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Method for detecting particle size distribution based on near infrared spectrum technology

A technology of near-infrared spectroscopy and particle size distribution, which is applied in the field of detection of particle size distribution based on near-infrared spectroscopy technology, can solve the problems of secondary crushing of materials, failure of material detection, occupation of human resources, etc., and achieves stable performance, good adaptability, and small size of the instrument. small effect

Active Publication Date: 2019-05-10
山东金璋隆祥智能科技有限责任公司
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Problems solved by technology

[0004] The traditional particle size detection method is mainly based on the screening method. This method is mostly manual screening or mechanical vibration screening. Both of these methods have many disadvantages: secondary crushing of materials; long time consumption; large amount of human resources ; All materials cannot be tested; Online testing cannot be performed without affecting the continuity of the production process

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  • Method for detecting particle size distribution based on near infrared spectrum technology
  • Method for detecting particle size distribution based on near infrared spectrum technology

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Embodiment Construction

[0023] In order to make the technical solutions and beneficial effects of the present invention clearer and clearer, the present invention will be further described in detail with reference to the accompanying drawings and specific embodiments. It should be understood that the specific embodiments described here are only for understanding of the present invention, and are not intended to limit All other embodiments of the present invention obtained by those of ordinary skill in the art without creative work fall within the protection scope of the present invention.

[0024] The invention discloses a method for detecting particle size distribution based on near infrared spectroscopy technology, which includes:

[0025] Step 1. Sample collection and editing, using static sampling method to collect the near-infrared spectra of I and II objectives;

[0026] Step 2. Data preprocessing, including model transfer, sum and difference calculation, shearing, averaging, MSC, SNV, normalization, ...

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Abstract

The invention discloses a method for detecting particle size distribution based on a near infrared spectrum technology, and mainly relates to the technical field of application of analytical chemistryinstruments. The method comprises the following steps of sample collection and edition, data preprocessing, sample analysis, model correction, equipment installation, sample prediction and predictionresult output, wherein chemometrics is adopted, if compositions of samples are the same, spectrums of the samples are the same, and vice versa. If a corresponding relation (called an analysis model)between the spectrum and parameters to be measured is established, so long as the spectrum of the sample is measured, the required quality parameter data can be obtained quickly through the spectrum and the corresponding relation.

Description

Technical field [0001] The invention mainly relates to the technical field of analytical chemical instrument application, in particular to a method for detecting particle size distribution based on near infrared spectroscopy technology. Background technique [0002] Near infrared light (Near Infrared, NIR) is an electromagnetic wave between visible light (VIS) and mid-infrared light (MIR). The wavelength range of the near-infrared spectrum defined by ASTM is 780~2526nm, which is customarily divided into the near-infrared region There are two areas of near-infrared shortwave (780~1100nm) and near-infrared longwave (1100~2526nm). [0003] Near-infrared spectroscopy is mainly due to the non-resonance of molecular vibration when the molecular vibration transitions from the ground state to the higher energy level. The recording is mainly the frequency doubling and combination of the hydrogen-containing group X-H (X=C, N, O) vibration Frequency absorption. Different groups (such as met...

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Application Information

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IPC IPC(8): G01N15/02
Inventor 邹振民董海平孙茂耿龙飞朱传港
Owner 山东金璋隆祥智能科技有限责任公司