103results about How to "Tissue distribution" patented technology

The invention provides a method for preparing an ultra-high hardness cladding layer through the synchronous ultrasonic vibration assisting laser technology. According to the specific scheme, the method includes the steps that ultrasonic vibration is synchronously introduced in the Ni-based metal ceramic coating cladding process, mobility of liquid metal can be improved in the mode, tissue distribution is more uniform, in the solidification process, a growing dendrite net can be broken and made to be dispersed to all portions of melt, small crystal nucleuses which are uniformly distributed are formed, segregation of metal ceramic is avoided, and therefore it is guaranteed that the cladding layer is not prone to cracking when ultra-high hardness is acquired; equipment is simple, calibration and installation are facilitated, energy consumption is low, the working environment is good, and acquired coating metal ceramic particles are uniform in distribution, high in hardness and good in abrasion resistance.

The invention relates to a crack-controlling method of metal parts by laser melting formation in laser material processing domain, which comprises closed-loop control of fused bath temperature, which comprises the two specific steps of exerting closed-loop feedback control on fused bath temperature by using optical imaging system and PID control device with calorific radiation transmitted from melting zone and adjusting horsepower of laser, and introduction of ultrasonic vibration, which comprises the specific steps of introducing ultrasonic vibration under the piece of work when forming by laser melting. The invention can deduce residual stress and crack, improve structure and can be used in multiple relative domains such as forming, manding and surface peening by laser melting.

A controlled rolling and controlled cooling system for bars comprises a first cooling section at the position of an outlet of an intermediate mill group, a machine cooling section of a finishing mill group, a second cooling section between the finishing mill group and a third flying shear, a third cooling section between the third flying shear and a cooling bed, a sensor module and a central control unit. The first cooling section, the second cooling section and the third cooling section respectively comprise one or a plurality of cooling lines arranged on a horizontal moving trolley and a bypass roll table, one cooling line or the bypass roll table can be selectively connected to a production line by horizontally moving the horizontal moving trolley, and every production line comprises one or a plurality of series connection coolers. Every cooler is connected to a water supply main pipe through one water supply branched pipe, control valves are arranged in the water supply branched pipes, and the coolers connected to the production lines are selected and used by opening and closing of the control valves. According to the controlled rolling and controlled cooling system, a plurality of cooling sections can be selected flexibly, the coolers in every cooling section can also be selectively used simultaneously, and accordingly the system not only is good in applicability, but also improves bar finished product performances.

The invention provides a method and device for conducting laser cladding with the assistance of electromagnetic stirring in a forced cooling environment. The device comprises a fiber laser, a liquid nitrogen forced cooling platform, an electromagnetic stirring platform, a temperature detection and feedback system and a computer control system. The method comprises the steps that a sample is placed on a special clamp made of red copper, the red copper clamp is forcibly cooled through liquid nitrogen, then cold is indirectly transmitted to the sample, and thus forced cooling of the sample in the laser cladding process is achieved. Meanwhile, the magnetic field intensity of the electromagnetic stirring platform is adjusted and controlled through a computer, and thus the laser cladding process with the assistance of electromagnetic stirring under forced cooling is achieved. According to the method and device for conducting laser cladding with the assistance of electromagnetic stirring in the forced cooling environment, laser cladding is conducted with the assistance of forced cooling and electromagnetic stirring to prepare a composite coating so that the good metallurgical bonding capacity of the composite coating with a matrix can be remarkably improved, a hard phase and uniform tissue distribution in the clad coating are achieved, grains are refined, and stress concentration is avoided; and defects such as cracks and pores of the laser clad coating are eliminated, and the quality of the clad coating is improved.

The invention provides a method for preparing WC-Co cemented carbide through microwave sintering. The method comprises the steps of WC powder and Co powder batching and mixing, compacting and sintering, wherein in the step of sintering, compacts, SiC chips, carbon black and alumina powder are put in an alumina fiber insulating bag sleeve and then the alumina fiber insulating bag sleeve is put in a microwave high temperature furnace, the products in the furnace are heated to 500-600 DEG C at a heating speed of 5-10 DEG C/min and the heat is preserved and then the products are heated to 1400-1500 DEG C at a heating speed of 30-80 DEG C/min and the heat is preserved, thus obtaining the WC-Co cemented carbide. The method has the advantages of simple process, convenience in operation, short sintering period and low energy consumption, can replace the existing WC-Co cemented carbide processes, is used for producing the WC-Co cemented carbide by adopting the intermittent or continuous microwave sintering mode and is suitable for industrial application. The prepared WC-Co cemented carbide has excellent performances.

A vanadium-containing carbidic austempered ductile iron comprises the following ingredients in percent by mass: 3.20-3.70 percent of C, 2.50-3.30 percent of Si, 0.4-0.8 percent of Mn, less than or equal to 0.040 percent of P, less than or equal to 0.007 percent of S, 0.01-0.04 percent of Ce, 0.01-0.04 percent of Mg, 0.30-1.80 percent of Cr, 0.25-0.70 percent of V and the balance of Fe. The preparation method of the vanadium-containing carbidic austempered ductile iron comprises the following steps: (1), heating and smelting pig iron, steel scrap, ferromanganese and ferrovanadium; (2), placing a rare-earth magnesium nodularizer into a groove in the bottom of a ladle, placing a nucleating agent on the rare-earth magnesium nodularizer, casting for 10-30 s at the temperature of 1,350-1,430 DEG C, and cooling to obtain ductile iron; and (3), heating the cooled ductile iron to reach a temperature of 850-920 DEG C, keeping the temperature for 2-4 h, then placing the heated ductile iron into 45% KNO3+55% NaNO3 molten salt at the temperature of 280-320 DEG C, keeping the temperature for 1-3 h, taking out the ductile iron, and cooling the ductile iron to the ordinary temperature to obtain the vanadium-containing carbidic austempered ductile iron. The vanadium-containing carbidic austempered ductile iron is high in ductility and hardness and excellent in comprehensive mechanical property.

The invention discloses a cold-rolled shifting fork steel member for an automobile and a producing method. The cold-rolled shifting fork steel member is characterized by comprising the steel chemical ingredients, by weight percentage, of 0.20-0.35% of C, 0.10-0.35% of Si, 0.50-1.50% of Mn, 0.40-1.50% of Cr, 0.0030-0.0070% of Ca, 0.0008-0.005% of B, 0.40-1.10% of Ni, 0.015-0.030% of Als, 0.015-0.040% of Nb, 0.015-0.030% of Ti, smaller than or equal to 0.15% of P, smaller than or equal to 0.008% of S, the balanced of Fe and unavoidable impurities. By means of appropriate hot rolling, cold rolling and cover annealing, the excellent accurate stamping performance can be achieved. The shifting fork portion is quenched and tempered, so that the hardness of the work portion of the shifting fork portion is greatly improved, and the service life of the shifting fork portion is prolonged.

The invention discloses a complex metal part forming method adopting combination of an electric arc additive and a laser additive. The complex metal part forming method comprises the steps that three-dimensional modeling is conducted on a part entity, geometric feature decomposition is conducted on a three-dimensional entity model, a part feature additive forming method is divided, forming processparameters of all features are determined, forming sorting is conducted on all the features, slicing and layering treatment is conducted on all the features, and all the features are sequentially formed according to the feature forming sorting and a treatment method of a combination interface between the adjacent features. According to the complex metal part forming method, the advantages of efficient electric arc additive manufacturing forming and fine laser additive manufacturing forming are effectively combined, compared with traditional forging, the machining period is shortened, the overall forming performance of a part is guaranteed, the quality of a fine and complex structure is guaranteed, the production efficiency is improved, and the machining cost is reduced. Meanwhile, a laserremelting method is adopted, the number of cracks and air holes in a combination interface area of a dissimilar additive process is reduced, meanwhile, structure distribution is more uniform, and themechanical property of the combination interface is improved.

The invention belongs to the technical field of tubing steel manufacturing, and particularly relates to a steel material for a CT80 level coiled tubing and a manufacturing method thereof. The steel material comprises the following chemical components in percentage by mass: carbon: 0.11 to 0.13%, silicon: 0.30 to 0.40%, manganese: 0.70 to 0.90%, chromium: 0.50 to 0.60%, nickel: less than or equal to 0.25%, Mo: 0.13 to 0.15%, copper: 0.30 to 0.40 %, niobium: 0.02 to 0.04%, and the balance being iron and inevitable impurities, wherein nitrogen is less than or equal to 0.004%, phosphorus is less than or equal to 0.015% and sulfur is less than or equal to 0.005% in the purities. The manufacturing method comprises the following steps: the alloy is smelted, a solid core metal calcium cored wire is used for final deoxidation in the smelting process, and then the controlled rolling and controlled cooling rolling is carried out after an ingot is formed, and the finished product is a 4.5mm strip. The steel material provided by the invention has the advantages of complete deoxidation, fine grain and uniform microstructure, and better yield strength, elongation and hardness value.

The invention provides a preparation method of a NiAlIr alloy. The preparation method is method that after being smelted, raw materials are cast through pressure to obtain the nickel aluminum iridium alloy under the condition of vacuum. Compared with the prior art, the preparation method has the advantages that the NiAlIr alloy prepared by the provided preparation method of the NiAlIr alloy is completely composed of a NiAl phase and an IrAl phase of a B2 crystal structure; structure distribution of the NiAlIr alloy is uniform; the minimum diameter of a prepared NiAlIr alloy wire is up to 0.8 mm; and a difficult problem that the NiAlIr alloy material used for an electrode slice of sparking plug can not be prepared in the prior art is solved; and therefore, application prospects of the preparation method of the NiAlIr alloy are very broad.

The invention discloses a Cu-W-Ni copper matrix composite used for a liner, an electroforming method and an electroforming solution thereof, belonging to the electroforming field. The electroforming solution comprises the following components by proportion: 200-250g/L of NiSO4.7H2O, 60-90g/L of Na2WO4.2H2O, 6-10g/L of CuSO4.5H2O, 1-3g/L of CuCl2.2H2O, 270-320g/L of Na3C6H5O7.H2O, 0.3-0.5g/L of C12H25SO4Na, 1.0-1.5g/L of saccharin and 0.25-1mL/L of 1,4-butynediol. The electroforming condition comprises: the pH value of 10% of dilute sulphuric acid is regulated at 5.5-7.0, the temperature is 50-70 DEG C, the current density is 5-15A/dm2, the mechanical stirring is adopted, and a phosphorus-copper plate with 99.9% of Cu and 0.02-0.06% of P is used as an anode. The Cu-W-Ni copper matrix composite prepared in the invention has fine grains and homogeneous structure, and the Cu-W-Ni copper matrix composite liner is easily thickened through electroforming and has no defect on the surface and stable process.

The invention discloses a direct production method for a lead calcium rare earth alloy. The method is characterized by comprising the following steps of: A, putting lead ingots into an open iron pot, and heating to smelt the lead ingots into liquid lead; B, putting the needed metal calcium and rare earth into an iron bell jar; C, arranging the bell jar in the step B on an end part of a stirrer shaft, stirring the liquid lead and rapidly mixing the calcium and rare earth in the bell jar so as to prepare lead calcium rare earth alloy liquid in the liquid lead; and D, casting the lead calcium rare earth alloy liquid produced in the step C into ingots so as to prepare the lead calcium rare earth alloy ingot products, wherein the needed metal calcium and rare earth in the steps B and C are rapidly thrown into the whirlpool of the stirred liquid lead so as to prepare lead calcium rare earth alloy liquid. The method is mainly used for directly producing the lead calcium rare earth alloy.

The invention relates to the technical field of laser cladding additive manufacturing, and discloses a steel mill pinch roll surface laser cladding Fe-Cr alloy wear-resistant coating preparation technology. The steel mill pinch roll surface laser cladding Fe-Cr alloy wear-resistant coating preparation technology comprises the steps that spherical powder is prepared by powder materials by molar mass percentage; an electromagnetic power mixing device is used for mixing powder, and the grain size is 45-105[mu]m; the number of cladding layers of laser cladding is 2, a cladding track of a first layer cladding layer adopts the alternating mode of two spiral lines, the first spiral line is started from one end of a pinch roll, and after the operation of a first spiral line track is completed, a second spiral line is started from the other end; and a second layer of the cladding layers adopts the partition cladding mode, symmetric cladding is carried out according to four areas, and stress relief treatment is carried out by adopting vibration aging equipment in the cladding process of each area. Through the combination of the blending of the powder materials and the cladding mode, by combining with the synchronous vibration aging treatment, the wear-resisting property and average Rockwell hardness of surface coatings of the pinch roll can be improved, the coating quality is improved, and a change cycle of parts on a production line is prolonged.

The invention discloses a surface modified SiC reinforced aluminum-based composite material and a preparation method thereof. The surface modified SiC reinforced aluminum-based composite material is characterized by taking a metal aluminum as a matrix and taking a surface modified SiC porous ceramic as a reinforcement; the preparation method includes the steps that firstly SiC is deposited on a carbon foam substrate through a CVI method; a carbon foam framework is removed through an oxidation method to obtain a SiC porous ceramic blank body; the SiC porous ceramic is further obtained through aPIP method; then porous SiC whiskers are prepared on an outer layer of the SiC porous ceramic through laser sintering; and finally the SiC reinforced aluminum-based composite material is prepared through high-pressure infiltration. The surface-modified SiC reinforced aluminum-based composite material is uniform in structure distribution and good in forming property, and due to surface modification, the strength of the composite material is ensured and the wear resistance of the composite material is improved. By means of the surface modified SiC reinforced aluminum-based composite material, the problems that SiC of a traditional silicon carbide reinforced aluminum-based composite material is not uniformly dispersed in an aluminum matrix, the wear resistance is poor are solved, and the surface modified SiC reinforced aluminum-based composite material can be widely applied to bearing structural parts in the aerospace field.

The invention belongs to the technical field of brazing filler metal and relates to lead-free brazing filler metal. The lead-free brazing filler metal is composed of, by mass, 0.5% to 4.0% of Cu, 0.04% to 0.2% of Ni, 0.005% to 1.0% of Ge, 0.05% to 2.0% of Bi and the balance Sn. Compared with the prior art, 0.005% to 1.0% of Ge and 0.05% to 2.0% of Bi are added to the brazing filler metal, structure distribution of the brazing filler metal can be even, and the melting point and the melting range of brazing filler metal alloy are reduced; due to the fact that germanium is high in oxyphile skin effect and can be concentrated on the surface of the melting brazing filler metal, the brazing filler metal is prevented from being further oxidized. Thus, oxidization resistance of the brazing filler metal can be remarkably improved by adding tiny germanium and the brazing filler metal is prevented from becoming yellow. In addition, the moisture and the tensile strength of the brazing filler metal can be remarkably improved by adding tiny germanium.

The invention discloses a method for preparing a tungsten carbide ceramic material, wherein the method comprises the steps: putting a tungsten carbide powder into a graphite mold, firstly, applying the pressure of 17-20 MPa and carrying out cold compression, then removing the pressure, starting to heat up when the vacuum degree is less than 10 Pa, heating up to 1900-2000 DEG C, controlling the pressure to be 25-30 MPa and keeping for 25-30 minutes, and cooling to 800-1000 DEG C. The method can obtain a binder-free tungsten carbide hard alloy having the advantages of high density, fine crystal grains and uniform distribution of microstructure.

The invention provides a titanium alloy additive manufacturing method based on an inside-laser powder feeding laser processing nozzle, and belongs to the technical field of titanium alloy manufacturing. The method is characterized in that it is guaranteed that L < t > is smaller than or equal to L < q > in the additive manufacturing process, wherein the L < q > is the distance from a powder centerto the outermost side of protective gas, and the L < t > is the maximum distance from the powder center to the position, where the temperature is 400 DEG C, of a formed part in the additive manufacturing process. According to the method, it is guaranteed that the L < t > is smaller than or equal to the L < q >in the additive manufacturing process through a closed-loop control means, which means that it is guaranteed that the protective gas can fully cover the high-temperature area of the formed part in the additive manufacturing process, the situation that the local temperature is too high and uncontrollable due to heat accumulation in the additive manufacturing process is avoided, and it is guaranteed that a final titanium alloy is uniform in components and stable in performance; and according to the data of the embodiment, the surface of the titanium alloy formed part obtained through the embodiment is bright silvery white, and when the stacked height reaches 40 mm, no obvious oxidation discoloration exists; and meanwhile, the content of oxygen elements in all parts of the interior of the formed part is lower than 1,000 ppm.

The invention relates to an ultrafine grained Ta material and a preparation method thereof. Grain size of the ultrafine grained Ta material is smaller than or equal to 3 mu m; ultimate strength of thematerial is higher than or equal to 410 MPa, and yield strength is higher than or equal to 300 MPa. The preparation method of the material comprises the following steps: electron beam melting is performed on a Ta source, after ingot casting, an ingot is sheathed in a protective atmosphere; 3D hot-forging cogging is performed, total deformation of cogging is 65%-75%, and cogging temperature is 1150-1250 DEG C; after cogging, a sheath is removed, and low-temperature and high-temperature cross alternate rolling is performed; the ultrafine grained Ta material is obtained. The process is simple, and the prepared Ta ribbon has uniform and quite fine grains and is endowed with favorable strength, plasticity and toughness. The designed and prepared ultrafine grained Ta ribbon is applied to the high-technology fields of electronics, metallurgy, steel, chemical industry, hard alloys, atomic energy, superconducting technology, automotive electronics, aerospace, medical health and scientific research.

The invention discloses a boron magnesium co-doped VO2 powder, a preparation method and an application thereof. The preparation method comprises the following steps: dissolving a magnesium source anda boron source into hydrogen peroxide, and then adding a vanadium source, thereby preparing a V5+ complex hydrogel containing B3+ and Mg2+; adding a reducing agent into the V5+ complex hydrogel for performing reduction reaction, thereby acquiring a blue V4+ precursor solution; performing hydrothermal reaction on the V4+ precursor solution till generating sediment, cleaning and drying sediment, thereby acquiring an initial VO2 powder; calcining the initial VO2 powder under a protective gas atmosphere, thereby acquiring the boron magnesium co-doped VO2 powder. The invention can solve the problemof the prior art that a VO2 material with both low phase-transition temperature and high visible light transmittance cannot be acquired.

The invention relates to an unleaded brazing filler metal, and belongs to the technical field of brazing filler metal. The brazing filler metal is prepared from, by mass, 0.3%-1.0% of Cu, 0.01%-0.11% 0f Ni, 0.005%-0.10% of Ge, 0.05%-2.0% of Bi, 0.05%-2.0% of Zn, 0.005%-0.5% of Ce, 0.005%-0.3% of Er and the balance Sn. Compared with the prior art, tissue distribution of alloy of the unleaded brazing filler metal is uniform; in addition, the unleaded brazing filler metal has functions of anti-oxidation and stain inhibiting, and has good wettability, good mechanical property and low melting point at the same time.

The invention discloses a method for preparing high silicon steel strip by powder tape casting and high-temperature diffusion sintering. According to the method, water-atomized iron powder and high-purity ferrosilicon powder with the Si content being 50-70% are adopted as raw materials to form Fe-4.5-6.7% Si mixed powder; a solvent, a dispersing agent, an adhesive and a plasticizer are added intothe mixed powder so as to prepare stable slurry which is uniformly dispersed, and a biscuit is prepared on a tape casting machine; the biscuit is subjected to vacuum or reducing atmosphere protectionsintering at 1060-1160 DEG C, so that Fe powder particles are not completely sintered, Si and Fe are partially alloyed, and a multi-hole and incompletely-alloyed high silicon steel blank is formed; and repeated cold rolling and incomplete sintering are carried out on the high silicon steel blank, finally vacuum or reducing atmosphere protection sintering is carried out on the high silicon steel blank at 1250-1320 DEG C, so that homogenization alloying of the high silicon steel is realized, and the high silicon steel strip with the Si content being 4.5-6.7%, the thickness being 0.1-0.5 mm and the density greater than or equal to 7.38 g/cm<3> is obtained.