This invention discloses a modular, controllable
atmosphere high-temperature oxidation device for the
recovery of substandard
sponge zirconium, relating to the fields of
nuclear fuel cycle and materials technology. The device includes: a furnace
body system, comprising, from the outside to the inside, a steel outer shell, a
refractory insulation layer, and a detachable furnace liner; multiple independently controlled heating zones arranged along the furnace
body axis, each equipped with an independent
heating element and
thermocouple; an
atmosphere control system including
nitrogen and
oxygen sources, an
inert gas source, a
mass flow controller, and a mixer; a sealing and cooling
system employing a high-temperature sealing ring and a double-layer furnace shell design, with circulating cooling water flowing through the interlayer; and an
automatic control system equipped with a temperature-
atmosphere-time automated control program for
fully automated operation and remote monitoring of the
oxidation process. The device provided by this invention can achieve efficient and uniform oxidation treatment of irregular porous
sponge zirconium within the range of 500-1000℃, transforming it into
zirconium oxide with consistent physical properties.