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9% Ni steel ultra-large rotor forging for ultra-low temperature engineering and its preparation method

A technology for rotor forgings and super-large specifications, which is applied in the field of ultra-low temperature engineering 9% Ni steel super-sized rotor forgings and its preparation, and achieves the effects of excellent room temperature and low temperature mechanical properties, good grain state, and good internal structure uniformity.

Active Publication Date: 2021-12-03
CENT IRON & STEEL RES INST +3
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The manufacture of 9% Ni steel rotors with a section size exceeding Φ1000mm used under ultra-low temperature conditions is still blank in the prior art

Method used

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  • 9% Ni steel ultra-large rotor forging for ultra-low temperature engineering and its preparation method
  • 9% Ni steel ultra-large rotor forging for ultra-low temperature engineering and its preparation method
  • 9% Ni steel ultra-large rotor forging for ultra-low temperature engineering and its preparation method

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preparation example Construction

[0033] The invention provides a method for preparing a 9% Ni steel ultra-large rotor forging for ultra-low temperature engineering, comprising the following steps:

[0034] Weigh the corresponding raw materials according to the following weight percentages: C 0.02~0.06%, Si≤0.20%, Mn 0.50~0.80%, S≤0.003%, P≤0.008%, Cr≤0.20%, Ni 9.50%~10.0%, Mo 0.08 ~0.14%, Cu0.10~0.20%, Al≤0.015%, As≤0.005%, Sn≤0.005%, Sb≤0.0015%, Pb≤0.005%, Bi≤0.005%, H≤1.0ppm, O≤20ppm, N≤50ppm, the balance is high-purity Fe;

[0035] The weighed raw materials are smelted by vacuum induction-electroslag remelting process, and the obtained smelting liquid is cast to obtain steel ingots;

[0036] Stepwise heating and forging the steel ingot to obtain a rotor forging;

[0037] The rotor forging is sequentially subjected to preliminary heat treatment and performance heat treatment to obtain a 9% Ni steel ultra-large rotor forging for ultra-low temperature engineering.

[0038]The present invention weighs corre...

Embodiment 1

[0077] Weigh raw materials according to the following weight percentages: C 0.05%, Si 0.16%, Mn 0.74%, S 0.002%, P0.007%, Cr 0.12%, Ni 9.71%, Mo 0.09%, Cu 0.15%, Al 0.006%, As 0.003%, Sn0.002%, Sb 0.0012%, Pb 0.002%, Bi 0.002%, H 0.5ppm, O 10ppm, N 36ppm, the balance is high-purity Fe;

[0078] The weighed raw materials are smelted by vacuum induction-electroslag remelting process, and the obtained smelting liquid is cast to obtain steel ingots; the parameters of the vacuum induction-electroslag remelting include: the parameters of vacuum induction melting include: the chemical power is 700kW , the rate of power increase is 200kW / h; the refining temperature is 1570°C, and the vacuum degree is <0.1Pa; at the end of refining, Ca is used for early deoxidation, and after the composition is adjusted to pass, Ni-Mg alloy is used for final deoxidation, and the final tapping temperature is controlled at 1590°C ; The electroslag remelting process preferably includes: 4 sets / sets of vac...

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Abstract

The invention provides a 9% Ni steel ultra-large rotor forging for ultra-low temperature engineering and a preparation method thereof, belonging to the technical field of low-temperature metal materials. In the present invention, by rationally controlling the composition of raw materials, forging process, preparatory heat treatment process and performance heat treatment process, the grain size of the final rotor forging is not lower than grade 6, and the grain state is good; when the ultrasonic flaw detection test is carried out, the diameter reaches 1000mm, The attenuation of the rotor forging with a length of nearly 7500mm does not exceed 2.2dB / m, which proves that the internal structure of the rotor forging is uniform. At the same time, a full-section and omni-directional systematic test was carried out on the 9% Ni steel super-sized rotor forgings for ultra-low temperature engineering, and it was obtained: the tensile strength at room temperature reached 679-728MPa, the impact energy at ‑196°C reached 160-300J, and the fracture toughness at ‑196°C The pressure reaches 166~201MPa·m 1 / 2 , with excellent comprehensive mechanical properties at room temperature and low temperature.

Description

technical field [0001] The invention relates to the technical field of low-temperature metal materials, in particular to a 9% Ni steel super-sized rotor forging for ultra-low temperature engineering and a preparation method thereof. Background technique [0002] 9% Ni steel has high low-temperature strength and excellent low-temperature toughness, and is suitable for working in various extreme low-temperature environments. 9% Ni steel was first invented by the American INCO company in the 1940s for the manufacture of LNG storage tanks. The United States, Japan, South Korea and a few Western European countries have mastered the relevant key technologies of 9% Ni steel earlier, and these countries have carried out a lot of basic theoretical and experimental research work on 9% Ni steel. The development of 9% Ni steel in my country is later than developed countries such as Europe, America and Japan, and it is one of the most difficult steel grades recognized by domestic iron a...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22C38/02C22C38/04C22C38/06C22C38/42C22C38/44C22C38/60B21J5/00C21D8/00C22B9/18C22C33/04C21D9/00
CPCY02P10/25
Inventor 梁剑雄张智峰王长军陈万华周恩民董凯刘振宝程莉廖达雄杨志勇李向孙永庆
Owner CENT IRON & STEEL RES INST