Method for regulating and controlling LPFG sensitivity by polymethacrylic acid
A polymethacrylic acid and methacrylic acid technology, which is applied in the measurement of phase influence characteristics, instruments, optical waveguides and light guides, etc., can solve the problem of low response sensitivity of low-refractive index media, and achieve the effect of stable growth of thin films.
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Embodiment 1
[0038]The mixed solution of 5 ml dimethyl sulfoxide was formulated with 0.86 g of 2-methacrylic acid, 1.98 g of polyethylene glycol dimethyl methacrylate and 0.2 g of 2,2'-azobutyronitrile, stirred well, will The solution was poured into a liquid reaction tank that fixed the long period of the raster, and the reaction temperature was transferred to 50 ° C, control the reaction time, stop the reaction time to stop the reaction time when the sensitivity of the refractive index reaches the desired request, and fully rinsed with secondary distilled water.
Embodiment 2
[0040]0.06 mol of 2-methacrylic acid and 0.04 mol of polyethylene glycol dimethyl methacrylate were prepared into 10 ml of tetrahydrofuran solution, and 0.001 mol of 2,2'-azo diisobutyronitrile was added, and the stirring was uniform. In the liquid reaction tank of the fixed long period grating, the reaction temperature was transferred to 60 ° C, and the reaction time was controlled, so that the long period grating stopped the reaction when the sensitivity of the refractive index reached the required requirements, and fully rinsed with secondary distilled water .
Embodiment 3
[0042]3.44 g of 2-methacrylic acid, 3.96 g of polyethylene glycol dimethacrylate is compounded into 5 mL dimethyl sulfoxide solution, and two solutions are mixed, and then 0.3 g of 2,2'-azo two different. Nitrile, stirring makes it uniform. In the reaction tank of the formulated solution, the temperature of the solution was adjusted to 80 ° C, control the reaction time, so that the long period grating on the sensitivity of the refractive index reached the required requirements, and used two The distilled water is fully rinsed.
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