Method and device for measuring caking strength parameters of granular material through single solid bridge

A technology of granular materials and fixed particles, which is applied in the direction of measuring devices, monitoring particle agglomeration, and analyzing materials, etc. It can solve the problems of inability to achieve multi-flux, long measurement cycle, single consumption of accelerated agglomeration method, etc.

Active Publication Date: 2020-05-15
TIANJIN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In terms of the consumption of test samples, the consumption of the bagging method is huge, and the single consumption of the accelerated agglomeration method is also at the level of 100 grams. Such a high consumption is almost unbearable for some precious samples.
In terms of measuring devices, the bagging method occupies a large area and cannot be adjusted for temperature and humidity; the sample preparation device for the accelerated test method is often relatively large, and in a conventional temperature and humidity control box (0.5 to 1 cubic meter of space) ) can only place one sample preparation device, and cannot achieve multi-throughput
[0010] Therefore, in order to solve the problems of low accuracy, long measurement period, large consumption of dosage, and difficulty in multi-throughput of the measuring device in the traditional method of measuring caking strength parameters, a method and supporting device are urgently needed to achieve efficient caking strength parameters. accurate measurement

Method used

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  • Method and device for measuring caking strength parameters of granular material through single solid bridge
  • Method and device for measuring caking strength parameters of granular material through single solid bridge
  • Method and device for measuring caking strength parameters of granular material through single solid bridge

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Embodiment 1

[0041] The experimental setup in this example is described below.

[0042] Figure 2A It is a schematic diagram of a preferred embodiment of the present invention. As shown in the figure, 1 is a fixed particle device, and a microscope 2 is placed above it, and the fixed particle device 1 and the microscope 2 are placed in an oven 3 . see Figure 2B ,for Figure 2A Schematic diagram of the immobilized particle device and microscope. Two of the test particles 4 are respectively adhered and fixed on two fixed probes 5, the fixed probes 5 are connected to the pressure / tension sensor 6, the pressure / tension sensor 6 is connected to the telescopic rod 7, and the telescopic rod 7 is connected to the telescopic rod control motor 8 Link to each other, telescopic rod control motor 8 links to each other with platform 9.

[0043] The measurement method of this embodiment is described as follows by taking the measurement of the agglomeration strength parameter of potassium chloride cr...

Embodiment 2

[0047] The experimental setup in this example is described below.

[0048] Figure 3A It is a schematic diagram of another preferred embodiment of the present invention. As shown in the figure, 1 is a particle fixing device, and there is a microscope 2 on its side, and the particle fixing device 1 and the microscope 2 are placed in an oven 3 . There are multiple fixed particle devices 1 for realizing multi-flux measurement. see Figure 3B , two particles 4 are vertically stacked in the glass tube 10 , the lower end of the glass tube 10 is sealed, and its inner diameter is 1 to 1.9 times the diameter of the particles 4 , and the particles put in later are stuck by the lifting mechanical arm 11 .

[0049] The measurement method of this embodiment is described as follows by taking the measurement of the agglomeration strength parameter of potassium chloride crystal as an example.

[0050] In this embodiment, the mechanical arm 11 is controlled to move up and down so that the ...

Embodiment 3

[0053] The experimental setup in this example is described below.

[0054] Figure 4A It is a schematic diagram of another preferred embodiment of the present invention. As shown in the figure, 1 is a particle fixing device, and there is a microscope 2 above it, and the particle fixing device 1 and the microscope 2 are placed in an oven 3 . see Figure 4B , two particles 4 are placed horizontally on the platform 13, one of the particles 4 is adhered and fixed by the fixed probe 5, the fixed probe 5 is connected to the connecting rod 12, the bottom of the platform 13 is connected to the screw rod 14, and the screw rod 14 is connected to the manual rocker 15 , the bottom ends of the connecting rod 12 and the manual rocker 15 are all connected and fixed with the platform 9, and the side below the platform is connected with an adjustable foot 16. see Figure 4C ,for Figure 4B The top view of the fixed particle device. Two particles are placed stably in the grooves of platfo...

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Abstract

The invention relates to a method and a device for measuring caking strength parameters of a granular material through a single solid bridge. Two particles are fixed through the device, a single solidbridge is generated between the two particles through temperature and humidity control, the radius of the fixed bridge is measured through a microscope, the solid bridge is destroyed through externalforce, and therefore the caking strength parameter of the material is obtained through calculation according to the formula sigma = C/pib2 or sigma = G/pibc2, wherein sigma is the caking strength parameter of the granular material, b is the radius of a solid bridge, and C is the force required by the solid bridge with the crushing radius of b, namely the caking strength; G is the particle weight,and bc is the critical solid bridge radius. The device is composed of a temperature and humidity control box, a particle fixing device and a microscope. The particle fixing device can be in the formsof double-mechanical-arm pressure sensing, lifting, platform descending, vibration and the like. The method has the advantages of more accurate physical significance and credibility, high precision,strong repeatability, short measurement period, less sample consumption, high flux and the like.

Description

technical field [0001] The invention relates to a measuring method and device, in particular to a method and device for measuring the agglomeration strength parameters of granular materials through a single solid bridge. Background technique [0002] Solid particles are a very common product form in industrial production. In the fields of medicine, chemistry, food, fertilizer, detergent, military industry, etc., solid products tend to be prepared in a single, dispersed state to have good fluidity and stability, thereby enhancing commercial competitiveness. However, in the downstream process of granular products (filtering, washing, drying, transportation, storage and sales), agglomeration is very easy to occur, resulting in the loss of fluidity and stability of the product, a significant decrease in product value, and an increase in production and use costs. The pervasiveness and harmfulness of agglomeration plague many production fields and become the main factor hindering...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N15/00
CPCG01N15/00G01N2015/0092
Inventor 龚俊波陈明洋余畅游姚孟惠刘岩博汤伟伟吴送姑杜世超高振国侯宝红尹秋响
Owner TIANJIN UNIV
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