Energy spectrum analysis method for large-size samples

An analytical method and large-volume technology, applied in the field of energy spectrum analysis of large-volume samples, can solve cumbersome and complicated problems, and achieve the effect of simple method, simple energy spectrum analysis method, and easy operation

Active Publication Date: 2018-10-12
NANJING UNIV OF AERONAUTICS & ASTRONAUTICS
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Problems solved by technology

[0006] The purpose of the present invention is to solve the inadequacies of the current gamma spectrum analysis method, such as cumbersome and complicated, through neutron self-shielding correction, transform the nonlinear problem between the element content and the characteristic response into a linear problem, and invert the single element response spectrum, Build a single element response library

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  • Energy spectrum analysis method for large-size samples
  • Energy spectrum analysis method for large-size samples
  • Energy spectrum analysis method for large-size samples

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Embodiment Construction

[0038] In order to enable those skilled in the art to better understand the technical solutions in the present application, the technical solutions in the embodiments of the present application will be clearly and completely described below in conjunction with the drawings in the embodiments of the present application.

[0039] see figure 1 , a gamma energy spectrum analysis method for large-volume samples, comprising the following steps:

[0040] Step 1: Set a sample with a certain concentration gradient, irradiate the sample with a neutron source without changing the surrounding environment, and obtain the gamma energy spectrum of the sample based on the scintillator detector.

[0041] Specifically, based on the principle of PGNAA technology, the neutron flow generated by the neutron source is used to bombard the nuclei of various elements in the sample, and the nuclei undergo reactions such as radiation capture and inelastic scattering, and emit gamma rays with energy of 2k...

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Abstract

The invention relates to an energy spectrum analysis method for large-size samples. Based on an instantaneous gamma-ray neutron activation analysis technique, gamma energy spectra are obtained by a scintillator detector. The obtained gamma energy spectra are subjected to neutron self-shielding correction treatment according to the element nonlinear response. The gamma energy spectra are analyzed by a least square method, single element response energy spectra are obtained, a single element spectral library is established, and nuclides in the samples can be identified and analyzed by the singleelement spectral library. Aiming at the defect that other spectral library analysis methods require a large number of samples, the single element spectral library which is not affected by backgroundelements is obtained by a few of calibrated samples based on a physical mechanism of the influence of multielement components on PGNAA analysis results. The measured energy spectra can be fitted directly by the single element spectral library, and the fast and accurate analysis of the nuclides in complex samples having multiple components and different reaction cross sections can be achieved.

Description

technical field [0001] The invention relates to the field of gamma energy spectrum analysis, in particular to an energy spectrum analysis method for large-volume samples. Background technique [0002] At present, in the field of measurement and analysis, PGNAA has become a routine analysis and detection technology. It has many advantages that other analysis techniques do not have, including high penetration, non-destructive, on-line in-situ measurement, and high analysis accuracy. Based on its unique advantages, it has been widely used in various fields such as social security, industry, environment, and medicine in recent years. The principle of PGNAA technology is to use neutrons to bombard the target nucleus of the material to be tested, and through thermal neutron capture, inelastic scattering and other reactions in a very short time (less than 10 -13 s) Emitting characteristic gamma rays, by detecting characteristic gamma rays and measuring the intensity of characteri...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N23/20066
CPCG01N23/20066
Inventor 黑大千李佳桐贾文宝程璨孙爱赟汤亚军
Owner NANJING UNIV OF AERONAUTICS & ASTRONAUTICS
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