Adhesive for bottom-sprayed powder air supply element, preparation method and bonding method thereof
A gas supply element and adhesive technology, which is applied in the field of refractory materials, can solve the problems of short service life of the bottom dusting gas supply element, easy loosening of the inner lining pipe and outer casing, and weak bonding of the adhesive. Excellent bonding performance, tight and firm bonding, and the effect of improving the bonding effect
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Embodiment 1
[0043](1) Take by weighing 50 parts of alumina powder with a particle size of 160 objects and 50 parts of aluminum dihydrogen phosphate liquid respectively;
[0044] (2) Add 26 parts of alumina powder into the liquid phosphate and stir for 3 minutes to obtain the first viscous solution;
[0045] (3) Add 12 parts of alumina powder into the first viscous solution and stir for 5 minutes to obtain the second viscous solution;
[0046] (4) Add 12 parts of alumina powder into the second viscous solution and stir for 20 minutes to obtain a homogeneous solution;
[0047] (5) Apply the homogeneous solution on the outer wall of the inner lining tube and the inner wall of the outer casing of the bottom spraying powder air supply element, slowly insert the inner lining tube into the outer casing and continue to apply the adhesive to ensure full filling, at 2°C / min Raise the temperature to 140°C and keep it warm for 2 hours; at a heating rate of 5°C / min, raise the temperature to 180°C, ke...
Embodiment 2
[0049] (1) Take by weighing 80 parts of alumina powders with a particle size of 350 objects and 20 parts of aluminum dihydrogen phosphate liquid respectively;
[0050] (2) Add 40 parts of alumina powder into liquid phosphate, stir for 5 minutes to obtain the first viscous solution;
[0051] (3) Add 20 parts of alumina powder into the first viscous solution and stir for 10 minutes to obtain the second viscous solution;
[0052] (4) Add 20 parts of alumina powder into the second viscous solution and stir for 40 minutes to obtain a homogeneous solution;
[0053] (5) Apply the homogeneous solution to the outer wall of the inner lining tube and the inner wall of the outer casing of the bottom powder spraying air supply element, slowly insert the inner lining tube into the outer casing and continue to apply the adhesive to ensure full filling, at 5°C / min Raise the temperature to 80°C and keep it warm for 4 hours; at a heating rate of 10°C / min, raise the temperature to 260°C, keep i...
Embodiment 3
[0055] (1) Take by weighing 60 parts of alumina powder with a particle size of 180 objects and 40 parts of aluminum dihydrogen phosphate liquid respectively;
[0056] (2) Add 30 parts of alumina powder into the liquid phosphate, and stir for 3 minutes to obtain the first viscous solution;
[0057] (3) Add 15 parts of alumina powder into the first viscous solution and stir for 5 minutes to obtain the second viscous solution;
[0058] (4) Add 15 parts of alumina powder into the second viscous solution and stir for 20 minutes to obtain a homogeneous solution;
[0059] (5) Apply the homogeneous solution on the outer wall of the inner lining tube and the inner wall of the outer casing of the bottom spraying powder air supply element, slowly insert the inner lining tube into the outer casing and continue to apply the adhesive to ensure full filling, at 2°C / min Raise the temperature to 120°C and keep it warm for 2 hours; at a heating rate of 5°C / min, raise the temperature to 200°C, ...
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