Composite bulletproof plate and preparation method thereof
A technology of composite materials and bulletproof plates, applied in the field of composite materials, can solve the problems of three-dimensional braids that are easy to break, and achieve the effects of improving bullet impact resistance, avoiding breakage, and high bulletproof performance
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[0024] Such as figure 1 As shown, the embodiment of the present invention relates to a method for preparing an alumina-based ceramic composite bulletproof plate, comprising the following steps:
[0025] Impregnation: Pressurize and impregnate the aluminum oxide fiber non-weft cloth in the impregnating liquid aluminum sol with a solid content of 10% to 50% under vacuum conditions, the pH of the impregnating liquid aluminum sol is 3 to 10, and the pressure is 2 to 5 MPa;
[0026] Granulation: choose ɑ-Al with an average particle size of 1-5 μm 2 o 3 Powder, according to aluminum sol and ɑ-Al 2 o 3 Powder weight ratio 5:95~1:1 to ɑ-Al 2 o 3 Adding a binder aluminum sol with a solid content of 10% to 50% to the powder is granulated to obtain ceramic granules;
[0027] Lamination: The alumina fiber non-weft cloth obtained in the impregnation step is pressed according to [0° / 90°] T The method is to lay layers in the mould, the mold is preferably a steel mold mould, and a laye...
Embodiment 1
[0034] Impregnation: Pressurize and impregnate the alumina fiber non-weft cloth in the aluminum sol with a solid content of 20% under vacuum conditions, and the pressure is 4MPa;
[0035] Granulation: choose ɑ-Al with an average particle size of 5 μm 2 o 3 Powder, to ɑ-Al 2 o 3 Add aluminum sol with a solid content of 30% to the powder and then granulate to obtain ceramic particles. The weight ratio of aluminum sol in ceramic particles is 10%, that is, aluminum sol and ɑ-Al 2 o 3 Powder weight ratio is 1:9;
[0036] Lamination: The alumina fiber non-weft cloth obtained in the impregnation step is pressed according to [0° / 90°] T The method is to lay layers in the steel mold, and evenly spread a layer of ceramic particles between two adjacent layers of alumina fiber non-weft cloth to obtain a five-layer structure of laid materials, and dehydrate the laid materials;
[0037] Molding: Put the steel mold in a hydraulic press, heat it up to 120°C, keep it warm for 4 hours, and...
Embodiment 2
[0042] Impregnation: Pressurize and impregnate the alumina fiber non-weft cloth in the aluminum sol with a solid content of 30% under vacuum conditions, and the pressure is 2MPa;
[0043] Granulation: choose ɑ-Al with an average particle size of 3 μm 2 o 3 Powder, to ɑ-Al 2 o 3 Add aluminum sol with a solid content of 30% to the powder and then granulate to obtain ceramic particles. The weight ratio of aluminum sol in ceramic particles is 15%, that is, aluminum sol and ɑ-Al 2 o 3 The powder weight ratio is 3:17;
[0044] Lamination: The alumina fiber non-weft cloth obtained in the impregnation step is pressed according to [0° / 90°] TThe method is to lay layers in the steel mold, and evenly spread a layer of ceramic particles between two adjacent layers of alumina fiber non-weft cloth to obtain a five-layer structure of laid materials, and dehydrate the laid materials;
[0045] Molding: Put the steel mold in a hydraulic press, heat it up to 150°C, keep it warm for 1 hour, ...
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