco, tobacco processing and other directions, to improve the quality of smoking, increase the coordination of smoke, reduce the effect of miscellaneous gas and irritation

Active Publication Date: 2017-08-11
CHINA TOBACCO GUANGXI IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, it is still relatively rare to add natural materials to cigarette filters to prepare composite filters to achieve the purpose of moisturizing.

Method used

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  • Preparation method of chitosan/agarose xerogel particles and application of chitosan/agarose xerogel particles in cigarette filter tip
  • Preparation method of chitosan/agarose xerogel particles and application of chitosan/agarose xerogel particles in cigarette filter tip
  • Preparation method of chitosan/agarose xerogel particles and application of chitosan/agarose xerogel particles in cigarette filter tip

Examples

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Effect test

example 1

[0035] Weigh chitosan and agarose in a mass ratio of 0.2:1 and place them in 2% citric acid solution at a ratio of 40% to prepare a uniform chitosan / agarose hydrogel after heating at 100°C. The resulting hydrogel is frozen The xerogel obtained after drying is mechanically pulverized and sieved to obtain chitosan / agarose xerogel powder. Chitosan / agarose xerogel powder is prepared into granules by high-speed stirring and granulation, dried at a constant temperature of 60°C for about half an hour to obtain chitosan / agarose xerogel particles, and sieved to obtain 20-40 mesh standards Sample particle 1.

example 2

[0037] Weigh chitosan and agarose at a mass ratio of 1:1 and place them in 1.5% citric acid solution at a ratio of 30% to prepare a uniform chitosan / agarose hydrogel after heating at 100°C. The resulting hydrogel is frozen The xerogel obtained after drying is mechanically pulverized and sieved to obtain chitosan / agarose xerogel powder. Chitosan / agarose xerogel powder is prepared into granules by high-speed stirring and granulation, dried at a constant temperature of 60°C for about half an hour to obtain chitosan / agarose xerogel particles, and sieved to obtain 20-40 mesh standards Sample particle 2.

example 3

[0039]Weigh chitosan and agarose according to the mass ratio of 2:1, place them in 1% citric acid solution at a ratio of 25% and heat them at 100°C to prepare a uniform chitosan / agarose hydrogel, and the resulting hydrogel is frozen The xerogel obtained after drying is mechanically pulverized and sieved to obtain chitosan / agarose xerogel powder. Chitosan / agarose xerogel powder is prepared into granules by high-speed stirring and granulation, dried at a constant temperature of 60°C for about half an hour to obtain chitosan / agarose xerogel particles, and sieved to obtain 20-40 mesh standards Sample particles3.

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Abstract

The invention provides a preparation method of chitosan / agarose xerogel particles and an application of the chitosan / agarose xerogel particles in a cigarette filter tip. The preparation method comprises the following steps: adding chitosan and agarose to a citric acid solution, conducting heating and stirring so as to obtain a clear solution, and cooling the clear solution to room temperature, so that a transparent hydrogel is obtained; and freeze-drying the transparent hydrogel so as to obtain a xerogel, conducting mechanical crushing and screening so as to obtain xerogel powder, conducting uniform mixing and implementing a high-speed stirring granulating method so as to obtain chitosan xerogel particles, drying the chitosan xerogel particles at constant temperature and sieving the particles so as to obtain target particle samples which are 20-40 meshes. A composite filter tip, which is added with the particles, can effectively improve a moisture content in smoke; and meanwhile, smoking quality of cigarette can be enhanced. In addition, the method is simple and easy to implement and is applicable to large-scale industrial production.

Description

technical field [0001] The invention belongs to the field of moisture-retaining materials for cigarette filters, in particular to the preparation of chitosan / agarose xerogel particles and their application in cigarette filters. Background technique [0002] With the development of the national economy, consumers and the market have higher and higher requirements for the quality of cigarettes, especially the quality of smoking. As the core competitiveness of Chinese-style cigarettes, the research and development of cigarette moisture retention technology has been highly concerned by the cigarette industry. But the traditional moisture retention technology has become more and more difficult to meet the requirements of improving the smoking quality of cigarettes. Improving the moisture retention performance of cigarettes, that is, the moisture content in the smoke during smoking can effectively improve the smoking taste and quality of cigarettes, thereby enhancing the core com...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A24B15/18
Inventor 吴彦刘鸿李志华周俊农李政陈义昌黄东业宁振兴宋凌勇潘连华黄宇亮黄善松胡超班强务文涛
Owner CHINA TOBACCO GUANGXI IND
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