Technology for preparing sulfur-free expandable graphite by utilizing high-concentration perchloric acid
A technology of expanded graphite and perchloric acid, applied in the field of graphite, can solve problems such as corrosion of seals, and achieve low cost, simple method, and uniform oxidation
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment
[0008] A kind of technology that utilizes high-concentration perchloric acid to prepare sulfur-free expandable graphite of the present embodiment comprises the following steps: (1) adding hydrogen peroxide into flake graphite, and stirring evenly, then adding a concentration of 98% perchloric acid acid, stirred in an ice-water bath for 35min, and the ratio of hydrogen peroxide, flake graphite, and perchloric acid was 1:5:10; (2) after stirring, put it into a 20°C water bath for oxidation for 1h, and then use a concentration of Wash with 30% perchloric acid solution and suction filter, then add dropwise anhydrous acetic acid solution with a concentration of 70%, and stir while adding dropwise, after stirring evenly, react for 20min, then wash with water, suction filter, at 50°C Drying under certain temperature conditions to obtain sulfur-free expandable graphite.
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com