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Method for preparing flexible trans-polymer dispersed liquid crystal film by using photoetching technology

A photolithography technology and liquid crystal dispersion technology, which is applied in the field of preparing trans-polymer dispersed liquid crystal films, can solve the problems of poor optical contrast of flexible R-PDLC films, etc.

Active Publication Date: 2020-04-10
HARBIN INST OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] The present invention aims to solve the technical problem of poor optical contrast of existing flexible R-PDLC films, and provides a method for preparing flexible trans-polymer dispersed liquid crystal films using photolithography technology

Method used

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  • Method for preparing flexible trans-polymer dispersed liquid crystal film by using photoetching technology
  • Method for preparing flexible trans-polymer dispersed liquid crystal film by using photoetching technology
  • Method for preparing flexible trans-polymer dispersed liquid crystal film by using photoetching technology

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specific Embodiment approach 1

[0024] Specific Embodiment 1: This embodiment is a method for preparing a flexible trans-polymer dispersed liquid crystal film using photolithography technology, specifically according to the following steps:

[0025] 1. Coating photoresist on the ITO-PET film: Coat the negative photoresist on the ITO of the ITO-PET film. 15min, then placed on a hot table for thermal curing, the curing temperature is 90°C to 120°C, and the curing time is 90s to 200s;

[0026] 2. Photolithographic grooves, development: put the ITO-PET film coated with photoresist into the photolithography machine to fix, photolithographic parallel grooves, the width of each groove is equal and the width of the groove is 1 μm to 10 μm , exposure 120mJ / cm 2 ~170mJ / cm 2 , the distance between the central axes of two adjacent grooves is twice the width of the groove; after photolithography, take out the sheet, soak it in the developing solution for development, the soaking time is 40s~60s, rinse the excess develo...

specific Embodiment approach 2

[0033] Embodiment 2: This embodiment differs from Embodiment 1 in that: the thickness of the ITO-PET film described in Step 1 is 150 μm-200 μm. Others are the same as the first embodiment.

specific Embodiment approach 3

[0034] Embodiment 3: The difference between this embodiment and Embodiment 1 or 2 is that the negative photoresist described in step 1 is SU-8 negative photoresist. Others are the same as those in Embodiment 1 or 2.

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Abstract

The invention discloses a method for preparing a flexible trans-polymer dispersed liquid crystal film by using a photoetching technology, and relates to a method for preparing a trans-polymer dispersed liquid crystal film. The technical problem that an existing flexible R-PDLC film is poor in optical contrast is solved. According to the invention, by changing the width of an orientation groove, the structure and proportion of a liquid crystal ultraviolet polymerizable monomer, the pre-orientation degree of liquid crystal molecules, the polymer network, the molecular weight, the branching degree and the like are changed, a R-PDLC film with flexibility is formed, the strong light protection performance of high light transmittance in a non-electrified state and low light transmittance in an electrified state is achieved, the maximum value and the minimum value of the transmittance are 81.2% and 3.9% respectively, the optical contrast is high, and the photoelectric properties are stable.

Description

technical field [0001] The invention relates to a method for preparing a trans polymer dispersed liquid crystal film. Background technique [0002] The problem of light pollution continues to heat up, and more and more designs of buildings, car windows and aircraft windshields take into account the protection of transient glare. Polymer dispersed liquid crystal (PDLC) is a new type of electrochromic functional film, in which the liquid crystal is dispersed in the polymer matrix in a droplet state, and the difference in refractive index between the liquid crystal and the polymer makes the film transparent in light / Scattering state can be switched freely. PDLC film has the advantages of fast response, high optical contrast, and easy large-scale preparation, and is considered to be the most promising protective material. However, there are still some technical problems with PDLC films: firstly, PDLC needs to be continuously powered on when it is in a transparent state, which...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G02F1/1334G02F1/1337G02F1/1333
CPCG02F1/1334G02F1/133788G02F1/1337G02F1/133305G02F1/13345G02F1/13347
Inventor 朱嘉琦张智博杨磊杨亚楠张锐聪闵萍萍张昕宇姬栋超
Owner HARBIN INST OF TECH
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