A kind of production method of industrial grade ammonium dihydrogen phosphate co-production water-soluble fertilizer
A technology of high-grade ammonium dihydrogen phosphate and its production method, which is applied in the direction of ammonium orthophosphate fertilizer, alkaline orthophosphate fertilizer, phosphate fertilizer, etc., and can solve the problem of low direct utilization rate, poor material uniformity, useless industrial monoammonium phosphate, etc. question
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Embodiment 1
[0049] Embodiment 1: Industrial grade ammonium dihydrogen phosphate co-production water-soluble fertilizer production process:
[0050] 1. Production process of ammonium dihydrogen phosphate
[0051] 1.1. Mix wet-process phosphoric acid and phosphate rock powder as a desulfurizing agent evenly, and then enter the desulfurization reactor for desulfurization reaction. The desulfurization reaction temperature is 70°C, and the reaction time is 30 minutes. After the reaction, the desulfurized phosphoric acid slurry is sent to the push material Centrifugal separation in a screw centrifuge, the filtrate is sent to a neutralizer for neutralization reaction with liquid ammonia, the temperature of the first neutralization reaction is 70°C, and the pH value of the neutralization reaction slurry is 4;
[0052]1.2. After the neutralization reaction in step 1.1 is completed, the slurry is sent to a pusher screw centrifuge for centrifugation, and the centrifuged filtrate of the primary neutr...
Embodiment 2
[0058] Embodiment 2: Industrial grade ammonium dihydrogen phosphate co-production water-soluble fertilizer production process:
[0059] 1. Production process of ammonium dihydrogen phosphate
[0060] 1.1. Mix wet-process phosphoric acid and phosphate rock powder as a desulfurizing agent evenly, and then enter the desulfurization reactor for desulfurization reaction. The desulfurization reaction temperature is 85°C, and the reaction time is 40 minutes. After the reaction, the desulfurized phosphoric acid slurry is sent to the push material Centrifugal separation in a screw centrifuge, and the filtrate is sent to a primary neutralizer for neutralization reaction with liquid ammonia. The temperature of the primary neutralization reaction is 80°C, and the pH value of the neutralization reaction slurry is 4.3;
[0061] 1.2. After the neutralization reaction in step 1.1 is completed, the slurry is sent to a pusher screw centrifuge for centrifugation, and the centrifugal filtrate of ...
Embodiment 3
[0067] Embodiment 3: Industrial grade ammonium dihydrogen phosphate co-production water-soluble fertilizer production process:
[0068] 1. Production process of ammonium dihydrogen phosphate
[0069] 1.1. Mix wet-process phosphoric acid and phosphate rock powder as a desulfurizing agent evenly, and then enter the desulfurization reactor for desulfurization reaction. The desulfurization reaction temperature is 90°C, and the reaction time is 50 minutes. After the reaction, the desulfurized phosphoric acid slurry is sent to the push material Centrifugal separation in a screw centrifuge, the filtrate is sent to a neutralizer for neutralization reaction with liquid ammonia, the temperature of the first neutralization reaction is 90°C, and the pH value of the neutralization reaction slurry is 4.6;
[0070] 1.2. After the neutralization reaction in step 1.1 is completed, the slurry is sent to a pusher screw centrifuge for centrifugation, and the centrifugal filtrate of the primary ne...
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