Continuous waste lubricating oil steam treatment method
A waste lubricating oil and treatment method technology, which is applied in the direction of lubricating compositions, etc., can solve the problems that waste lubricating oil cannot meet the effective base oil standard and increase the cost of waste lubricating oil treatment, so as to improve the atmospheric pressure evaporation efficiency and prevent coking problem effect
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Embodiment 1
[0073] figure 1 It is the process equipment flowchart of the first embodiment of the present invention. according to figure 1 In the shown equipment, the waste lubricating oil of the present invention can implement the following process. According to the description in the specification and the claimed scheme, the connection relationship of the equipment can also be adjusted accordingly, omitted or added.
[0074] Step a) is carried out first. The stored waste lubricating oil raw material is introduced into the raw material buffer tank (not shown in the figure), pressurized by the raw material pump, and after exchanging heat with the heat from the atmospheric pressure evaporator, it is connected with the distillation reagent delivery pipeline The basic reagents are mixed and mixed, and then transported into the first reactor 1, and the reaction temperature of 1 in the first reactor is controlled to be 80°C;
[0075] In this embodiment, the first reactor 1 adopts a plug flow...
Embodiment 2
[0085] figure 1 with figure 2 The combination of is used as embodiment 2 of the present invention. That is, Example 2 implements figure 1 shown in the first paragraph processing, and figure 2 shown in the second paragraph processing.
[0086] The process of the first stage of treatment in embodiment 2 is the same as that in embodiment 1, and will not be repeated here. Further, when an extraction side line is set in the middle of the first decompression evaporator 4 to extract the first stage base oil through the heat exchanger 9 and the condenser 8, the first stage base oil at the outlet is transported to figure 2 In the transfer line of the second reactor 21 (i.e., step d is carried out). Thereafter, the first stage base oil is used as the raw material for the second stage treatment, and the following flow process is carried out:
[0087] Step e), providing the obtained Stage I base oil to the second reactor 21; and, before being supplied to the second reactor, provi...
Embodiment 3
[0097] image 3 and refer to figure 1 It is the third embodiment of the technical solution of the present invention. In this embodiment, four side-drawn oil products are used in the second stage of treatment, so that base oils with different distillation ranges and viscosities can be obtained, and the physical and chemical indicators of the oil products are further optimized. Specifically, see image 3 , when the technique of embodiment 2 was carried out to decompression evaporation, from the first section base oil extraction pipeline 211, the second section base oil extraction pipeline 212, the third section base oil extraction pipeline 213; the fourth section base oil extraction pipeline 214 The first-stage base oil, the second-stage base oil, the third-stage base oil and the fourth-stage base oil were extracted respectively.
[0098] The physical and chemical indicators obtained are as follows:
[0099] Table 4: Each stage base oil product index of embodiment 3
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Abstract
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