False tooth adhesive and preparation method thereof
An adhesive and denture technology, which is applied to dental preparations, pharmaceutical formulations, dental prostheses, etc., can solve the problems of short action time, insufficient bonding strength, insufficient action time, etc., and achieves simple preparation method, low production cost, easy-to-achieve effects
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Embodiment 1
[0026] A kind of denture adhesive, is made up of base mixture and modified nano-diamond, the weight ratio of described modified nano-diamond and base mixture is 0.1%, and described base mixture is made up of following raw material: polyoxyethylene 0.3125g, carboxylate 0.1540 g of ethyl cellulose, 0.5625 g of montmorillonite, 1.2500 g of methyl cellulose, 0.5625 g of sodium alginate, and 12 ml of ethanol with a purity of 90%.
[0027] The modified nano-diamond is prepared by the following method: the nano-diamond is placed in a NaOH solution with a concentration of 0.11g / L, at a stirring speed of 60rpm and a temperature of 80°C, after stirring for 4h, the centrifugal speed is 4000rpm, Centrifuge for 30 minutes, take the precipitate and wash it repeatedly with deionized water until the pH value of the supernatant is 7; then dry it at 120°C for 4 hours, add to the silane coupling agent KH-550 with a mass fraction of 20% In the alcohol aqueous solution (the alcohol aqueous solutio...
Embodiment 2
[0033] A kind of denture adhesive, is made up of base mixture and modified nano-diamond, the weight ratio of described modified nano-diamond and base mixture is 0.05%, and described base mixture is made up of following raw material: polyoxyethylene 0.5g, carboxylate 0.1 g of ethyl cellulose, 0.6 g of montmorillonite, 2 g of methyl cellulose, 0.8 g of sodium alginate, and 13 ml of ethanol with a purity of 90%.
[0034] The modified nano-diamond is prepared by the following method: the nano-diamond is placed in a NaOH solution with a concentration of 0.11g / L, at a stirring speed of 100rpm and a temperature of 100°C, after stirring for 6h, the centrifugal speed is 4200rpm, Centrifuge for 10 minutes, take the precipitate and wash it repeatedly with deionized water until the pH value of the supernatant is 7; then dry it at 80°C for 12 hours, add to the silane coupling agent KH-550 with a mass fraction of 20% In the alcohol aqueous solution (the alcohol aqueous solution is prepared ...
Embodiment 3
[0040] A kind of denture adhesive, is made up of base mixture and modified nano-diamond, the weight ratio of described modified nano-diamond and base mixture is 0.3%, and described base mixture is made up of following raw material: polyoxyethylene 0.1g, carboxyl 0.4 g of ethyl cellulose, 0.8 g of montmorillonite, 1 g of methyl cellulose, 0.4 g of sodium alginate, and 12 ml of ethanol with a purity of 90%.
[0041] Refer to Example 1 for the preparation method of modified nano-diamond and denture adhesive.
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