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Preparation method of a honeycomb ceramic regenerator with ultra-thick outer wall

A technology of honeycomb ceramics and regenerators, applied in the field of porous ceramics processing, can solve the problems of insufficient strength of the outer wall of the honeycomb ceramic regenerator, failure to form a whole, and a pass rate of less than 50%, so as to reduce deformation defects and damage rates , The effect of improving the firing pass rate

Active Publication Date: 2021-03-09
JIANGXI BOCENT TEC CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

First of all, due to the thinner outer wall thickness of the honeycomb ceramic green body, the support strength of the green body is poor during the drying and firing process, and bending deformation is easy to occur, which reduces the qualified rate of the product
Especially in the preparation of large-scale honeycomb ceramic regenerators, the qualified rate of the product is often less than 50%; secondly, as a brittle material, honeycomb ceramics are easily damaged by vibration, scratches and collisions during handling, transfer and transportation. Edge defects, edge chipping, and even overall fragmentation, and the thinner outer wall thickness further exacerbates such losses
Even in the assembly stage when the product is put into use, there is also the problem of damage caused by the insufficient strength of the outer wall of the honeycomb ceramic regenerator. All of the above problems have led to a great reduction in the use rate of the product and caused great unnecessary waste.
[0004] However, due to the limitations of the shape and formula of the honeycomb ceramic regenerator, the ratio of the thickness of the inner wall to the outer wall is difficult to break through 1:1.5, because when the thickness of the outer wall of the green body is further increased, the extrusion speed of the outer wall of the mold is much higher than The extrusion speed of the inner wall extrusion area, which causes the blank to be unable to form a whole after being extruded through the die, and even causes the inner core and the outer wall to separate into two parts

Method used

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  • Preparation method of a honeycomb ceramic regenerator with ultra-thick outer wall
  • Preparation method of a honeycomb ceramic regenerator with ultra-thick outer wall
  • Preparation method of a honeycomb ceramic regenerator with ultra-thick outer wall

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0039](1) The extrusion die of the honeycomb ceramic regenerator is cut with 45# steel or die steel. The extrusion die includes an outer mold cover 1 and an inner mold core 7, and several outer walls formed around one end of the outer mold cover Mud entry holes 5, a number of inner wall mud entry holes 3 are formed on one end of the inner mold core, an outer wall 4 is formed at one end of the outer wall mud entry holes, and several criss-cross inner walls 2 are formed at one end of the inner wall mud entry holes. The surface of the extrusion area of ​​the outer wall (the surface of the extrusion area of ​​the outer wall refers to the surface of the outer mold sleeve forming the outer surface of the outer wall) is processed to a roughness requirement of Ra3.2, and groove cutting is performed at the same time, and the parallel interval on the surface of the outer mold sleeve is 10 mm , process a groove 6 with a width of 5 mm and a depth of 1 mm, and adjust the ratio of the cross-...

Embodiment 2

[0044] (1) The extrusion die of the honeycomb ceramic regenerator is cut with 45# steel or die steel. The surface roughness of the extrusion area of ​​the outer wall of the outer die sleeve is required to be Ra3.2. At the same time, groove cutting is performed. Every parallel interval of 10 mm on the surface, process a groove 6 with a width of 5.5 mm and a depth of 0.8 mm, and adjust the ratio of the cross-sectional area of ​​the mud entry hole of the mold to the cross-sectional area of ​​the extrusion outer wall to be 1.5; The internal fixation is provided with a pin 8, and the pin is a paper clip (fixed in the mud entry hole by the elasticity of the paper clip).

[0045] (2) Choose 325-mesh spherical and nearly spherical ceramic powder. The ceramic powder is composed of 30 parts of cordierite, 28 parts of alumina, 10 parts of clay, 17 parts of talcum powder and 15 parts of deionized water. 5% of the weight of the base material is added to the base material as an organosilane...

Embodiment 3

[0049] (1) The extrusion die of the honeycomb ceramic regenerator is cut with 45# steel or die steel. The surface roughness of the extrusion area of ​​the outer wall of the outer die sleeve is required to be Ra3.6. At the same time, groove cutting is performed. Every parallel interval of 10 mm on the surface, process a groove 6 with a width of 4.5 mm and a depth of 0.7 mm, and adjust the ratio of the cross-sectional area of ​​the mud entry hole of the mold to the cross-sectional area of ​​the extrusion outer wall to be 2.0; The internal fixation is provided with a pin 8, and the pin is a paper clip (fixed in the mud entry hole by the elasticity of the paper clip).

[0050] (2) Select 300-mesh spherical and nearly spherical ceramic powder. The ceramic powder is composed of 26 parts of cordierite, 30 parts of alumina, 15 parts of clay, 11 parts of talcum powder and 18 parts of deionized water. Add 3% titanate coupling agent of the weight of the base material as a surfactant, and...

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Abstract

The invention discloses a preparation method of a honeycomb ceramic regenerator with an ultra-thick outer wall. On the outer wall surface of a mold sleeve outside the honeycomb ceramic regenerator, grooves parallel to the extruding direction of mud are arranged at intervals, and the outer wall of the mold sleeve is The surface is processed so that the surface roughness is above 3.2, and pins are arranged in the mud entry hole on the outer wall of the outer mold casing. Spherical fine particle ceramic raw materials and auxiliary materials are selected, and after kneading, mud refining and aging, the mud is extruded with a mud refining machine. , and then add the mud material to the extrusion die sleeve of the extrusion molding machine to make a honeycomb ceramic green body. After the green body is dried and shaped, it is fired at a high temperature. The heat storage per unit volume of the present invention can be increased by 2% to 5%; heat exchange efficiency It can be increased by 3% to 5% accordingly, and the damage rate of the product in the process of handling, transfer, transportation and application assembly is significantly reduced; the deformation defect in the drying and firing process is significantly reduced, the firing pass rate is increased, and the product is reduced. rate, on the other hand to achieve the purpose of energy saving and emission reduction.

Description

technical field [0001] The invention relates to the technical field of porous ceramic processing, in particular to a preparation method of a honeycomb ceramic regenerator with an ultra-thick outer wall. Background technique [0002] Honeycomb ceramic regenerator is widely used in energy-saving technology of industrial thermal equipment, which can improve equipment efficiency and reduce energy consumption, and is an important means to solve energy and environmental problems. Honeycomb ceramics have high specific surface area and good physical and chemical stability, in addition to low density, high permeability, good energy absorption performance, high temperature resistance, corrosion resistance, high chemical stability and dimensional stability, easy to Regeneration and many other features. In recent years, with the development of preparation technology, its application range has been continuously expanded, and its application level has been continuously improved. [0003...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B28B3/20B28B3/26B28C1/16C04B35/10C04B35/195C04B38/00
CPCB28B3/20B28B3/269B28C1/16C04B35/10C04B35/195C04B38/0006
Inventor 吴汉阳徐鹏
Owner JIANGXI BOCENT TEC CO LTD
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