Porous medium reaction heat effect monitoring device and method
A technology of porous media and monitoring devices, applied in the direction of material thermal development, etc., can solve the problems of unfavorable catalyst evaluation, affecting oxidation/combustion reaction and catalyst catalytic activity, and achieve the effect of increasing difficulty
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[0052] Before the experiment, crude oil and quartz sand were mixed evenly at a mass ratio of 1:4. According to the above-mentioned experimental method, the transparent quartz reactor 1 was filled and a differential thermocouple 5 was placed, the filling length of the reaction sample was 5 cm, and the temperature-rising oxidation experiment was carried out at an air flow rate of 1 L / min. After the transparent quartz reactor 1 is continuously heated to 455°C, stop heating up, keep the transparent quartz reactor at a constant temperature of 455°C, and close the control valve 1 81 and the gas flow meter 71 above the high-pressure air bottle 91 at 115 minutes, and open the high-pressure Control valve one 81 and gas flowmeter 71 above the helium gas cylinder 92, monitor the temperature of the two differential thermocouples 5 on the computer, when it is found that the temperature difference between the two differential thermocouples 5 gradually decreases, and the temperature of the re...
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