Preparation method of humanized whole blood matrix quality control product for portable blood glucose meters
A technology of quality control products and blood glucose meters, which is applied in the field of quality control products of human whole blood matrix for various blood glucose meters, and can solve the hidden dangers hidden in the management and treatment of diabetic patients, the cost of matching calibration products or quality control products, and the detection As a result, there are problems such as incompatibility, achieving the value of large market promotion and application, meeting the requirements of quality control, and good interoperability
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preparation example Construction
[0028] The method for preparing the human whole blood matrix quality control product provided by the present invention specifically comprises the following steps:
[0029] (1) Take normal whole blood and centrifuge at 1500g for 10 minutes in a low-speed centrifuge. The upper layer is plasma and the lower layer is whole blood cells. Separate the plasma and whole blood cells for use;
[0030] (2) Add the whole blood cells obtained in step (1) to a fixative, and fix at room temperature for 24-48h; the volume ratio of the whole blood cells to the fixative is 1:(5-10);
[0031](3) Centrifuge at 1500g for 10min after fixation, discard the upper fixation solution, add 0.9% normal saline to wash the lower fixation for 3-5 times, the volume ratio of fixation to normal saline is 1:(5-10), wash Specifically: fully mix the fixation with normal saline, centrifuge at 1500g for 10 min, discard the upper layer of washing solution, and leave the layer of fixation; then filter the washed lower ...
experiment example 1
[0038] Experimental example 1. The homogeneity verification of the human whole blood matrix quality control substance prepared by the method of the present invention and used in a portable blood glucose meter
[0039] Referring to the CNAS-GL29 standard issued by the China National Accreditation Service for Conformity Assessment - "General Principles and Statistical Methods for Valuation of Standard Materials / Standard Samples" on the evaluation of uniformity research, use HORIBA glucose electrode analyzer (LP-150C ) were tested, and 10 samples (No. 1-10) were randomly selected from the quality control products of each blood glucose concentration (low, medium, high) as samples for uniformity evaluation, and each sample was repeatedly measured 3 times. The order of the first determination in the measurement process is: 1-3-5-7-9-2-4-6-8-10; the order of the second determination is: 10-9-8-7-6-5 -4-3-2-1; the order of the third measurement is: 2-4-6-8-10-1-3-5-7-9, the results ar...
experiment example 2
[0055] Experimental Example 2. Stability verification of the human whole blood matrix quality control product prepared by the method of the present invention
[0056] With reference to the CNAS-GL29 standard issued by the China National Accreditation Service for Conformity Assessment——"General Principles and Statistical Methods for Valuation of Standard Materials / Standard Samples" about the stability evaluation requirements for the human-derived whole blood matrix quality control product prepared by the method of the present invention A short-term 2-8°C stability evaluation was performed. Randomly select 3 quality control substances for each blood glucose concentration (low, medium, high) as samples, repeat the measurement twice for each sample, and complete each measurement within 10 minutes, then immediately store the remaining samples at 2-8°C. Use the HORIBA glucose electrode analyzer (LP-150C) to measure continuously for 20 days, and observe the difference between the res...
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