High temperature resistance three-dimensional manufacture material and a method for manufacturing three-dimensional object with same
A three-dimensional manufacturing, high temperature resistance technology, applied in the direction of additive processing, etc., can solve the problems of limited application scope of products and poor high temperature resistance effect.
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Embodiment 1
[0043] Stir and mix 67wt% of 2,2-bis(4-cyanophenyl)propane and 30wt% acrylated epoxy resin at 150°C for 30 minutes, after cooling, add 3wt% of photoinitiator,
[0044] After the above materials were mixed, they were formed using the light-curing three-dimensional manufacturing equipment as described herein. After the three-dimensional manufacturing, the three-dimensional structure 5 was taken out, rinsed with alcohol solution and placed in an oven set at 110°C for 12 hours. After that, three-dimensional manufacturing is completed. The glass transition temperature of the three-dimensional object is about 208°C.
Embodiment 2
[0046] 67wt% benzoxazine and 30wt% phthalonitrile resin were stirred and mixed for 2 hours, after cooling, 3wt% photoinitiator was added,
[0047] After mixing the above-mentioned materials, use the light-curing three-dimensional manufacturing equipment as described in this article to form them. During the forming process, cool the materials so that the temperature does not exceed 25°C. Rinse and place in an oven set at 30°C for 24 hours, after heating, the 3D fabrication is complete. The glass transition temperature of the three-dimensional object is about 236°C.
Embodiment 3
[0049] Stir and mix 67wt% of 2,2-bis(4-cyanophenyl)propane and 30wt% acrylated epoxy resin at 150°C for 30 minutes, after cooling, add 3wt% of photoinitiator,
[0050] After the above materials were mixed, they were formed using the light-curing three-dimensional manufacturing equipment as described herein. After the three-dimensional manufacturing, the three-dimensional structure 5 was taken out, rinsed with alcohol solution and placed in an oven set at 200°C for 6 hours. After heating After that, three-dimensional manufacturing is completed. The glass transition temperature of the three-dimensional object is about 224°C.
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