A kind of production technology of poly(p-phenylene benzobisoxazole) fiber continuous polymerization spinning
A technology of benzobisoxazole and poly-p-phenylene, which is applied in the production process of continuous polymerization spinning of poly-p-phenylene benzobisoxazole fiber, and in the field of fiber spinning production process, which can solve the problem that industrial continuous production cannot be realized , not the PBO fiber continuous production process and other issues, to reduce the risk of equipment failure, increase accuracy, and improve production efficiency
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Embodiment 1
[0036] A production process for continuous polymerization and spinning of poly-p-phenylene benzobisoxazole fibers, comprising the following process steps:
[0037] A. Degassing prepolymerization
[0038] With all 4,6-diaminoresorcinol hydrochloride, phosphorus pentoxide, the terephthalic acid of 80% of total charging capacity and the polyphosphoric acid of 76% of total charging capacity add in the degassing still, at 50 Under the temperature condition of ℃, the degassing reaction is carried out for 10 hours to obtain the prepolymer, and then the prepolymer is transferred to the defoaming mixed batch tank through the delivery pump;
[0039] B. TPA mix
[0040] In the slurry mixing tank, mix and stir terephthalic acid and polyphosphoric acid at a temperature of 50°C to prepare a 3% TPA / PPA slurry;
[0041] C. Post-polymerization
[0042] The prepolymer in the defoaming mixing batch tank in step A and the TPA / PPA slurry in the slurry mixing tank in step B are input into the tw...
Embodiment 2
[0046] A production process for continuous polymerization and spinning of poly-p-phenylene benzobisoxazole fibers, comprising the following process steps:
[0047] A. Degassing prepolymerization
[0048] With all 4,6-diaminoresorcinol hydrochloride, phosphorus pentoxide, the terephthalic acid of 99% of total charging capacity and the polyphosphoric acid of 98% of total charging capacity add in the degassing still, at 120 Under the temperature condition of ℃, the degassing reaction is carried out for 20 hours to obtain the prepolymer, and then the prepolymer is transferred to the defoaming mixed batch tank through the delivery pump;
[0049] B. TPA mix
[0050] In the slurry mixing tank, mix and stir terephthalic acid and polyphosphoric acid at a temperature of 100°C to prepare a 10% TPA / PPA slurry;
[0051] C. Post-polymerization
[0052] The prepolymer in the defoaming mixing batch tank in step A and the TPA / PPA slurry in the slurry mixing tank in step B are input into the t...
Embodiment 3
[0056] A production process for continuous polymerization and spinning of poly-p-phenylene benzobisoxazole fibers, comprising the following process steps:
[0057] A. Degassing prepolymerization
[0058] With all 4,6-diaminoresorcinol hydrochloride, phosphorus pentoxide, the terephthalic acid of 90% of total charging capacity and the polyphosphoric acid of 87% of total charging capacity add in the degassing still, at 85 Under the temperature condition of ℃, the degassing reaction was carried out for 15 hours to obtain the prepolymer, and then the prepolymer was transferred to the defoaming mixed batch tank through the delivery pump;
[0059] B. TPA mix
[0060] In the slurry mixing tank, mix and stir terephthalic acid and polyphosphoric acid at a temperature of 75°C to prepare a 6.5% TPA / PPA slurry;
[0061] C. Post-polymerization
[0062] The prepolymer in the defoaming mixing batch tank in step A and the TPA / PPA slurry in the slurry mixing tank in step B are input into th...
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