A cu-mof/bivo 4 Preparation method and application of composite photoelectrode
A composite photoelectrode technology, applied in electrodes, electrolytic components, electrolytic processes, etc., can solve the problems of easy recombination and confinement of photogenerated electrons and holes, and achieve cheap and non-toxic materials, enhanced capture ability, good chemical The effect of stability
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Embodiment 1
[0027] A Cu-MOF / BiVO 4 The preparation method of composite photoelectrode comprises steps as follows:
[0028] A. BiVO with worm-like structure prepared on FTO substrate 4
[0029] The BiVO with worm-like structure prepared on the FTO substrate 4 The steps are:
[0030] (1) First, prepare liquid A as 0.4M KI solution and 0.04M Bi(NO 3 ) 3 The mixed solution of the solution is 50ml in total, adjust the pH=1.7 with concentrated nitric acid (3 drops of concentrated nitric acid), the B solution is 20ml of 0.23M ethanol solution of p-benzoquinone, and the AB solution is mixed evenly;
[0031] (2) Then use the mixed solution as the electrolyte, and use the constant voltage electrochemical deposition method to perform electrodeposition on the FTO substrate, and electrodeposit it for 5 minutes under the applied bias voltage -0.1V (relative to Ag / AgCl), and then obtain the BiOI photoelectrode ;
[0032] (3) Prepare 10ml of 0.2M dimethyl sulfoxide (DMSO) solution of vanadyl acety...
Embodiment 2
[0042] A Cu-MOF / BiVO 4 The preparation method of composite photoelectrode comprises steps as follows:
[0043] A. BiVO with worm-like structure prepared on FTO substrate 4
[0044] The BiVO with worm-like structure prepared on the FTO substrate 4 The steps are:
[0045] (1) First, prepare liquid A as 0.4M KI solution and 0.04M Bi(NO 3 ) 3 The mixed solution of the solution is 50ml in total, adjust the pH=1.7 with concentrated nitric acid (3 drops of concentrated nitric acid), the B solution is 20ml of 0.23M ethanol solution of p-benzoquinone, and the AB solution is mixed evenly;
[0046] (2) Then use the mixed solution as the electrolyte, and use the constant voltage electrochemical deposition method to perform electrodeposition on the FTO substrate, and electrodeposit it for 5 minutes under the applied bias voltage -0.1V (relative to Ag / AgCl), and then obtain the BiOI photoelectrode ;
[0047] (3) Prepare 10ml of 0.2M dimethyl sulfoxide (DMSO) solution of vanadyl acety...
Embodiment 3
[0053] A Cu-MOF / BiVO 4 The preparation method of composite photoelectrode comprises steps as follows:
[0054] A. BiVO with worm-like structure prepared on FTO substrate 4
[0055] The BiVO with worm-like structure prepared on the FTO substrate 4 The steps are:
[0056] (1) First, prepare liquid A as 0.4M KI solution and 0.04M Bi(NO 3 ) 3 The mixed solution of the solution is 50ml in total, adjust the pH=1.7 with concentrated nitric acid (3 drops of concentrated nitric acid), the B solution is 20ml of 0.23M ethanol solution of p-benzoquinone, and the AB solution is mixed evenly;
[0057] (2) Then use the mixed solution in step (1) as the electrolyte, utilize the constant voltage electrochemical deposition method to carry out electrodeposition on the FTO substrate, and electrodeposit 5min under the applied bias voltage-0.1V (relative to Ag / AgCl), That is, the BiOI photoelectrode is obtained;
[0058] (3) Prepare 10ml of 0.2M dimethyl sulfoxide (DMSO) solution of vanadyl ...
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