Lithium ion secondary battery and method for manufacturing same
A secondary battery, lithium ion technology, used in secondary batteries, lithium storage batteries, batteries, etc., can solve the problem of low conductivity, and achieve the effect of excellent storage characteristics and cycle characteristics
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Embodiment 1
[0164]
[0165] Li as a Li-containing compound 2 CO 3 , CO as a Co-containing compound 3 o 4 , Mg(OH) as a magnesium-containing compound 2 , ZrO as a zirconium-containing compound 2 , and Al(OH) as an Al-containing compound 3 After adding into a mortar and mixing at an appropriate mixing ratio, solidified into a granular form, fired at 950°C for 24 hours in an atmospheric atmosphere (atmospheric pressure) using a muffle furnace, and synthesized an ICP (inductively coupled plasma , Inductive Coupled Plasma) method obtained composition formula is LiCo 0.9795 Mg 0.011 Zr 0.0005 Al 0.009 o 2 lithium cobaltate (A1).
[0166] Next, the pH value was set to 10, and 10 g of the aforementioned lithium cobaltate (A1) was added to 200 g of a lithium hydroxide aqueous solution at a temperature of 70° C., stirred to disperse, and then Al(NO 3 ) 3 9H 2 O: 0.0154g and ammonia water used to suppress pH fluctuations to generate Al(OH) 3 Co-precipitates are attached to the surfac...
Embodiment 2
[0188] The composite Si-2 (average particle size 5 μm, specific surface area 7.9m 2 / g, the amount of carbon material in the complex is 8 mass %) use as negative electrode active material, the volume ratio of the mixed solvent used in the non-aqueous electrolytic solution is made as propylene carbonate: diethyl carbonate=30:70, except Other than that, it carried out similarly to Example 1, and produced the lithium ion secondary battery.
Embodiment 3
[0190] Graphite A (graphite obtained by coating the surface of mother particles made of natural graphite with amorphous carbon using pitch as a carbon source, with an average particle size of 10 μm): 30% by mass and the aforementioned Si-1: 70% by mass, and The V-type mixer was mixed for 12 hours to obtain the negative electrode active material. Hereinafter, a lithium ion secondary battery was produced in the same manner as in Example 1, except that the aforementioned negative electrode active material was used and the lithium foil 33 having a mass of 14 mg per sheet was used.
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