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69results about How to "The production process is simple and controllable" patented technology

Nitrogen and sulfur-codoped graphene quantum dot and preparation method thereof

The invention discloses a nitrogen and sulfur-codoped graphene quantum dot and a preparation method thereof. The preparation method comprises the steps that after a precursor pyrene is mixed with 80-100 ml of fuming nitric acid, refluxing and stirring are performed, nitro functionalizing treatment is performed on the surfaces of pyrene grains, a reactant is taken out, filtered and deacidified, an appropriate amount of NaOH is added to regulate the PH value, dispersion treatment is performed by adopting 300-W ultrasonic waves, the reactant is transferred into a polytetrafluoroethylene tank for a hydrothermal reaction, and after natural cooling is performed, a reactant is taken out, filtered, dialyzed and then dried; after a graphene quantum dot is dissolved into an appropriate amount of deionized water, an appropriate amount of ammonia water is added according to the proportion of the reactant, uniform mixing is performed, the mixture and an appropriate amount of sublimed sulfur are fully mixed to be uniform through stirring, the mixture is transferred into a polytetrafluoroethylene tank, a hydrothermal reaction is performed for 24 h by keeping the temperature of 180 DEG C-200 DEG C, and after cooling is performed, a reactant is taken out, filtered and dialysed to obtain the nitrogen and sulfur-codoped graphene quantum dot. The preparation method is simple in synthesis process, high in yield and finished product rate, environmentally friendly, poisonless, few in impurity and capable of easily obtaining the raw materials.
Owner:GUILIN UNIVERSITY OF TECHNOLOGY

SiC trench gate power MOSFET device and preparation method thereof

The invention relates to a SiC trench gate power MOSFET device, and belongs to the technical field of power semiconductors. The SiC trench gate power MOSFET device comprises a trench source structure,a P-type polycrystalline silicon and a trench gate structure which are manufactured in a trench. The trench source structure can reduce gate-drain capacitance (Cgd) and switching loss, when a sourcedielectric layer is made of a high-K dielectric material, the electric field intensity of a source dielectric can be effectively reduced, the P-type polycrystalline silicon realizes integration of anHJD in the N-channel SiC trench gate power MOSFET, the HJD has lower forward conduction voltage drop, conduction of a body diode is inhibited, a reliability problem caused by bipolar degradation is avoided, and the integrated HJD does not additionally increase the area of a chip. The integrated SiCHJD is a unipolar device, the reverse recovery characteristic is superior to that of a bipolar body diode, and stability is better due to the fact that parasitic parameters brought by an external diode lead are avoided, in addition, the device is simple and controllable in manufacturing process and high in compatibility with an existing process.
Owner:HANGZHOU SILICON-MAGIC SEMICON TECH CO LTD

Graded porous polyvinylidene fluoride hollow-fiber composite film and production method thereof

The invention relates to the technical field of water treatment and particularly relates to and discloses a graded porous polyvinylidene fluoride hollow-fiber composite film. The graded porous polyvinylidene fluoride hollow-fiber composite film comprises a graded porous macroporous middle layer, an outer separation layer and an inner separation layer which cover the two sides of the macroporous middle layer, wherein the three-layer structure is integrally made from the same material, pores of adjacent two layers communicate with one another, and structures of the outer separation layer and theinner separation layer are denser than that of the macroporous middle layer. The invention further discloses a production method of the composite film. The method comprises the steps: (1) preparing apolyvinylidene fluoride casting solution; (2) subjecting the casting solution to composite forming, so as to prepare complex type hollow fibers; (3) carrying out air spacing, then, carrying out water-bath coagulating forming, and carrying out traction winding, thereby obtaining the polyvinylidene fluoride hollow-fiber composite film. According to the graded porous polyvinylidene fluoride hollow-fiber composite film and the production method thereof, disclosed by the invention, the graded porous polyvinylidene fluoride hollow-fiber composite film has the advantages of small pore size, high flow rate, high strength and pollution resistance. The production method has the advantages that production procedures are simple and controllable, and the production cost is low.
Owner:ZHEJIANG CHANGXING CREFLUX MEMBRANE TECH CO LTD

Functional pipetting head with double purification functions of ultra-filtration and solid extraction and application of functional pipetting head

The invention relates to an experiment device for pretreatment on samples, and in particular to a functional pipetting head with double purification functions of ultra-filtration and solid extraction, and application of the functional pipetting head in pretreatment and quantitative analysis on a biological sample in the medicine analysis process. The functional pipetting head comprises a pipetting head body, a solid-phase extraction material and a hollow fiber membrane, wherein the hollow fiber membrane is arranged at the sharp end of the pipetting head body; an adhesive is uniformly applied at the cross part of the sharp end of the pipetting head and the hollow fiber membrane; an upper end opening and a lower end opening are formed in the hollow fiber membrane; the upper end opening is sealed; the lower end opening is kept in an opened state; the solid-phase extraction material is arranged inside the pipetting head body. The functional pipetting head is simple, convenient and controllable in manufacturing process, flexible in extraction condition adjustment, scientific and reasonable in method, convenient in obtaining materials, and good in application prospect.
Owner:ZHEJIANG ACAD OF TRADITIONAL CHINESE MEDICINE

Preparation method of RGD polypeptide grafted poly(maleic anhydride-hexamethylendiamine-DL-lactic acid)/modified hydroxyapatite porous composite material

InactiveCN104910410AHigh affinityPrevent aseptic necrosisProsthesisSide chainUltrasonic dispersion
The invention relates to a preparation method of an RGD polypeptide grafted poly(maleic anhydride-hexamethylendiamine-DL-lactic acid) / modified hydroxyapatite porous composite material. The preparation method comprises the following steps: (1) introducing maleic anhydride and hexamethylendiamine to a side chain of polylactic acid at first, and then grafting adhesive RGD polypeptide; (2) dissolving the generated RGD polypeptide grafted poly(maleic anhydride-hexamethylendiamine-DL-lactic acid) in dichloromethane, adding modified nano modified hydroxyapatite, performing ultrasonic dispersion, stirring fully to mix uniformly, weighing sodium chloride particles screened by a molecular sieve, adding the sodium chloride particles into the mixed solution and stirring; and (3) when a solvent is volatilized, drying to perform volatilization, and soaking the material in distilled water to separate out the sodium chloride particles, thereby obtaining the RGD polypeptide grafted poly(maleic anhydride-hexamethylendiamine-DL-lactic acid) / modified hydroxyapatite porous composite material at last. The preparation method provided by the invention has the advantages that a manufacturing process is simple and controllable.
Owner:WUHAN UNIV OF TECH

Method of machining special passivated stainless steel surface

The invention relates to a method of machining a special passivated stainless steel surface. The method includes a first step of cold rolling raw materials, rolling by adopting roller with 2.0 micrometers to 3.0 micrometers of roughness Ra, controlling cold rolling reduction rate within 5% to 10%, controlling rolling lubrication oil amount within 2000 liters per minute to 4000 liters per minute, a second step of passivating cold rolled materials, conducting annealing and pickling on cold rolled surfaces, controlling furnace temperature of an annealing furnace within 350 DEG C to 550 DEG C, controlling ratio of acid liquid in an acid groove to be 10 grams per liter to 25 grams per liter of hydrofluoric acid (HF) to 80 grams per liter to 200 gram per liter of hydrogen nitrate (HNO3), controlling pickling passivation temperature within 40 DEG C to 60 DEG C, and controlling running speed within 25 meters per minute to 40 meters per minute. Due to the facts that machining is conducted with the help of devices in a stainless steel enterprise and similar products are produced without need of additionally configuring a surface coating production line, production cost is greatly saved. Due to the fact that production technology process is relatively simple and controllable, production efficiency is high. Due to the fact that corrosion resistance of the surfaces which are pickled and passivated is greatly improved, stability is good.
Owner:NINGBO BAOXIN STAINLESS STEEL

Medicament for treating liver-yang hyperactivity, extinguishing liver-wind and nourishing kidney-yin as well as preparation method

The invention discloses medicine for treating liver-Yang hyperactivity, calming liver wind, and tonifying kidney yin and a preparation method. The medicine consists of Tuckahoe, scutellaria, uncaria, prunella, corn silk, cortex moutan, root of rehmannia, prepared rhizome of rehmannia, Chinese wolfberry, dogwood, radix cyathulae, Chinese yam, and medicated leaven. The preparation method comprises: firstly, soaking the Chinese yam in grain alcohol; secondly, soaking the prepared rhizome of rehmannia and the radix cyathulae in the grain alcohol; thirdly, drying and crushing the Tuckahoe, the scutellaria, the cortex moutan, chrysanthemum, the prunella, the uncaria, the corn silk, the Chinese yam, the root of rehmannia, the Chinese wolfberry, the dogwood, the medicated leaven, the prepared rhizome of rehmannia, and the radix cyathulae; and fourthly, putting fine powder into a sugar coating machine, adding 20 to 30 percent of dilute hydromel into the fine powder, stirring the mixture to prepare water-containing pills, and packaging the pills. The medicine has the advantages of reasonable formulation, remarkable medicine effect, full absorption, alleviation function, innocuousness, low cost, simple process, remarkable curative effect; in addition, the medicine can calm nerves, benefit kidney essence, fill encephalon, nourish Yin and calm wind. The preparation method has the advantages of simple process, remarkable curative effect, full absorption, alleviation function, innocuousness and low cost, and is suitable for industrialized production.
Owner:武汉市正兴和生物科技有限公司

III-V family nitride semiconductor epitaxial structure, device comprising epitaxial structure and preparation method thereof

The invention relates to a III-V family nitride semiconductor epitaxial structure comprising a (1) substrate; (2) an epitaxial buffer layer; (3) an epitaxial transition layer; and (4) an epitaxial effective layer. The epitaxial buffer layer is provided with an upper surface and a lower surface which is contacted with the substrate. The epitaxial transition layer covers the epitaxial buffer layer, and a microscopic hole structure is arranged at the interface of the epitaxial transition layer and the epitaxial buffer layer. The microscopic holes are periodically or non-periodically arranged so that the interface of the epitaxial transition layer and the epitaxial buffer layer is enabled to be partially connected, and the connected parts and the hole parts appear in a spacing way at the interface. The epitaxial transition layer is provided with a flat upper surface. The epitaxial effective layer is arranged at the upper surface of the epitaxial transition layer. The epitaxial effective layer comprises an n-type epitaxial layer, a luminescent layer and a p-type epitaxial layer which are arranged from the bottom to the top. The invention also provides a manufacturing method of the epitaxial structure, a device comprising the epitaxial structure and a manufacturing method thereof.
Owner:SHANGHAI XINYUANJI SEMICON TECH

Glass fiber enhanced high-density polyethylene (HDPE) double-walled winding pipe and manufacture method thereof

The invention relates to a glass fiber enhanced high-density polyethylene (HDPE) double-walled winding pipe, which is formed by spirally winding a glass fiber enhanced HDPE plastic pipe and welding the glass fiber enhanced HDPE plastic pipe by plastic hot melt adhesives, wherein the glass fiber enhanced HDPE plastic pipe is a hollow rectangular glass fiber enhanced HDPE plastic pipe with the long glass fiber content being 5 percent to 40 percent by weight. A manufacture method of the glass fiber enhanced HDPE double-walled winding pipe comprises the following steps that HDPE mixed materials are prepared, modified long glass fiber is prepared, the HDPE mixed materials and the modified long glass fiber take reaction and are coextruded into a hollow square pipe, and the hollow square pipe is made into the glass fiber enhanced HDPE double-walled winding pipe through spiral winding and plastic hot melt adhesive welding. The glass fiber enhanced HDPE double-walled winding pipe has the advantages that the creep resistance, the modulus, the impact resistance, the scratch resistance, the slow crack expansion resistance, the environment stress cracking resistance and the high-temperature resistance are good, the whole body has sufficient sewing stretching intensity, and the integral performance of pipelines is effectively improved.
Owner:SHANGHAI QINGYUAN PIPE TECH

Pharmaceutical composition and health care product and preparation method

The invention relates to the field of pharmaceuticals and particularly relates to a pharmaceutical composition and health care product and a preparation method. The pharmaceutical composition and health care product comprise haematoccus pluvialis which can regulate immune cells, enhance immunity, clear free radicals in a body, resist oxidation and relieve fatigue of the body, and can be used as a principal drug for playing a principal health care role; an aloe extract has the effects of relaxing the bowels with purgative, clearing liver-fire, clearing free radicals, resisting oxidation, reducing injuries caused by ultraviolet radiation, enhancing immunity and resisting tumors, and is used as an assistant drug for playing a complementary role; and villous amomum fruits and noni fruit pulp are matched to have the effects of removing dampness, appetizing, regulating qi, warming the spleen, improving insomnia, inflammation, pain, endocrine disorders and an immune system and realizing other nourishing and conditioning effects, and are respectively used as a complement drug and a guide drug for realizing the effects of consolidating basis and promoting drug efficacy. Aloe is a bitter cold product impairing the spleen, the villous amomum fruits are matched to warm the interior, reinforce the spleen, inhibit the coldness and prevent harming vital qi. Animal functional tests prove that the pharmaceutical composition and health care product can effectively realize the effects of resisting oxidation and alleviating physical fatigue, thereby being a good compound traditional Chinese medicine health care food.
Owner:HAINAN UNIVERSITY

Cold-fever-treating granules and preparation method thereof

The invention discloses cold-fever-treating granules and a preparation method thereof. The preparation method comprises the following steps: finishing and preparing 30-40% of folium isatidis, 30-40% of isatis root, 10-20% of fructus forsythiae and 10-20% of bistort rhizome, then adding water and decocting for twice while controlling the temperature, pressure, time, adding amount, solution discharge amount and times of the decoction, and then concentrating the decoction while controlling the temperature, pressure and solution charge amount during the concentration; then continuing to precipitate with ethanol, concentrating, precipitating with water, and concentrating into a paste with a weight which is not less than 12.5% of a raw medicine amount; crushing and sieving, drying, straightening and mixing, sub-packaging and packaging. The cold-fever-treating granules and the preparation method thereof disclosed by the invention have the following advantages: the prepared granules are sweet in taste, slightly bitter (without saccharose) and uniform, are capable of clearing away heat and toxic materials, and dispelling wind and relieving exterior syndrome, and are used for upper respiratory infection, acute tonsillitis, sphagitis, extrapelvic wind-heat, heat-toxin obstruction, fever and swollen sore throat; the production process is simple and easy to control, and only needs four medicinal materials.
Owner:HUBEI FUREN JINSHEN PHARMA

Diclofenac sodium dual-release enteric-coated preparation, as well as preparation method and control method thereof

The invention relates to a diclofenac sodium dual-release enteric-coated preparation, as well as a preparation method and a control method thereof. The diclofenac sodium dual-release enteric-coated preparation comprises the following components in percentage by weight: 11%-44% of microcrystalline cellulose, 2%-5% of ethyl cellulose, 3%-10% of povidone, 1%-6% of Eudragit S100, 2%-16% of Eudragit RL PO, 2%-12% of Eudragit RS PO, 1.5%-12% of tributyl citrate, 0.01%-0.1% of sodium hydroxide, 0.05%-1% of propylene glycol, 6%-15% of talc powder, 0.1% of silicon dioxide, 0.3% of titanium dioxide and 0.3% of dimethyl silicone oil, A and B pills with two release mechanisms are respectively prepared, and double-layer tablets, capsules or granules are prepared, wherein a prepared intermediate product has the laser spectral band pass of 5.0nm, the transmission spectral band pass of 10.0nm, the excitation wavelength of 340nm and the fluorescence intensity of 330-380 under the condition that the transmission wavelength is 510nm. The quality of the diclofenac sodium dual-release enteric-coated preparation disclosed by the invention is in line with the standard, and quality control is performed before production, so that rework can be reduced, the production cost can be saved, the energy consumption can be reduced and the production efficiency can be improved.
Owner:广东全瑞医药有限公司

Tandem liquid phase micro-extraction device and method for extracting, purifying and chemically deriving traditional Chinese medicine volatile oil

The invention relates to a tandem liquid phase micro-extraction device for extracting, purifying and chemically deriving a traditional Chinese medicine volatile oil. The tandem liquid phase micro-extraction device for extracting, purifying and chemically deriving the traditional Chinese medicine volatile oil comprises an extraction device, a purification device, and a chemical derivatization device; the extraction device comprises a fraction guiding tube, a first heating device and an extraction container; the purification device comprises a separation container, a cooling device, a volatile oil guiding tube, a separation hollow fiber membrane, a first quantitative syringe, and a pressure regulating tube; and the chemical derivatization device comprises a derivatization container, a secondheating device, a derivatization hollow fiber membrane, a sample receiving vial, a second quantitative syringe and an analyte guiding tube. The preparation process of the invention is simple and controllable, the application method is scientific and reasonable, the pre-treatment conditions are flexibly adjusted, the material is convenient to be taken, and the prospect is good.
Owner:ZHEJIANG ACAD OF TRADITIONAL CHINESE MEDICINE

Nitride semiconductor microcavity laser structure with low electric resistance and low thermal resistance

The invention provides a nitride semiconductor microcavity laser structure and a preparation method thereof. A microcavity laser is prepared on the (0001) nitrogen surface of a nitride semiconductor,and p-type ohmic contact on a (0001) gallium surface adopts a whole surface contact manner, so that the series resistance of the microcavity laser is greatly reduced; the heat of the microcavity laseris directly transferred into a heat sink with high heat conductivity, a microcavity laser is prepared on the (0001) nitrogen surface, and the side wall of the microcavity laser is manufactured by using a wet etching method, so that the stability of the microcavity laser can be greatly promoted, the optical limiting layer of the microcavity laser is prepared by using AlInGaN, ITO, AZO, IGZO, porous GaN, Ag, Al, ZnO, MgO, Si, SiO2, SiNx, TiO2, ZrO2, AlN, Al2O3, Ta2O5, HfO2, HfSiO4 and AlOH materials, and high optical limitation is provided. The novel nitride semiconductor microcavity laser structure provided by the invention has the advantages of low electric resistance, low thermal resistance, easy implementation of electric injection, high stability, high reliability and the like, the performance of the nitride semiconductor microcavity laser can be greatly enhanced, and the service life of the nitride semiconductor microcavity laser is greatly prolonged.
Owner:江西省纳米技术研究院 +1
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