Injectable presentations, syringes and compositions with sustained and/or controlled release of lanreotide
A technology of syringes, compositions, applied in the field of injectable dosage forms, capable of solving problems such as not satisfactorily resolved
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Embodiment 1
[0189] Preparation of compositions with 18-21% or 22% or even 25% of lanreotide in the form of lanreotide acetate in two types of solvents: water and a 95:5% water / ethanol mixture
[0190] The preparation is carried out by a reciprocating technique between 2 reservoirs of the syringe type, closed on one side by a piston and on the other side by means connected to a valve to allow the regulation of lansel acetate optionally under vacuum Peptide powder, hydrate the powder with a solvent and reciprocate mix the product through the connection opening of the regulating valve, which optionally measures the force applied to control the type of mixture to be prepared.
[0191] By comparing the method of making these blends with the method of making a 25% lanreotide composition comparable to the commercially available product, we see that making these 18-22% formulations is easier and faster and requires less mixing force. Mixtures of this type can then also be extrapolated to much la...
Embodiment 2
[0195] Composition comprising 19.0% lanreotide in water
[0196] Batch prepared from 1.88 g of lanreotide acetate and purified water.
[0197] The formulation was prepared by the reciprocating technique described in Example 1 using 2 plastic syringes connected to a connector that allowed mixing after the lanreotide acetate powder was hydrated with water. The obtained compositions were dispensed in different injection systems to evaluate injection force and other parameters such as peptide content and chromatographic purity.
Embodiment 3
[0199] Composition comprising 19.5% lanreotide in water and ethanol
[0200] A batch prepared from 0.36 g of lanreotide acetate and a 95:5 mixture of purified water and ethanol. A 95:5 water-alcohol mixture was prepared by mixing 1.906 g of purified water with 0.103 g of 96% ethanol.
[0201] Preparation was performed by the reciprocating technique described in Example 1, using 2 plastic syringes connected to a connector allowing mixing after hydration of the lanreotide acetate powder with the water / ethanol mixture. The obtained compositions were dispensed in different injection systems to evaluate injection force and other parameters such as peptide content and chromatographic purity.
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