A kind of functional ceramic powder material and its preparation method and application
A technology of powder materials and functional ceramics, used in capacitors, electrical components, etc., can solve the problems of complex process and difficult control, and achieve the effect of broad application prospects, high dielectric constant, and good pressure-sensitive nonlinearity.
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Embodiment 1
[0020] A functional ceramic powder material, consisting of the following components by weight: CaCO 3 20 parts, CuO 20 parts, Al 2 o 3 10 parts, Fe 2 o 3 15 parts, NiO 5 parts, Ti 3 C 2 20 servings.
[0021] This embodiment also provides a preparation method of a functional ceramic powder material, the specific steps are as follows:
[0022] Step 1, weigh the following components by weight: CaCO 3 20 parts, CuO 20 parts, Al 2 o 3 10 parts, Fe 2 o 3 15 parts, 5 parts of NiO, spare;
[0023] Step 2, the above-mentioned CaCO 3 , CuO, Al 2 o 3 , Fe 2 o 3 , NiO, Ti 3 C 2 Grinding to a particle size of 0.06 μm yields CaCO 3 Powder, CuO powder, Al 2 o 3 Powder, Fe 2 o 3 Powder, NiO powder;
[0024] Step 3. Take Ti 3 AlC 2 Put it into a plastic reaction container, slowly add a sufficient amount of hydrofluoric acid with a mass fraction of 40%, shake it for 10 minutes while adding, and react in a water bath at 60°C for 10 hours to obtain a reaction soluti...
Embodiment 2
[0029]A functional ceramic powder material, consisting of the following components by weight: CaCO 3 40 parts, CuO 35 parts, Al 2 o 3 20 parts, Fe 2 o 3 20 parts, NiO 10 parts, Ti 3 C 2 30 servings.
[0030] This embodiment also provides a preparation method of a functional ceramic powder material, the specific steps are as follows:
[0031] Step 1, weigh the following components by weight: CaCO 3 40 parts, CuO 35 parts, Al 2 o 3 20 parts, Fe 2 o 3 20 parts, 10 parts of NiO, spare;
[0032] Step 2, the above-mentioned CaCO 3 , CuO, Al 2 o 3 , Fe 2 o 3 , NiO, Ti 3 C 2 Grinding to a particle size of 0.08 μm yields CaCO 3 Powder, CuO powder, Al 2 o 3 Powder, Fe 2 o 3 Powder, NiO powder;
[0033] Step 3. Take Ti 3 AlC 2 Put it into a plastic reaction container, slowly add a sufficient amount of hydrofluoric acid with a mass fraction of 40%, shake it for 20 minutes while adding, and react in a water bath at 60°C for 20 hours to obtain a reaction solut...
Embodiment 3
[0038] A functional ceramic powder material, consisting of the following components by weight: CaCO 3 30 parts, CuO 30 parts, Al 2 o 3 15 parts, Fe 2 o 3 17 parts, NiO 8 parts, Ti 3 C 2 25 servings.
[0039] This embodiment also provides a preparation method of a functional ceramic powder material, the specific steps are as follows:
[0040] Step 1, weigh the following components by weight: CaCO 3 30 parts, CuO 30 parts, Al 2 o 3 15 parts, Fe 2 o 3 17 parts, 8 parts of NiO, spare;
[0041] Step 2, the above-mentioned CaCO 3 , CuO, Al 2 o 3 , Fe 2 o 3 , NiO, Ti 3 C 2 Grinding to a particle size of 0.07 μm yields CaCO 3 Powder, CuO powder, Al 2 o 3 Powder, Fe 2 o 3 Powder, NiO powder;
[0042] Step 3. Take Ti 3 AlC 2 Put it into a plastic reaction container, slowly add a sufficient amount of hydrofluoric acid with a mass fraction of 40%, shake it for 15 minutes while adding, and react in a water bath at 60°C for 15 hours to obtain a reaction solut...
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