The invention relates to a liquid-phase sintered
boron carbide bulletproof material and a preparation method thereof. The bulletproof material comprises the following components by
mass: 60 to 98% of
boron carbide, 1 to 20% of alpha-Si3N4, 1 to 10% of alpha-SiC, 0 to 3% of
carbon black and 0 to 25% of an Al-Y additive. The preparation method comprises the following steps: weighing raw materials, putting the weighed
boron carbide, alpha-Si3N4, alpha-SiC and
carbon black into a bowl mill and successively carrying out
wet milling with deionized water as a medium and screening; then carrying out
spray granulation and screening; subjecting obtained
slurry to dry-pressing molding so as to prepare a
green body; and finally, subjecting a processed biscuit to
sintering in the presence of the Al-Y additive under the protection of
argon so as to prepare the liquid-phase sintered
boron carbide bulletproof material. The bulletproof material provided by the invention has
volume density of 2.59 to 2.72 g / cm3 and good
hardness, bending strength, breaking tenacity, elasticity modulus, etc., production cost is low, and production efficiency is high.