High-stability environment-friendly calcium-zinc stabilizer for PVC and preparation method thereof

A calcium-zinc stabilizer and a high-stability technology are applied in the field of environmental-friendly calcium-zinc stabilizer for high-stability PVC and its preparation, which can solve the problems of easy discoloration, poor weather resistance, and the reduction of the strength of PVC materials by adding content.

Inactive Publication Date: 2021-01-22
SHENZHEN AIMSEA IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] However, the PVC stabilizers currently on the market have poor weather resistance, are prone to

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0054] Add the raw materials into a high-speed mixer, and stir at 80°C for 20 minutes to obtain the environmentally friendly calcium-zinc stabilizer for high-stability PVC, and the stirring speed is 800 rpm;

[0055] Described raw material is:

[0056] Calcium stearate 100 parts

[0057] Zinc stearate 80 parts

[0058] Sulfonated polystyrene coated hydroxyapatite 30 parts

[0059] Polyethylene wax 5 parts

[0060] Octaphenylamino cage silsesquioxane 5 parts

[0061] 1,3-dibromopropane 5 parts

[0062] Antioxidant 1010 1 part

[0063] 1 part of N-[3-(triethoxysilyl)propyl]-4,5-dihydroimidazole

[0064] KH-550 1 part

[0065] 1 copy of KH-560;

[0066] The preparation method of the sulfonated polystyrene coated hydroxyapatite is:

[0067] (1) Add 10 grams of hydroxyapatite (average particle size of 200 nanometers), 2 grams of hydroxypropyl starch and 1 gram of KH-550 to 200 ml of ethanol in sequence, raise the temperature to 70°C and stir for 30 minutes;

[0068] (2) T...

Embodiment 2

[0070] Add the raw materials into a high-speed mixer, and stir at 80°C for 20 minutes to obtain the environmentally friendly calcium-zinc stabilizer for high-stability PVC, and the stirring speed is 800 rpm;

[0071] Described raw material is:

[0072] Calcium stearate 100 parts

[0073] Zinc stearate 120 parts

[0074] Sulfonated polystyrene coated hydroxyapatite 50 parts

[0075] Polyethylene wax 10 parts

[0076] Octaphenylamino cage silsesquioxane 15 parts

[0077] 10 parts of 1,3-dibromopropane

[0078] Antioxidant 1010 10 parts

[0079] 10 parts of N-[3-(triethoxysilyl)propyl]-4,5-dihydroimidazole

[0080] KH-550 5 parts

[0081] KH-560 5 copies;

[0082] The preparation method of the sulfonated polystyrene coated hydroxyapatite is:

[0083] (1) Add 10 grams of hydroxyapatite (average particle size of 200 nanometers), 2 grams of hydroxypropyl starch and 1 gram of KH-550 to 200 ml of ethanol in sequence, raise the temperature to 70°C and stir for 30 minutes;

[...

Embodiment 3

[0086] Add the raw materials into a high-speed mixer, and stir at 80°C for 20 minutes to obtain the environmentally friendly calcium-zinc stabilizer for high-stability PVC, and the stirring speed is 800 rpm;

[0087] Described raw material is:

[0088] Calcium stearate 100 parts

[0089] Zinc stearate 100 parts

[0090] Sulfonated polystyrene coated hydroxyapatite 43 parts

[0091] Polyethylene wax 8 parts

[0092] Octaphenylamino cage silsesquioxane 11 parts

[0093] 9 parts of 1,3-dibromopropane

[0094] Antioxidant 1010 8 parts

[0095] 7 parts of N-[3-(triethoxysilyl)propyl]-4,5-dihydroimidazole

[0096] KH-550 3 copies

[0097] KH-560 3 copies;

[0098] The preparation method of the sulfonated polystyrene coated hydroxyapatite is:

[0099] (1) Add 10 grams of hydroxyapatite (average particle size of 200 nanometers), 2 grams of hydroxypropyl starch and 1 gram of KH-550 to 200 ml of ethanol in sequence, raise the temperature to 70°C and stir for 30 minutes;

[0100]...

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Abstract

The invention relates to a high-stability environment-friendly calcium-zinc stabilizer for PVC, which is prepared from the following raw materials in parts by weight: calcium stearate, zinc stearate,sulfonated polystyrene coated hydroxyapatite, polyethylene wax, octaphenylamino polyhedral oligomeric silsesquioxane, 1, 3-dibromopropane, an an antioxidant 1010, N-[3 (triethoxysilane)propyl]-4, 5-dihydro-imidazole, KH550 and KH560. The invention also relates to a preparation method of the calcium-zinc stabilizer.

Description

technical field [0001] The invention belongs to the technical field of stabilizers. More specifically, the invention relates to an environment-friendly calcium-zinc stabilizer for high-stability PVC and a preparation method thereof. Background technique [0002] As we all know, the performance of stabilizers has a great influence on the stability of PVC materials. Commonly used heat stabilizers are mainly lead salt stabilizers, which are cheap and have good heat stabilization effects, but they are highly toxic, seriously endangering human health and polluting the environment. The non-toxic calcium-zinc compound Ca / Zn heat stabilizer is a non-toxic and environment-friendly heat stabilizer recognized by the world, and has the advantages of low price and good lubricity, and has a very broad development space. [0003] However, the PVC stabilizers currently on the market have poor weather resistance, are prone to discoloration, and will significantly reduce the strength of PVC ...

Claims

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Application Information

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IPC IPC(8): C08L27/06C08L83/08C08L23/06C08L63/00C08K13/06C08K9/10C08K3/32C08K5/098C08K5/02C08K5/134C08K5/544C08K5/5435C08K5/3445
CPCC08K2003/325C08L27/06C08L2201/08C08L2205/03C08L2205/035
Inventor 严晴严一丰
Owner SHENZHEN AIMSEA IND
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