Ceramic coating for lithium or sodium metal electrodes
An electrode and metal technology, applied in the field of lithium or sodium metal electrodes, can solve the problems of increasing battery impedance, reducing cycle efficiency and cycle life
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[0090] An anode comprising a lithium metal active material coated with a mesoporous membrane comprising a ceramic oxide is fabricated according to methods of the present technology. This whole process is carried out in a glove box. More specifically, a binder solution was prepared comprising 6% by weight polyvinylidene fluoride (PVDF) in N-methyl-2-pyrrolidone (NMP). Will Li 2 SiO 3 Add to the binder solution and disperse with a planetary mixer (THINKY, Laguna Hills, CA) for about 5 minutes to form a 2 SiO 3 and a slurry of 5-20% by weight binder solution and having a viscosity of 5000-6000 cps. 0.5 mL of this slurry was applied to the surface of the lithium metal anode, and the electrode was rotated at about 2000 rpm for about 30 seconds. The rotation is repeated as many times as necessary until a predetermined thickness is reached, which in this example is about 1-10 microns. A final spin at about 3000 rpm for about 10 seconds was performed to remove additional slurry ...
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