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9% Ni steel super-large-sized rotor forging applied to ultralow-temperature engineering and preparation method thereof

A technology for oversized, rotor forgings, used in metal processing equipment, furnace types, manufacturing tools, etc., to achieve good grain condition, excellent room temperature and low temperature mechanical properties, and good internal structure uniformity.

Active Publication Date: 2021-04-20
CENT IRON & STEEL RES INST +3
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The manufacture of 9% Ni steel rotors with a section size exceeding Φ1000mm used under ultra-low temperature conditions is still blank in the prior art

Method used

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  • 9% Ni steel super-large-sized rotor forging applied to ultralow-temperature engineering and preparation method thereof
  • 9% Ni steel super-large-sized rotor forging applied to ultralow-temperature engineering and preparation method thereof
  • 9% Ni steel super-large-sized rotor forging applied to ultralow-temperature engineering and preparation method thereof

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preparation example Construction

[0033] The invention provides a method for preparing a 9% Ni steel ultra-large rotor forging for ultra-low temperature engineering, comprising the following steps:

[0034] Weigh the corresponding raw materials according to the following weight percentages: C 0.02~0.06%, Si≤0.20%, Mn0.50~0.80%, S≤0.003%, P≤0.008%, Cr≤0.20%, Ni 9.50%~10.0%, Mo0 .08~0.14%, Cu0.10~0.20%, Al≤0.015%, As≤0.005%, Sn≤0.005%, Sb≤0.0015%, Pb≤0.005%, Bi≤0.005%, H≤1.0ppm, O≤ 20ppm, N≤50ppm, the balance is high-purity Fe;

[0035] The weighed raw materials are smelted by vacuum induction-electroslag remelting process, and the obtained smelting liquid is cast to obtain steel ingots;

[0036] Stepwise heating and forging the steel ingot to obtain a rotor forging;

[0037] The rotor forging is sequentially subjected to preliminary heat treatment and performance heat treatment to obtain a 9% Ni steel ultra-large rotor forging for ultra-low temperature engineering.

[0038]The present invention weighs corres...

Embodiment 1

[0077] Weigh raw materials according to the following weight percentages: C 0.05%, Si 0.16%, Mn 0.74%, S 0.002%, P0.007%, Cr 0.12%, Ni 9.71%, Mo 0.09%, Cu 0.15%, Al 0.006%, As 0.003%, Sn0.002%, Sb 0.0012%, Pb 0.002%, Bi 0.002%, H 0.5ppm, O 10ppm, N 36ppm, the balance is high-purity Fe;

[0078] The weighed raw materials are smelted by vacuum induction-electroslag remelting process, and the obtained smelting liquid is cast to obtain steel ingots; the parameters of the vacuum induction-electroslag remelting include: the parameters of vacuum induction melting include: the chemical power is 700kW , the rate of power increase is 200kW / h; the refining temperature is 1570°C, and the vacuum degree is <0.1Pa; at the end of refining, Ca is used for early deoxidation, and after the composition is adjusted to pass, Ni-Mg alloy is used for final deoxidation, and the final tapping temperature is controlled at 1590°C ; The electroslag remelting process preferably includes: 4 sets / sets of vac...

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Abstract

The invention provides a 9% Ni steel super-large-specification rotor forging applied to ultralow-temperature engineering and a preparation method thereof, and belongs to the technical field of low-temperature metal materials. Through reasonable control of components of the raw materials, a forging process, a preparation heat treatment process and a performance heat treatment process, the grain size of the final rotor forging is not lower than the sixth grade; the grain state is good; when ultrasonic flaw detection test is carried out, attenuation of the rotor forging with a diameter of 1000mm and a length near 7500mm is not greater than 2.2dB / m, proving that the rotor forging has good internal structure uniformity; Meanwhile, full-cross-section and all-directional system test of the 9% Ni steel super-large-sized rotor forging applied to ultralow-temperature engineering shows that the room-temperature tensile strength reaches 679-728 MPa, the impact energy at 196 DEG C below zero reaches 160-300J, the fracture toughness at 196 DEG C below zero reaches 166-201 MPa.m<1 / 2>, and the 9% Ni steel super-large-sized rotor forging has extremely excellent room-temperature and low-temperature comprehensive mechanical properties.

Description

technical field [0001] The invention relates to the technical field of low-temperature metal materials, in particular to a 9% Ni steel super-sized rotor forging for ultra-low temperature engineering and a preparation method thereof. Background technique [0002] 9% Ni steel has high low-temperature strength and excellent low-temperature toughness, and is suitable for working in various extreme low-temperature environments. 9% Ni steel was first invented by the American INCO company in the 1940s for the manufacture of LNG storage tanks. The United States, Japan, South Korea and a few Western European countries have mastered the relevant key technologies of 9% Ni steel earlier, and these countries have carried out a lot of basic theoretical and experimental research work on 9% Ni steel. The development of 9% Ni steel in my country is later than developed countries such as Europe, America and Japan, and it is one of the most difficult steel grades recognized by domestic iron a...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C38/02C22C38/04C22C38/06C22C38/42C22C38/44C22C38/60B21J5/00C21D8/00C22B9/18C22C33/04C21D9/00
CPCY02P10/25
Inventor 梁剑雄张智峰王长军陈万华周恩民董凯刘振宝程莉廖达雄杨志勇李向孙永庆
Owner CENT IRON & STEEL RES INST