The invention relates to 
yttrium aluminum garnet and 
yttrium oxide double-
crystal transparent 
ceramic as well as the preparation method thereof. The transparent 
ceramic is characterized in that the YAG and Y2O3 double-
crystal transparent 
ceramic is prepared under the conditions that the weight percentage of 
yttrium aluminum garnet and yttrium 
oxide range from 60 percent to 99.99 percent, and the weight percentage of Y2O3 ranges from 40 percent to 39.9 percent. The preparation of the double-
crystal transparent ceramic is mainly divided into two stages: firstly, YAG and Y2O3 are mixed with a milling medium, a 
grinding ball and 
sintering additives (0.01 to 5.0 wt percent of the 
sintering additives is further added), the 
slurry is dried to obtain composite 
powder, and the composite power is screened; and secondly, the composite 
powder is subjected to static pressure molding through 
dry pressing and temperature reduction, and is sintered under no pressure, the 
sintering temperature is 1,650 DEG C to 1,850 DEG C, and the 
holding time is 1 hour to 50 hours. The maximum transmission efficiency of the 2mm double-crystal transparent ceramic within the 
wave band of 400 nm to 1,100 nm can reach more than 81 percent. The preparation method has the advantages of wide 
raw material sources, simple process and convenient control. The double-crystal transparent ceramic is applicable to the 
laser and 
luminescence field by serving as matrix materials.