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Process for preparing natural magnesium aluminium silicate gel

A technology of magnesium aluminum silicate and magnesium silicate, which is applied in the direction of aluminum silicate and silicate, can solve the problems of reducing the purification and separation effect, poor pulp dispersion effect, and poor purification effect, so as to improve the concentration of pulping operation, Achieve large-scale production and avoid iron pollution

Inactive Publication Date: 2002-08-14
国家非金属矿深加工工程技术研究中心
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  • Claims
  • Application Information

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Problems solved by technology

[0004] Although the above-mentioned results have achieved preliminary results in exploring the preparation technology of natural magnesium aluminum silicate gel, from the perspective of practical application, there are still following defects: 1, because the third step adopts natural sedimentation method (or gravity method) in Purify the mineral particles in the pulp in a static state, and the operating concentration is strictly limited. In other words, the concentration of the pulp must be lower than the solid-liquid ratio of 1:10, that is, the concentration by weight must be lower than 9%, otherwise the pulp will be affected by the concentration. Too high and too high viscosity lead to poor purification effect
Moreover, the purification process of natural sedimentation method is slow, generally takes 14 to 16 hours, and the production efficiency is extremely low
2. In the second step, if a viscosity reducer is used, the viscosity and colloidal properties of the final product will be greatly reduced. If the viscosity reducer is not used, the dispersion effect of the pulp will be poor, which will greatly reduce the purification and separation effect. Do not dare to use viscosity reducer or strictly control the dosage during the purification process, which leads to insufficient dispersion of pulp, which also leads to poor purification effect and low purification degree of target minerals in the product, which directly affects the application range of the product
3. Due to the low degree of mineral purification and the simple modification process, the quality of the final gel product is poor. The gel viscosity of its 5% aqueous dispersion is only 40-60 mPa·s, and the thixotropy value is only 1.3- 1.4, and the stability of the gel is poor

Method used

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  • Process for preparing natural magnesium aluminium silicate gel
  • Process for preparing natural magnesium aluminium silicate gel
  • Process for preparing natural magnesium aluminium silicate gel

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Embodiment

[0030]Embodiment: referring to shown in accompanying drawing 2, a kind of preparation method of natural magnesium aluminum silicate gel, take natural smectite mineral as raw material, prepare according to the following steps:

[0031] 1. The smectite ore (mainly composed of MgO 7.0% CaO 13.70% Al 2 o 3 9.32% Fe 2 o 3 2.64%) is crushed to a fineness of 100-200 mesh mineral powder through an iron-free medium.

[0032] 2. Add water to the ore powder to make a slurry with a concentration of 20-30% by weight, and pound it for 40 minutes. When pounding, add 0.5-10% of dry ore weight to the slurry. Sodium hexametaphosphate.

[0033] 3. The ore pulp obtained from the pulping operation is sorted by the secondary hydrocyclone, and the ore feeding pressure is 0.1-0.5Mpa (MPa), and the overflow ore pulp obtained is then purified by a centrifugal classifier under the condition of a separation factor of 600-2000 Separation to obtain purified pulp with a concentration of 4% to 5%. In ...

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Abstract

A process for preparing natural gel of magnesium aluminium silicate from bentonite, attapulgite, bentone, etc includes such steps as pulverizing, preparing slurry, adding pour depressor, stirring, dynamic centrifugal separation, adding inorganic salt containing one-valence metal ions, stirring, pre-activating, adding organic salt containing at least Na ions, stirring for modifying, and post-treating.

Description

technical field [0001] The invention relates to a method for preparing inorganic gel, in particular to a method for preparing natural magnesium-aluminum silicate gel by using clay minerals containing magnesium-aluminum components as raw materials. Background technique [0002] Natural magnesium aluminum silicate gel is a purified and modified mineral gel material obtained from clay minerals containing magnesium and aluminum components through purification, purification, modification and other processes. This mineral gel material has an amazing expansion ability in water, and can form a gel with a house-of-card structure. It becomes thin under action and has good fluidity. It is an excellent viscosity regulator, thickener, suspending agent, emulsion stabilizer, and fluid thixotropy regulator. It is widely used in daily chemicals, pharmaceuticals, building materials, paints, petroleum, etc. Industries such as drilling, rubber and precision casting. ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01B33/26
Inventor 程卫泉
Owner 国家非金属矿深加工工程技术研究中心
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