Preparation method of aquaculture bactericide
A technology for aquaculture and fungicides, applied in botany equipment and methods, biocides, chemical instruments and methods, etc., can solve the problem that the sterilization effect is easily affected by water hardness, light, temperature, toxicity and Corrosiveness and other problems, to achieve the effect of large unit sterilization treatment capacity, wide application range and easy operation control
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Embodiment 1
[0026] A preparation method of aquaculture bactericide, comprising mixing the dispersion of chitosan quaternary ammonium salt in a dispersion medium with activated carbon; the modifier for the preparation of the above-mentioned chitosan quaternary ammonium salt is 2,3-epoxypropyl Trimethylammonium chloride, activator is glycolic acid and zinc L-lactate. Chitosan quaternary ammonium salt is the product of chitosan modified by alkylation, and the quaternary ammonium group of quaternary ammonium salt is substituted to the amino group of chitosan to form a stronger polycationic compound. The quaternization modification of chitosan greatly improves the solubility of chitosan, and it has more positive charges than chitosan, which interacts with the negative charges on the surface of the bacteria, thereby changing the penetration of the cell membrane of the bacteria, so that The transport of extracellular substances is blocked, thereby achieving better antibacterial and bactericidal ...
Embodiment 2
[0037] A kind of preparation method of aquaculture fungicide, its concrete steps are as follows:
[0038] 1) dissolving the crude chitosan in glacial acetic acid with a concentration of 5%, adding alkali to adjust the pH to 10, soaking for 10 hours, then centrifuging, and washing the obtained precipitate with water to neutrality to obtain pure chitosan;
[0039] 2) Place the pure chitosan in a water bath at 80°C, and dissolve it in isopropanol with magnetic stirring, then add a modifier and an activator, react at 60°C for 5.5h, then wash with absolute ethanol, and then Place in a dialysis bag for dialysis for 24 hours, concentrate the dialysate and vacuum freeze-dry to obtain chitosan quaternary ammonium salt, the addition of modifier is 38.5% of the weight of pure chitosan, and the addition of activator is pure chitosan. Product chitosan weight 0.45%, wherein the weight ratio of glycolic acid and L-zinc lactate is 1:2;
[0040] 3) Boil the activated carbon in a 5% hydrochlor...
Embodiment 3
[0044] A kind of preparation method of aquaculture fungicide, its concrete steps are as follows:
[0045] 1) dissolving the crude chitosan in glacial acetic acid with a concentration of 3.5%, adding alkali to adjust the pH to 9, soaking for 8.5 hours, then centrifuging, and washing the obtained precipitate with water until neutral to obtain pure chitosan;
[0046] 2) Place the pure chitosan in a water bath at 70°C, and dissolve it in isopropanol with magnetic stirring, then add modifier and activator, react at 75°C for 6.5h, then wash with absolute ethanol, and then Place in a dialysis bag for dialysis for 18 hours, concentrate the dialysate and vacuum freeze-dry to obtain chitosan quaternary ammonium salt, the addition of modifier is 34.5% of the weight of pure chitosan, and the addition of activator is pure chitosan. Product chitosan weight 0.15%, wherein the weight ratio of glycolic acid and L-zinc lactate is 1:1.5;
[0047] 3) Put the activated carbon in a hydrochloric ac...
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