Bamboo alpha-pulp for viscose and production method thereof
A production method and technology of bamboo pulp, applied in the field of bamboo pulp for viscose and its production, can solve the problems of insufficient fiber purity, increased consumption, and increased waste rubber rate, and achieve good reaction performance and uniform oxidation , reduce the effect of hemifiber increase
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Embodiment 1
[0029] Preparation: First, use a bamboo cutting machine to crush the bamboo into bamboo pieces with a length of 30 mm and a width of 20 mm. Soak them in clean water at room temperature and pressure for 10 hours to make them fully absorb water and swell to facilitate cooking. Rinse with water to remove impurities such as dust and dust to reduce the burden of cooking. , Improve slurry purity.
[0030] One-time cooking: long 30mm through the purification process, the small bamboo chips of wide 20mm are packed in the digester, the caustic soda consumption accounts for 15% (percentage of sodium hydroxide and dry raw material) of absolute dry slurry, and degree of sulfidation is 15% (sulfurized Sodium content to the percentage of sodium hydroxide and sodium sulfide total amount (calculated as sodium oxide)), liquid ratio 1: 2.5, heating time: 150 minutes, holding time: 100 minutes, holding temperature 180 ℃.
[0031] Secondary cooking: After fully washing, dehydrating, and drying th...
Embodiment 2
[0038] Preparation: First, use a bamboo cutting machine to crush the bamboo into bamboo pieces with a length of 20mm and a width of 10mm. Soak them in clean water at room temperature and pressure for 9 hours to make them fully absorb water and swell to facilitate cooking, and remove dust, dust and other impurities by washing with water to reduce the burden of cooking. , Improve slurry purity.
[0039] One-time cooking: the small bamboo chips through the purification process are packed into the digester, the caustic soda consumption accounts for 17% (the percentage of sodium hydroxide and the absolute dry material) of the absolute dry slurry, and the degree of sulfidation is 10% (the ratio of the amount of sodium sulfide to sodium hydroxide and the percentage of the total amount of sodium sulfide (calculated as sodium oxide)), the liquid ratio is 1:3, the heating time: 120 minutes, the holding time: 130 minutes, and the holding temperature is 168°C.
[0040] Secondary cooking: ...
Embodiment 3
[0047] Preparation: First, use a bamboo cutting machine to crush the bamboo into bamboo pieces with a length of 25mm and a width of 15mm, soak them in clean water at room temperature and pressure for 8 hours to make them fully absorb water and expand for cooking, and remove dust, dust and other impurities by washing with water to reduce the burden of cooking , Improve slurry purity.
[0048] One-time cooking: the small bamboo chips through the purification process are packed into the digester, the caustic soda consumption accounts for 20% (the percentage of sodium hydroxide and the absolute dry material) of the absolute dry slurry, and the degree of sulfidation is 5% (the ratio of the amount of sodium sulfide to sodium hydroxide and the percentage of the total amount of sodium sulfide (calculated as sodium oxide)), the liquid ratio is 1:4, the heating time: 150 minutes, the holding time: 150 minutes, and the holding temperature is 165°C.
[0049] Secondary cooking: After fully...
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