Abalone shell/calcium sulfate active bone cement and preparation method thereof
An abalone shell and bone cement technology, which is applied in the field of biological material preparation, can solve problems such as random discarding of abalone shells, and achieve the effects of good bone conductivity, mild conditions and stable crystal form.
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Embodiment 1
[0030] 1) Add 10g CaSO 4 2H 2 O was added to a 50ml beaker, 40ml of ultrapure water was added, and magnetically stirred for 1h to prepare a uniformly mixed suspension;
[0031] 2) Weigh 0.2g inorganic crystallization agent CaCl 2 and 0.08g organic crystallization agent succinic acid, it is added in the suspension liquid that step (1) makes, and magnetic force stirs 1h to make it fully dissolve, makes mixed solution;
[0032] 3) Transfer the mixed liquid obtained in step (2) to a high-pressure reactor, put it in an oven for hydrothermal reaction at 90°C for 10 hours, take out the reactor immediately after the reaction, and immediately transfer it to a high-pressure reactor heated to 90°C after boiling water suction filtration. Dry completely in the oven to get CaSO 4 1 / 2H 2 O powder;
[0033] 4) Remove the outer layer of the abalone shell with an electric file, crush and grind the inner layer until it passes through a 100-mesh filter to obtain abalone shell powder;
[003...
Embodiment 2
[0037] 1) Add 10g CaSO 4 2H 2 O was added to a 50ml beaker, 40ml of ultrapure water was added, and magnetically stirred for 2h to prepare a uniformly mixed suspension;
[0038] 2) Weigh 0.2g inorganic crystallization agent CaCl 2and 0.08g organic crystallization agent succinic acid, it is added in the suspension that step (1) prepares, and magnetic force stirs 2h to make it fully dissolve, and makes mixed solution;
[0039] 3) Transfer the mixed liquid obtained in step (2) to a high-pressure reactor, put it in an oven for hydrothermal reaction at 150°C for 8 hours, take out the reactor immediately after the reaction, and immediately transfer it to a high-pressure reactor heated to 100°C after boiling water suction filtration. Dry completely in the oven to get CaSO 4 1 / 2H 2 O powder;
[0040] 4) Remove the outer layer of the abalone shell with an electric file, crush and grind the inner layer until it passes through a 100-mesh filter to obtain abalone shell powder;
[004...
Embodiment 3
[0044] 1) Add 10g CaSO 4 2H 2 O was added to a 50ml beaker, 40ml of ultrapure water was added, and magnetically stirred for 1h to prepare a uniformly mixed suspension;
[0045] 2) Weigh 0.2g inorganic crystallization agent CaCl 2 and 0.08g organic crystallization agent succinic acid, it is added in the suspension liquid that step (1) makes, and magnetic force stirs 1h to make it fully dissolve, makes mixed liquor;
[0046] 3) Transfer the mixture obtained in step (2) to a high-pressure reactor, put it in an oven for hydrothermal reaction at 130°C for 6 hours, take out the reactor immediately after the reaction, and immediately transfer it to a high-pressure reactor heated to 130°C after boiling water suction filtration Dry completely in the oven to get CaSO 4 1 / 2H 2 O powder;
[0047] 4) Remove the outer layer of the abalone shell with an electric file, crush and grind the inner layer until it passes through a 100-mesh filter to obtain abalone shell powder;
[0048] 5) D...
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