A kind of metal chelating cationic emulsion for water-based wood sealing primer and preparation method thereof
A technology of cationic emulsion and sealing primer, applied in the field of emulsion, can solve the problems of tannic acid sealing and other problems, and achieve the effects of excellent sealing, high compactness and simple production process.
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preparation Embodiment 1
[0034]Add 20kg of cetyltrimethylammonium chloride and 300kg of deionized water into the reactor for mixing, and stir evenly until the cationic emulsifier is completely dissolved in the deionized water, then raise the temperature to 75°C to obtain an emulsifier solution. Subsequently, 410kg of acrylic acid and 270kg of deionized water were put into an emulsification tank for mixing and stirred for 25 minutes until the acrylic acid and deionized water were evenly mixed to obtain a pre-emulsion. Then add 90kg of pre-emulsion to the reaction kettle, that is, the emulsifier solution, then add 3.3kg of sodium ferric edetate and stir evenly, then raise the temperature of the reaction system to 80°C, and then continue to stir for 5 minutes to make the reaction system become The transparent system was then kept at a temperature of 80° C. for 20 minutes to make blue light appear in the reaction system. Afterwards, 354kg of pre-emulsion and 100kg of 5% ammonium persulfate aqueous solutio...
preparation Embodiment 2
[0036] Add 20kg of cetyltrimethylammonium chloride and 300kg of deionized water into the reactor for mixing, and stir evenly until the cationic emulsifier is completely dissolved in the deionized water, then raise the temperature to 75°C to obtain an emulsifier solution. Subsequently, 410kg of acrylic acid and 270kg of deionized water were put into an emulsification tank for mixing and stirred for 25 minutes until the acrylic acid and deionized water were evenly mixed to obtain a pre-emulsion. Then add 90kg of pre-emulsion to the reaction kettle, that is, the emulsifier solution, then add 4kg of sodium ferric edetate and stir evenly, then raise the temperature of the reaction system to 80°C, and then continue to stir for 5 minutes to make the reaction system become transparent. system, and then kept at a temperature of 80° C. for 20 minutes to make the reaction system appear blue light. Afterwards, 354kg of pre-emulsion and 100kg of 5% ammonium persulfate aqueous solution were...
preparation Embodiment 3
[0038] Add 20kg of cetyltrimethylammonium chloride and 300kg of deionized water into the reactor for mixing, and stir evenly until the cationic emulsifier is completely dissolved in the deionized water, then raise the temperature to 75°C to obtain an emulsifier solution. Subsequently, 410kg of acrylic acid and 270kg of deionized water were put into an emulsification tank for mixing and stirred for 25 minutes until the acrylic acid and deionized water were evenly mixed to obtain a pre-emulsion. Then add 90kg of pre-emulsion to the reaction kettle, that is, the emulsifier solution, and then add 3.6kg of sodium ferric edetate. After stirring evenly, the temperature of the reaction system is raised to 80°C, and then continues to stir for 5 minutes to make the reaction system change. It is a transparent system, and then kept at a temperature of 80° C. for 20 minutes to make the reaction system appear blue light. Afterwards, 354kg of pre-emulsion and 100kg of 5% ammonium persulfate ...
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