Self-emulsifying heavy oil viscosity reducer as well as preparation method and application thereof
A heavy oil viscosity reducer and self-emulsifying technology, which is applied in chemical instruments and methods, earthwork drilling, and fluid production, etc. problems such as low content of qualitative components, to achieve good economic and social benefits, good viscosity reduction effect, and improved recovery effect.
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Embodiment 1
[0027] Example one: Preparation of self-emulsifying thick oil viscosity reducer one
[0028] a. Modification of silica: add 3 parts by weight of propanol to the container, adjust the pH to 4.5 with formic acid, then add 0.5 parts by weight of water and mix well, add 1.5 parts by weight of diethylene triacetate while stirring Aminopropyltrimethoxysilane and 0.5 parts by weight of hexamethyldisilazane are fully hydrolyzed to obtain a modifier; 80 parts by weight of silica are added to 1000 parts by weight of deionized water, and then Adding 20 parts by weight of modifier, heating and refluxing for 3 hours, and drying the reaction product at 100°C to obtain modified silica;
[0029] b. Synthesis of self-emulsifying thick oil viscosity reducer: 92 parts by weight of modified silica are added to 500 parts by weight of absolute ethanol, and then 5 parts by weight of alkylphenol ether sulfosuccinate sodium salt And 3 parts by weight of acrylamide, stir to dissolve, heat to 70°C, replace ...
Embodiment 2
[0030] Embodiment two: Preparation of self-emulsifying thick oil viscosity reducer II
[0031] a. Modification of silica: add 5 parts by weight of propanol to the container, adjust the pH to 4.5 with formic acid, then add 1.5 parts by weight of water and mix well, add 2.5 parts by weight of diethylene triacetate while stirring Aminopropyltrimethoxysilane and 1.5 parts by weight of hexamethyldisilazane are fully hydrolyzed to obtain a modifier; 90 parts by weight of silica are added to 1000 parts by weight of deionized water, and then Adding 10 parts by weight of modifier, heating and refluxing for 6 hours, and drying the reaction product at 100°C to obtain modified silica;
[0032] b. Synthesis of self-emulsifying thick oil viscosity reducer: adding 96 parts by weight of modified silica to 500 parts by weight of absolute ethanol, and then adding 3 parts by weight of alkylphenol ether sulfosuccinate sodium salt And 1 part by weight of acrylamide, stirred and dissolved, heated to 7...
Embodiment 3
[0033] Embodiment three: Preparation of self-emulsifying thick oil viscosity reducer three
[0034] a. Modification of silica: add 4 parts by weight of propanol to the container, adjust the pH to 4.5 with formic acid, then add 1 part by weight of water and mix well, add 2 parts by weight of diethylene triacetate while stirring Aminopropyltrimethoxysilane and 1 part by weight of hexamethyldisilazane are fully hydrolyzed to obtain a modifier; 85 parts by weight of silica are added to 1000 parts by weight of deionized water, and then Adding 15 parts by weight of modifier, heating and refluxing for 4.5 hours, and drying the reaction product at 100°C to obtain modified silica;
[0035] b. Synthesis of self-emulsifying thick oil viscosity reducer: 94 parts by weight of modified silica are added to 500 parts by weight of absolute ethanol, and then 4 parts by weight of alkylphenol ether sulfosuccinate sodium salt And 2 parts by weight of acrylamide, stir to dissolve, heat to 70°C, replac...
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