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Concentrated rotating wheel adsorbing material and preparation method thereof

A technology for adsorbing materials and concentrating runners, applied in the field of adsorbent materials, can solve the problems of low efficiency, not easy to peel off, service life, low stability, etc., and achieve the effects of high sintering strength, low wind resistance, and high adsorption-desorption ratio.

Active Publication Date: 2019-04-09
SHANDONG AOFU ENVIRONMENTAL PROTECTION SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] In order to solve the above-mentioned technical problems, the present invention aims at the current situation of the production technology of concentrated runner adsorption materials, uses high-silicon type zeolite molecular sieve ZSM-5 as base material, configures inorganic binder, dispersant, lubricant, organic adhesive, according to The honeycomb material preparation process adopts the overall extrusion method to prepare the honeycomb structure concentrated runner adsorption material. The adsorption material is resistant to mechanical shock and thermal shock, not easy to peel off, and has a long service life; The problem of low efficiency and low stability in the process reduces production costs and improves production efficiency

Method used

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  • Concentrated rotating wheel adsorbing material and preparation method thereof
  • Concentrated rotating wheel adsorbing material and preparation method thereof
  • Concentrated rotating wheel adsorbing material and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0042] The process steps for preparing the concentrated runner adsorption material are as follows:

[0043] (1) Prepare raw materials:

[0044] The weight percentage of inorganic powder: 75% high silica zeolite molecular sieve ZSM-5 (hereinafter abbreviated as ZSM-5), 12.5% ​​activated alumina precursor with D50=0.98μm, 12.5% ​​fumed silica (D50 =9.23μm, specific surface 150m 2 / g).

[0045] Taking the inorganic powder as 100 parts by weight, take 8 parts by weight of methyl cellulose, 2.67 parts by weight of polyether polyol, 2.67 parts by weight of soybean oil, and 30 parts by weight of water, and mix;

[0046] (2) After full dry mixing, kneading, vacuum mud squeezing, it is extruded into a molecular sieve wheel sample block of 40×40×130mm, 400 holes / square inch, and a wall thickness of 7 mil. After drying, use the molecular sieve wheel in Table 1 to quickly burn The curve is calcined at 550°C for 4 hours, and the firing shrinkage is 2.1%.

[0047] In the roasting step, the process ...

Embodiment 2

[0058] (1) Prepare raw materials:

[0059] The weight percentage of inorganic powder: 80% of ZSM-5, 10% of activated alumina precursor with D50=0.98μm, 10% of D50=9.23μm, specific surface area of ​​380m 2 / g of fumed silica mixing;

[0060] Taking the inorganic powder as 100 parts by weight, take 8 parts by weight of methyl cellulose, 2.67 parts by weight of polyether polyol, 2.67 parts by weight of soybean oil, and 30 parts by weight of water, and mix them evenly;

[0061] (2) After full dry mixing, kneading, vacuum mud squeezing, it is extruded into a molecular sieve runner sample block of 40×40×130mm, 400 holes / square inch and 7mil wall thickness. After drying, use Table 1: Molecular sieve runner fast The sintering curve was sintered at 550°C for 4 hours (see Example 1 for the calcination process parameters, and the following examples are the same, unless otherwise specified), the firing shrinkage was 2.1%.

[0062] The performance of the adsorption material of the concentrated run...

Embodiment 3

[0065] (1) Prepare raw materials:

[0066] The weight percentage of inorganic powder: 90% ZSM-5, 5% active alumina precursor with D50=0.98μm, 5% D50=9.23μm, specific surface area is 220m 2 / g of fumed silica mixing;

[0067] Taking the inorganic powder as 100 parts by weight, take 8 parts by weight of methyl cellulose, 2.67 parts by weight of polyether polyol, 2.67 parts by weight of soybean oil, and 30 parts by weight of water, and mix them evenly;

[0068] (2) After full dry mixing, kneading, vacuum mud smelting, refining and kneading mud into mud section;

[0069] (3) Extruding the plastic mud section into a molecular sieve wheel sample block with a honeycomb structure of 40×40×130mm, 400 holes / square inch and a wall thickness of 7 mil, and then microwave;

[0070] (4) After the microwave, the green body is cut to a fixed height, then the drying and firing curves are shown in Table 1, the firing shrinkage is 2.0%, and the firing specific process parameters are shown in Example 1;

[0...

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Abstract

The invention belongs to the technical field of adsorbing materials, and particularly relates to a concentrated rotating wheel adsorbing material and a preparation method of the adsorbing material. The adsorbing material comprises a base material, a high-silicon type zeolite molecular sieve ZSM-5, an inorganic binding agent, fumed silica, an activated aluminum oxide precursor, a dispersing agent,alcohol ether, a lubricating agent, oil, an organic binding agent, alcohol and / or cellulose and pure water. The concentrated rotating wheel adsorbing material has the beneficial effects that the adsorbing material prepared from the raw materials by adopting the technology has the advantages of high molecular sieve content, high strength, high specific surface area, high adsorption and desorption ratio, low specific heat capacity, low wind resistance and the like, and solves the problems that a traditional molecular sieve adsorbing material is low in adsorption efficiency, low in strength, poorin thermal stability, short in usage period and the like.

Description

Technical field [0001] The present invention belongs to the technical field of adsorption materials, and specifically relates to a concentrated runner adsorption material, and also relates to a preparation method of the aforementioned adsorption material. Background technique [0002] The volatile organic compounds (VOCs) emitted by industrial production processes directly or indirectly constitute atmospheric haze, which is the key pollutant for air pollution control. With the increasingly stringent environmental regulations, VOCs emitted by industries such as chemicals, machinery, building materials, furniture, optoelectronics, printing, coating, food, medicine, and pesticides are characterized by low concentration and large air volume. Traditional treatment methods such as adsorption and absorption , Regenerative Oxidation Combustion (RTO / RCO), condensation, membrane separation, biological oxidation, plasma, etc., cannot achieve efficient treatment at low operating costs. In or...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J20/18B01J20/30B01D53/06
CPCB01D53/06B01D2257/708B01J20/186
Inventor 邢延岭潘吉庆张兆合刘洪月黄妃慧程国园王勇伟
Owner SHANDONG AOFU ENVIRONMENTAL PROTECTION SCI & TECH
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