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3502results about How to "Achieve mass production" patented technology

Co-N-C@RGO composite material, preparation method and application to modification of lithium-sulfur battery diaphragms

The invention discloses a method for preparing porous carbon@graphene composite material by taking a bimetal organic framework material as a precursor and application to modification of lithium-sulfur battery diaphragms thereof. The preparation method comprises the following steps: taking zinc salt and cobalt salt in a certain ratio as the raw materials, synthesizing a zinc / cobalt-bimetal organic framework@graphene composite material through a room-temperature liquid phase method, taking the zinc / cobalt-bimetal organic framework@graphene composite material as the precursor, carrying out high-temperature reaction under inert atmosphere, pickling and drying to obtain a cobalt / nitrogen double-doped porous carbon@graphene (Co-N-C@RGO) composite material. Co-N-C@RGO has high conductivity; the specific surface area of Co-N-C@RGO reaches up to 750-1000m<2> / g; the content of Co is 2-4At%; the content of N is 10-20At%. When the material is applied to the modification of the lithium-sulfur battery diaphragms, the material has the function of obviously inhibiting polysulfide shuttle effect and is capable of greatly improving actual specific capacity and cyclic performance of the lithium-sulfur batteries; meanwhile, the raw materials needed for synthesizing the material are simple; the operation is convenient; the large-scale production can be achieved; the material has certain promoting effect on commercialization of lithium-sulfur battery systems.
Owner:CENT SOUTH UNIV

Extrudable mixture for forming a porous block

An extrudable mixture is provided for producing a highly porous substrate using an extrusion process. More particularly, the present invention enables fibers, such as organic, inorganic, glass, ceramic or metal fibers, to be mixed into a mass that when extruded and cured, forms a highly porous substrate. Depending on the particular mixture, the present invention enables substrate porosities of about 60% to about 90%, and enables process advantages at other porosities, as well. The extrudable mixture may use a wide variety of fibers and additives, and is adaptable to a wide variety of operating environments and applications. Fibers, which have an aspect ratio greater than 1, are selected according to substrate requirements, and are mixed with binders, pore-formers, extrusion aids, and fluid to form a homogeneous extrudable mass. The homogeneous mass is extruded into a green substrate. The more volatile material is preferentially removed from the green substrate, which allows the fibers to interconnect and contact. As the curing process continues, fiber to fiber bonds are formed to produce a structure having a substantially open pore network. The resulting porous substrate is useful in many applications, for example, as a substrate for a filter or catalyst host, or catalytic converter.
Owner:GE02 TECH INC

Preparation method for vanadyl sulfate electrolyte of all-vanadium flow battery

The invention discloses a preparation method for vanadyl sulfate electrolyte of an all-vanadium flow battery. The preparation method is characterized by comprising the following steps of: adjusting pH value of vanadyl sulfate solution obtained from leaching vanadium slag and stone coal, back extracting and resin-analyzing treatments by using oxide or hydroxide of alkali metal or alkaline earth; adding an inorganic reducing agent; performing multi-grade counter-current extraction by using P204 or P507: TBP: sulfonated kerosene extracting agent; after the two-phase separation, washing the vanadium-loaded organic phase; performing 2-5 grades of multi-grade counter-current back extraction on the vanadium-loaded organic phase by using sulfuric acid solution to obtain the back extracting liquid of vanadyl sulfate; adjusting the pH value of the back extracting liquid of vanadyl sulfate, adding the organic reducing agent to adjust the potential value of the solution; extracting the solution by using the extracting agent; after the two-phase separation, washing the vanadium-loaded organic phase by using the sulfuric acid solution; performing multi-grade counter-current back extraction by using the sulfuric acid solution to obtain the vanadyl sulfate solution; and distilling until the concentration required for all-vanadium flow battery. The method provided by the invention can improve the purity, simplify the preparation procedure and reduce the cost.
Owner:GUANGDONG INST OF RARE METALS

Preparation method of titanium dioxide/active carbon composite nanofibrous membrane

The invention provides a preparation method of a titanium dioxide / active carbon composite nanofibrous membrane, characterized by comprising the following specific steps: dissolving polyacrylonitrile powder in N, N-dimethyl formamide; mixing titanium hydroxide gel with the polyacrylonitrile solution to obtain electrostatic spinning stock solution, and performing electrostatic spinning to get the composite nanofibrous membrane; placing the composite nanofibrous membrane in an electrically heated drying cabinet for being pre-oxidized; soaking the composite nanofibrous membrane in phosphoric acid or potassium hydroxide solution, washing the solution to be neutral by distilled water, and drying the composite nanofibrous membrane in the drying cabinet; and then, under nitrogen protection, heating up to 450-550 DEG C, and cooling to room temperature to get the titanium dioxide / active carbon composite nanofibrous membrane. The preparation method improves combination firmness between fibers and active ingredients of a photocatalyst, and also improves charge capacity of the fibers; the titanium dioxide / active carbon composite nanofibrous membrane is high in photo catalytic activity, good in absorption effect, reproducible and simple in a reproduction method, and can use sunlight, so that operations are easy and operation cost is low.
Owner:DONGHUA UNIV

Preparation method and application of electrochemical micro-fluidic sensing chip

The invention provides a preparation method and the application of an electrochemical micro-fluidic sensing chip. The preparation method comprises the following steps: directly coating an improved glass solution on a commercial standard printed electrode; and performing vacuum plasma treatment on a PDMS (Polydimethylsiloxane) chip with pre-designed pipelines and the printed electrode coated with the glass solution together, and directly bonding the PDMS chip on the commercial standard printed electrode to form a novel electrochemical microfluidic sensing platform. A sensor provided by the invention can perform ultrasensitive detection on various sample analytes in a biological fluid sample, taking the detection of a prostate cancer marker PSA (Prostate-specific Antigen) in human serum as an example, a coulomb amperometry is used for detection, and a result shows that the detection sensitivity can reach 0.84 pg / mL which is improved by two magnitudes than the standardized clinical testing requirement of 0.1 ng / mL, so that the sensor has superhigh detection sensitivity and accuracy, which are higher than those of other electrochemical detection devices, is convenient in operation, and can integrates sample processing, separation and the like on one micro electrochemical microfluidic sensing chip.
Owner:SHANGHAI JIAO TONG UNIV

Method for preparing load type nano arsenic-removing sorbent for drinking water

The invention relates to the elimination of the arsenic in drinking water, in particular to a preparation method of a supported type nano-adsorbent for removing arsenic from drinking water; the method includes the following steps: (1) activated carbon material with pore volume of 0.100-0.500cm<3> / g is selected for pretreatment; (2) soluble ferric salt solution is firstly used for soaking the activated carbon for 10-120 min; (3) alcoholic solution is taken as a dispersant to be added into the ferric salt solution; (4) under the protection of inert gases at room temperature, a strong reductant, potassium borohydride or sodium borohydride, is used for titrating the ferric salt, and agitation is carried out under the protection of inert gases; after the titration of potassium borohydride or sodium borohydride solution, agitation lasts for 10-120 min; (5) after agitation, centrifugation is carried out; oxygen-free water is firstly used for washing for 1-3 times, then organic solvent is adopted for washing for 1-3 times, and vacuum drying is done at 40-100 DEG C for 12-48h to obtain the product. The adsorbent of the invention has large adsorption capacity and small volume and is safe, stable and easy to store and transport.
Owner:SHENYANG INST OF APPL ECOLOGY CHINESE ACAD OF SCI

Mesoporous graphene foam as well as preparation method thereof

The invention belongs to the technical fields of a novel material as well as preparation, and particularly relates to mesoporous graphene foam as well as a preparation method thereof. The invention realizes hydrothermal preparation of a magnesium oxide texture structure and preparation of the mesoporous graphene foam by using textured magnesium oxide as a template. The mesoporous graphene foam material has abundant mesoporous structures and excellent electric property and can be used as an electrode material of batteries and supercapacitors, so that the energy density and the power density of the batteries or the supercapacitors are expectedly improved to a great extent. The cycling stability of the mesoporous graphene foam material is increased, and the mesoporous graphene foam material combined with materials with high draw ratio or the mesoporous graphene foam material can soften energy storage apparatuses. The advantages have important meaning for realization of commercialization of a new generation of energy storage apparatuses for electromobiles and development of smaller, lighter and flexible portable mobile power supplies. The business prospect is wide. Meanwhile, preparation processes of the high temperature hydrothermal method and a fluidized bed can realize engineering enlargement, so that the method is expected to be industrialized.
Owner:TSINGHUA UNIV

Silica-based three-dimensional heterogeneously-integrated radio frequency microsystem and manufacturing method thereof

The invention discloses a silica-based three-dimensional heterogeneously-integrated radio frequency microsystem and a manufacturing method thereof. The silica-based three-dimensional heterogeneously-integrated radio frequency microsystem comprises a first silica substrate layer, a second silica substrate layer, a third silica substrate layer, a fourth silica substrate layer, a radio frequency power amplification chip, a radio frequency low noise amplification chip, a radio frequency filter and a radio frequency switch, wherein the silica substrate layers are high-resistance silicon wafers; radio frequency chips and devices are made of different substrate materials through different processes; the radio frequency chips and devices are assembled inside cavities pre-etched in the first silicasubstrate layer and the third silica substrate layer; the first silica substrate layer, the second silica substrate layer, the third silica substrate layer and the fourth silica substrate layer are processed through low-temperature wafer-scale bonding into a whole and vertically connected through silicon through holes to form the silica-based three-dimensional heterogeneously-integrated radio frequency microsystem. The silica-based three-dimensional heterogeneously-integrated radio frequency microsystem achieves tree-dimensional integration of heterogeneous radio frequency chips and devices,thereby reducing the size, increasing the packaging density, reducing transmission loss of wire connection and enhancing the properties.
Owner:GREAT MICROWAVE TECH CO LTD
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