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Oil-based plugging agent and preparation method thereof

A leakage plugging agent, oil-based technology, applied in the field of oil-based leakage blocking agent and its preparation, can solve the problem of deterioration, degradation, poor durability of leakage plugging effect, great influence on rheological properties of oil-based drilling fluid, and oil-based drilling fluid. Poor compatibility and other problems, to achieve the effect of good compatibility, strong high temperature resistance, and not easy to degrade

Inactive Publication Date: 2019-01-04
中石化石油工程技术服务有限公司 +2
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the plugging materials under pressure in China generally use conventional water-based plugging materials such as walnut shells and sawdust, etc., which are highly hydrophilic and easy to expand in the oil-based drilling fluid environment, deteriorate, degrade, and have poor plugging effect durability. Moreover, the compatibility with oil-based drilling fluid is poor, and effective plugging cannot be formed, which has a great impact on the rheological properties of oil-based drilling fluid

Method used

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  • Oil-based plugging agent and preparation method thereof
  • Oil-based plugging agent and preparation method thereof
  • Oil-based plugging agent and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] The invention provides an oil-based plugging agent:

[0026] Measure 5L of oil-based drilling fluid, add 20% oil-based plugging agent under the condition of stirring (3000r / min), wherein the oil-based plugging agent is prepared according to the weight ratio of photo-like material and flexible material at 1:3 .

[0027] The plugging performance of the product of this embodiment is shown in Table 1, and each parameter is measured at room temperature.

[0028] The performance measurement method of the plugging product is carried out in accordance with the petroleum industry standard: "Indoor test method for bridging plugging materials for drilling fluid SY / T5840-2007" (the same below).

[0029] Table 1 Example 1 oil-based plugging product performance test data

[0030]

Embodiment 2

[0032] The invention provides an oil-based plugging agent:

[0033] Measure 5L of oil-based drilling fluid, and add 20% oil-based plugging agent under stirring (3000r / min), wherein the oil-based plugging agent is prepared according to the weight ratio of photo-like material and flexible material at 2:2 .

[0034] The plugging performance of the product of this embodiment is shown in Table 2, and each parameter is measured at room temperature.

[0035] Table 2 Example 2 oil-based plugging product performance test data

[0036]

Embodiment 3

[0038] The invention provides an oil-based plugging agent:

[0039] Measure 5L of oil-based drilling fluid, and add 20% oil-based plugging agent under stirring (3000r / min), wherein the oil-based plugging agent is based on the weight ratio of photo-like material, flexible material, elastic material, and rigid material Formulation for 1:3:1:2 formulation.

[0040] The plugging experiment situation of the product of this embodiment is as shown in Table 3, Table 4, and Table 5, and is measured at room temperature.

[0041] Table 3 Example 3 oil-based plugging product performance test data

[0042]

[0043]

[0044] Table 4 Example 3 oil-based plugging product performance test data

[0045]

[0046] Table 5 Example 3 oil-based plugging product performance test data

[0047]

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Abstract

The invention discloses an oil-based plugging agent. The oil-based plugging agent comprises a sheet-like material, a flexible material, an elastic material and a rigid material; the fineness of the sheet-like material is less than 5 mm; the average length of the flexible material is 5-10 mm; the grain fineness of the elastic material is 0.5-5 mm; the grain fineness of the rigid material is 1-3 mm;and the weight ratio of the sheet-like material to the flexible material to the elastic material to the rigid material is (1-2):(2-3):(1-3):(0.5-1). The oil-based plugging agent disclosed by the invention has the advantage that plugging effects of microcracks, micropores and medium cracks can be improved. The oil-based plugging agent can plug cracks with different widths of 3 mm and below by being added to an oil base drilling fluid, and the pressure bearing reaches 7 MPa, and the leakage is reduced by 70%.

Description

technical field [0001] The invention relates to the technical field of chemical product manufacturing, in particular to an oil-based leak stoppage agent suitable for oil-based drilling fluid and a preparation method thereof. Background technique [0002] In the development of deep shale gas, the buried depth of the reservoir is greater than 3,500 meters, and the formation pressure coefficient increases from 1.45-1.50 to 1.60-1.80. Due to the development of micro-fractures in the formation, the degree of formation fragmentation increases, and the pressure-bearing capacity of the formation needs to be further improved. , in order to improve the cementing quality and prevent the cement slurry from leaking during the cementing process, it is necessary to further improve the pressure bearing capacity of the formation. Pressure endurance. At present, the plugging materials under pressure in China generally use conventional water-based plugging materials such as walnut shells and ...

Claims

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Application Information

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IPC IPC(8): C09K8/42
CPCC09K8/426
Inventor 梁文利彭小平屈勇卞江刘俊君邢书超
Owner 中石化石油工程技术服务有限公司
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