Cannabinoid component-containing composition extracted from industrial hemp and application of cannabinoid component-containing composition in tobacco products
A technology for industrial hemp and tobacco products, which is applied in the fields of tobacco, tobacco preparation, and tobacco processing, can solve the problems such as the inability to satisfy consumers' pursuit of the taste function of electronic cigarettes.
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Embodiment 1
[0098] Example 1 Preparation of cannabinoids extracted from industrial hemp
[0099] (1) Grinding industrial hemp flower and leaf raw materials into 40-mesh coarse powder, baking at 110°C for 80 minutes, the measured moisture content is 3.6%;
[0100] (2) soak the medicinal material obtained in step (1) with 10 times of 95% ethanol at room temperature for 2 hours, extract by cold soaking for 3 times, and combine the obtained extracts;
[0101] (3) Concentrate the extract obtained in step (2) at 55°C to an alcohol content of 50%, add 95% ethanol to adjust the alcohol content to 60%, settle overnight, and obtain a supernatant;
[0102] (4) Pass the supernatant obtained in step (3) through the large-pore HPD 100 resin, wash 2BV with purified water, wash 4BV with 25% ethanol, and collect CBDV from liquid chromatography until the concentration of CBDV is detected to be lower than 0.5g / Stop collecting L, and use the rest as waste liquid to recover solvent; then elute 4BV with 45% ...
Embodiment 2
[0109] Example 2 Preparation of cannabinoids extracted from industrial hemp
[0110] (1) Grinding the industrial hemp mosaic raw material into a 60-mesh coarse powder, baking at 150°C for 30 minutes, and the measured moisture content is 3.2%;
[0111] (2) soak the medicinal material obtained in step (1) with 11 times of 95% ethanol at room temperature for 2 hours, extract by cold soaking for 3 times, and combine to obtain the extract;
[0112] (3) Concentrate the extract obtained in step (2) at 65° C. to an alcohol content of 72%, filter with a plate and frame, and obtain a supernatant;
[0113] (4) Put the supernatant obtained in step (3) over HZ18 macroporous resin overnight, wash 3BV with purified water, wash 5BV with 20% ethanol first, then elute 6BV with 80% ethanol, and combine the eluents;
[0114] (5) Concentrate the eluate obtained in step (4) to an alcohol content of 55%, and put it on a secondary chromatography column respectively, and the fillers are DM130 and MCI...
Embodiment 3
[0120] Example 3 Preparation of electronic cigarette liquid
[0121] The main composition of an electronic cigarette liquid is shown in the following table:
[0122] Table 1 A composition list of electronic cigarette liquid
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[0124]
[0125] The cannabinoids extracted from industrial hemp in Table 1 are prepared according to Example 1, wherein the mass percentage of CBD is 65%, the mass percentage of CBDV is 15%, the mass percentage of CBG is 12%, and the mass percentage of THCV is 8 %.
[0126] The preparation steps of the e-cigarette liquid are as follows: dissolving the cannabinoids extracted from industrial hemp in the solvent glycerin and purified water, adding syrup and preservative sodium benzoate after dissolving, and finally adding tobacco essence, and stirring thoroughly to obtain the e-cigarette liquid. e-liquid.
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