4095 results about "Sodium oxide" patented technology

The active component of ultrastable Y-type RE molecular sieve is composite modified Y-zeolite containing RE oxide 8-25 wt%, P 0.1-3.0 wt% and sodium oxide 0.3-2.5 wt%, and with degree of crystallization 30-55 % and unit cell parameter 2.455-2.477 nm. It is prepared with Y-zeolite as material and through the steps of exchange with RE and the first roasting to obtain RE-Na Y-zeolite; reaction with RE, reaction with P-containing compound, and the second roasting. The ultrastable Y-type RE molecular sieve is used as the active component of cracking catalyst and has the obvious effect of lowering olefin content in gasoline and the features of resulting in moderate coke yield and high diesel oil yield. The preparation process is simple and high in the utilization of the modifying elements.

The invention discloses a hydrocracking catalyst and a preparation method thereof. The catalyst comprises hydrogenation active metals and a carrier containing modified Y molecular sieve, alumina and amorphous aluminium silicon, wherein, the Y molecular sieve is prepared by the following method: the Y molecular sieve undergone hydro-thermal treatment by mixed water solution of aluminium salt and acid is adopted; the performance of the Y molecular sieve is as follows: specific surface is 800m<2>/g-900m<2>/g, total aperture volume is 0.40ml/g-0.50ml/g, relative crystallinity is 90%-130%, cell parameter is 2.434-2.440nm, aluminium silicon mol ratio is 20-100, infrared acid volume is 0.3-0.8mmol/g, the mol ratio of acid B and acid L is above 7.0, sodium oxide content is less than or equal to 0.05wt%. The catalyst prepared by the invention has the advantages of high catalytic activity, good target product selectivity and can produce heavy naphtha, aviation fuel and diesel fuel, and the like, with high yield and good quality.

The invention discloses a hydrocracking catalyst for producing heavy naphtha in great abundance and a preparation method thereof. The catalyst contains hydrogenation active metals and a carrier which consists of modified Y molecular sieves and alumina, wherein the Y molecular sieves are obtained by using a mixed aqueous solution of aluminum salts and an acid to perform hydro-thermal treatment. The properties of the modified Y molecular sieves are as follows: the specific surface area is between 750 m<2>/g and 850 m<2>/g; the total pore volume is between 0.35 and 0.48 ml/g; the relative crystallinity is between 90 and 130 percent; the cell parameter is between 2.437 and 2.445 nanometers; the silicon-aluminum mol ratio is between 15 and 70; the infrared acid amount is between 0.5 and 1.0 mmol/g; the B acid/L acid is more than 7.0; and the content of sodium oxide is less than or equal to 0.05 weight percent. The hydrocracking catalyst has the characteristics of good catalytic activity, high heavy naphtha selectivity, high yield, high latent content of heavy naphtha arene, and so on.

The invention belongs to the field of fine chemical materials, and more particularly relates to a method for preparing cellulose composite aerogel. The method is mainly characterized by taking a carbon material as a modifying agent, and comprises the following main processes of: firstly dissolving cellulose in a sodium hydroxide/thiourea aqueous solution, a sodium hydroxide/urea aqueous solution or other solvents to prepare a cellulose solution with a certain concentration, adding a carbon nanotube (CNT), graphene oxide (GOS), reduced graphene oxide (rGO) and other modifying agents, standing for carrying out gelation, carrying out solvent exchange on the obtained gel, and drying the composite gel to obtain the cellulose composite aerogel. The preparation technique provided by the invention has a simple process and convenience for operation, and can obviously shorten the time of forming the gel from the solution; and the prepared composite aerogel has higher compressive strength and modulus as well as good heat stability, and has wide application prospects in the biomedical, biological sensing and detecting and other fields.

The invention discloses a method for recovering polysilicon ingots, carborundum powder and polyethylene glycol from cutting waste mortar. The recovering method comprises the following steps shown as an attached diagram, wherein the high temperature purification comprises the following steps of: mixing the prepared silicon micro powder with a fluxing agent according to the weight ratio of 1: 0.5-5 into lumps, carrying out high temperature treatment in a high temperature vacuum furnace with the treatment temperature range of 1450-1800 DEG C and the treatment time range of 1-10h; and then carrying out directional solidification on melting-state high purity silicon subjected to the high temperature treatment to obtain the polysilicon ingots; wherein the fluxing agent is selected from one or any mixture of silica, alumina, calcium oxide, magnesium oxide, potassium oxide, sodium oxide, calcium fluoride, magnesium fluoride, sodium fluoride, sodium chloride, potassium chloride and calcium chloride. The invention has the advantages that: the yields of carborundum and polyethylene glycol are high and can reach more than 70-80 percent; and the recovered polysilicon ingots reach the purity of 6-7N and completely satisfy of the requirement for preparing silicon slices of silicon solar cell.

The catalytic cracking co-catalyst for increasing diesel oil yield is prepared through roasting kaolin at over 900 deg.c for in-situ crystallization. The co-catalyst contains type-Y zeolite in 5-20 wt%, as well as magnesia 0.5-3 wt%, RE oxide 0.5-5 wt%, and sodium oxide less than 0.6 wt%, and the zeolite has Si/Al ratio of 4.0-6.0. Adding certain amount of the catalytic cracking co-catalyst without altering the main catalyst in the oil refining apparatus can raise diesel oil yield of FCC catalyzed apparatus, improve product distribution, raise available catalyst utilization, and improve the activity stability of the catalyst system and heavy metal resistance.

An organic electroluminescent device having high efficiency, a long life time, and low cost, includes a substrate, a hole injecting electrode and an electron injecting electrode formed on the substrate, an organic material-containing organic layer between the electrodes, and an inorganic insulative electron injecting and transporting layer between the light emitting layer and the electron injecting electrode. The organic layer includes a light emitting layer containing a conjugated polymer, and the inorganic insulative electron injecting and transporting layer comprises three components. The first component is at least one oxide selected from the group consisting of lithium oxide, rubidium oxide, potassium oxide, sodium oxide, and cesium oxide. The second component is at least one of strontium oxide, magnesium oxide, and calcium oxide. The third component consists of silicon oxide, germanium oxide, or mixtures thereof.

An ink jet ink composition including from 40.0 to 99.0% by weight of water; from 0.1 to 20.0% by weight of a pigment dispersed with an oleoyl methyl taurine salt dispersant from 0 to 70.0% by weight of a water miscible co-solvent; and from 0.1 to 20.0% by weight of a water-reducible addition polymer; wherein the weight average molecular weight of the polymer is from 2,000 to 100,000; the acid number is from 50 to 400; and the acid group on the polymer is neutralized by an alkaline metal hydroxide such as lithium hydroxide, sodium hydroxide potassium hydroxide, or a mixture thereof; and wherein all weight percentages are based on the total weight of the ink composition. An ink jet printing method is also disclosed.

The present invention relates to an optical glass using silicic acid group as main body, said optic glass has high expansion coefficient, high Young modulus, excellent weatherability and high transmissivity in the infrared wave zone. Said glass composition contains (mole%) 36-66% of silicon dioxide, 0-12% of aluminium oxide, 0-6% of boric oxide, 0-10% of magnesium oxide, 0-16% of calcium oxide, 0-16% of strontium oxide, 0-16% of baria, 0-8% of zinc oxide, 0-32% of lithium oxide, 0-25% of sodium oxide, 0-25% of potassium oxide, 0-20% of cesium oxide, 0-6% of phosphorus pentoxide, 0-8% of scandium oxide and others.

The invention discloses a novel oxygen fertilizer and preparation and application methods of the oxygen fertilizer. Mixtures of one or more of calcium peroxide, sodium peroxide and magnesium peroxide act as a core; nano chitosan doped with sodium alginate as the binding agent serves as a wrapping membrane; and the outer layer of the wrapping membrane is further wrapped by paraffin as a conditioner, so that a slow-release oxygen fertilizer is prepared. The oxygen fertilizer contains 70-75% of the core by weight, 20-25% of the wrapping membrane by weight, and 3-10% of the conditioner by weight and the particle diameter of the oxygen fertilizer particles is 3-10mm. The novel oxygen fertilizer prepared by the preparation method disclosed by the invention can supply oxygen to waterlogged plants for a long time and is convenient and simple to apply, simple in production process and environment-friendly, and saves time and labor and can be used widely.

The invention discloses high-toughness enamel glaze. The enamel glaze is prepared from the following components in parts by weight: 40-50 parts of silicon dioxide, 15-25 parts of titanium dioxide, 5-15 parts of potassium oxide, 10-20 parts of sodium oxide, 1-5 parts of lithium oxide, 2-4 parts of calcium fluoride, 6-12 parts of vanadium pentoxide, 1-3 parts of tungsten carbide and 5-10 parts of aluminum oxide and zirconium dioxide. According to the enamel glaze, by means of the composition, the toughness of the enamel glaze can be greatly improved, meanwhile, the defect that ceramic cracks arecaused due to collision can be overcome, and therefore, the enamel glaze has a wide application prospect.

The invention relates to hollow glass microballoons and a production method thereof. The hollow glass microballoons are characterized by comprising the following raw materials in portion by weight: 75to 80 portions of silicon dioxide, 7 to 15 portions of boron oxide, 1 to 4 portions of aluminium oxide, 0.5 to 1.5 portions of calcium oxide, 0.8 to 1.2 portions of magnesium oxide, 5 to 6 portions of sodium oxide, 0.0 to 0.3 portion of sulfur trioxide and 0 to 0.05 portion of ferric oxide. The production method of the hollow glass microballoons comprises the following steps: compounding, melting, water quenching, drying, crushing, grading, hollow balling, collection and air separation, and is characterized in that the hollow balling comprises the following steps: ejecting a glass raw material, gas and combustion-supporting gas upwards from the bottom of a balling furnace for combustion, and cooling the glass microballoons upwards by a cooling device after melting under the action of a draft fan. The hollow glass microballoons have the advantages of good surface tension, high compression strength and chemical stability. The production method can better ensure material balling, and hassimple process, less equipment and good effect as much as possible.

Improved glass fibers compositions, typically useful for fire resistant blankets or containers to provide high burn-through resistance at high temperatures of 2,400° F. and higher, and typically comprising silica, sodium oxide, potassium oxide, calcium oxide, magnesium oxide, ferrous+ferric oxide, and titanium oxide; the improved glass compositions may further include alumina, lithium oxide, and boron oxide.

A mixed positive electrode active material is used. The mixed positive electrode active material is obtained by mixing a layered oxide whose initial charge-discharge efficiency when lithium metal is used for a counter electrode is less than 100% (hereinafter referred to as a first layered oxide) and a layered oxide whose initial charge-discharge efficiency is 100% or more (hereinafter referred to as a second layered oxide). Examples of the first layered oxide include Li_1+aMn_xCo_yNi_zO₂. A sodium oxide such as Li_ANa_BMn_XCo_YNi_ZO₂ other than a layered compound from which lithium is previously extracted by acid treatment or the like can be used as the second layered oxide whose initial charge-discharge efficiency is 100% or more. A layered oxide obtained by replacing (ion exchange) sodium in the foregoing Li_ANa_BMn_XCo_YNi_ZO₂ with lithium can be also used as the second layered oxide.

The invention discloses high-manganese high-nitrogen low-nickel stainless steel plate blank continuous casting crystallizer covering slag which comprises the following components in percentage by weight: 54-57% of wollastonite, 9-13% of fluorite, 9-13% of sodium carbonate, 0-1% of lithium carbonate, 5-7% of glass dust, 8-12% of vanadine soil, 2.5-2.7% of soot carbon and 3-3.5% of graphite, and comprises the chemical components in percentage by weight: 31.9-34.9% of calcium oxide, 32.1-35.1% of silicon dioxide, 7.3-8.3% of aluminium oxide, 0.5-1.5% of magnesium oxide, 0.5-1.4% of iron sesquioxide, 4.4-6.4% of fluorion, 6.5-7.5% of sodium oxide, 0-0.39% of lithium oxide, 4.5-6.0% of fixed carbon and 4-7% of gas volatile matters. The alkalinity of the covering slag, namely the ratio of CaO to SiO2, is 0.91 to 1.00, the melting point of the covering slag is 1100 DEG C to 1160 DEG C, and the viscosity of the covering slag is 0.3 to 0.6 Pa.s at 1300 DEG C. The invention can solve the problems of easy crusting, slag entrainment, slag inclusion, slag sticking on casting blank surfaces, bubbles under skins, cracks, deep chatter mark, felting, bleed-out, and the like of the covering slag in the crystallizer during high-manganese high-nitrogen low-nickel stainless steel plate blank continuous casting, and has the advantages of uniform and stable slagging in the crystallizer, good casting blank quality, difficult felting and bleed-out, and the like.

An object of the invention is to achieve an organic EL device which is resistant to a deterioration of an inorganic-organic interface, has performance equivalent or superior to that of a prior art device comprising hole and electron injecting and transporting layers using an organic substance, possesses an extended life, weather resistance and high stability, and is inexpensive. This object is accomplished by the provision of an organic EL device which comprises a substrate, a hole injecting electrode and a cathode formed on the substrate, and an organic substance-containing light emitting layer located at least between these electrodes, wherein an inorganic insulating electron injecting and transporting layer is located between the light emitting layer and the cathode, and an inorganic insulating hole injecting and transporting layer is located between the light emitting layer and the hole injecting electrode. The inorganic insulating electron injecting and transporting layer comprises as a main component one or two or more oxides selected from the group consisting of strontium oxide, magnesium oxide, calcium oxide, lithium oxide, rubidium oxide, potassium oxide, sodium oxide and cesium oxide, and the inorganic insulating hole injecting and transporting layer comprises as a main component an oxide of silicon and/or an oxide of germanium. The main component has an average composition represented by (Si1-xGex) Oy where 0</=x</=1, and 1.7</=y</=1.99. The light emitting layer comprises a layer made up of a host substance on a side thereof contiguous to the inorganic insulating electron injecting and transporting layer and/or the inorganic insulating hole injecting and transporting layer. A layer containing a dopant in addition to the host substance is located on the side of the light emitting layer that faces away from the layer made up of the host substance or between them.

The invention relates to a preparation method of high specific surface area graphene with well-developed mesopores. The method comprises the steps of mixing graphene oxide and an activating agent under a protective atmosphere; passing through an activating gas to active the mixture; and finally obtaining the high specific surface area graphene with the well-developed mesopores through processes of washing, filtering and drying. The activating agent is selected any one from potassium hydroxide, sodium hydroxide, phosphoric acid and zinc chloride or a combination of at least two of the above materials. The method is simple in equipment and low in cost, is safe and reliable, has small pollutions and high production efficiency, and is suitable for large-scale production. The obtained graphene has high specific surface area, and is more suitable for migration of electrolyte ions.

The invention relates to a high-specific area cerium zirconium oxide solid compound and relative production, wherein said compound is Ce1-xZrxNazOw or Cex'Zrx'MyNazOw, while the natron sodium oxide content is 5ppm-1000ppm. And the production comprises (1), preparing the solution as A; (2), dissolving the alkali material into water to obtain B; (3), adding A into B, to obtain deposition suspension; (4), adding additive, as surface activator, polymer, etc, mixing and heating, and crystallizing at high pressure; (5), filtering, and washing the deposit; (6), washing and filtering, drying, baking to obtain the solid. The invention has high crystallization degree, small grain and uniform distribution.

One aspect of the invention relates to a dehydrogenation catalyst composite containing alumina, chromium oxide, lithium oxide, and sodium oxide. The invention also relates to methods of making the dehydrogenation catalyst composite. Another aspect of the invention relates to method of dehydrogenating a dehydrogenatable hydrocarbon involving contacting the dehydrogenatable hydrocarbon with a dehydrogenation catalyst composite containing alumina, chromium oxide, lithium oxide, and sodium oxide to provide a dehydrogenated hydrocarbon, such as an olefin.

The invention discloses a technology for recovering production of electrolytic copper and zinc from smelting ash. The technology comprises a step of smelting ash leaching, a step of copper extraction and purification through copper electrodeposition, a step of iron removal through neutralization, a step of cadmium removal, and a step of zinc extraction and purification through zinc electrodeposition. The method is characterized in that chemical components in the smelting ash are analyzed, and the smelting ash is leached by a sulfuric acid solution leaching agent; the leachate obtained after the above leaching reaction undergoes a separation operation of copper extraction and purification through the copper electrodeposition; the resultant copper extraction liquor is neutralized by high-zinc dust which is a neutralizer to remove iron; cadmium is displaced and deposited by zinc powder having a mass same with cadmium after the iron removal through the neutralization; and the zinc extraction is carried out through the zinc electrodeposition by casting zinc ingot products. The technology has a wide adaptability, adopts two steps to complete the exchange reaction of zinc oxide and copper oxide in the raw material with an acid, and adopts the high-zinc dust as the neutralizer, so the massive zinc loss caused by entrainment of routine neutralizers comprising calcium oxide and sodium hydroxide is avoided. A zinc extraction liquor obtained in the above step is purified by N235, so economy and effectiveness are realized.

A preparation method of beta zeolite with multilevel pore canals is disclosed by the invention, and comprises: uniformly mixing a silicon source, a tetraethylammonium hydroxide solution, sodium hydroxide and a complete dissolved aluminium source, stirring at a certain constant temperature, and forming a xerogel; carrying out a first hydrothermal treatment for the obtained xerogel, cooling, grinding, and adding a proper amount of a silane coupling agent; and carrying out a second hydrothermal treatment, cooling, filtering, roasting, and obtaining the beta zeolite with multilevel pore canals. The preparation method and the post-processing method are simple, yield is high, and industrial amplification production is easy to realize.