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Building petroleum asphalt No.10 and preparation method thereof

A technology for petroleum asphalt and deoiled asphalt, which is used in construction, building components, building structures, etc., can solve problems such as environmental pollution caused by oxidation processes, and achieve the effect of solving production restrictions and enriching asphalt production processes.

Active Publication Date: 2021-07-16
SHANDONG JINGBO PETROCHEM +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] At this stage, construction petroleum asphalt No. 10 mainly adopts the production process of oxidation method, but the oxidation process has seriously polluted the environment, and the country has banned the construction of asphalt oxidation devices

Method used

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  • Building petroleum asphalt No.10 and preparation method thereof
  • Building petroleum asphalt No.10 and preparation method thereof
  • Building petroleum asphalt No.10 and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0030] In the present invention, the preparation method of described deoiled bitumen preferably comprises:

[0031] Prepared by solvent deasphalting process.

[0032] The present invention has no special limitation on the source of the deoiled asphalt, which can be prepared according to the above method, or purchased from the market, such as Hengli Petrochemical deoiled asphalt 200#.

[0033] In the present invention, the oily substance is selected from hydrogenated tail oil and / or re-refined oil; the kinematic viscosity of the oily substance at 100°C is preferably 1-10mm 2 / s, more preferably 2-8mm 2 / s, most preferably 3~6mm 2 / s; the flash point of the oily substance is preferably ≥ 260°C; the mass content of aromatics in the oily substance is preferably 65-75%, more preferably 68-72%, and most preferably 70%.

[0034] In the present invention, the hydrogenated oil can be purchased from the market, for example, hydrogenated tail oil from Hengli Petrochemical can be used....

Embodiment 1

[0051] Using deoiled asphalt (penetration at 25°C 2dmm, softening point 110°C), re-refined oil (kinematic viscosity at 100°C 2mm 2 / s, aromatics mass content 67%), SBS modifier (molecular weight 125,000), sulfur (content (purity) > 99%) prepares No. 10 of construction petroleum asphalt, with 150 weight parts of deoiled asphalt, 30 weight parts of back refining oil Mix evenly, heat and stir evenly at 150°C, then add 3 parts by weight of SBS, heat and stir at 170°C until there are no solid particles, add 0.017 parts by weight of sulfur, stir evenly at 170°C, and take 3 hours in total.

[0052] The performance test was carried out on No. 10 construction petroleum asphalt prepared in Example 1 of the present invention, and the test results are shown in Table 1.

[0053]Table 1 No. 10 performance test results of construction petroleum asphalt prepared by Example 1 of the present invention

[0054]

[0055]

Embodiment 2

[0057] Using deoiled asphalt (penetration at 25°C 2dmm, softening point 110°C), re-refined oil (kinematic viscosity at 100°C 2mm 2 / s, aromatics mass content 67%), SBS modifier (molecular weight 125,000), sulfur (content > 99%) prepare No. 10 construction petroleum asphalt, 160 weight parts of deoiled pitch, 20 weight parts of back refining oil are mixed uniformly, Heat and stir at 150°C, then add 2 parts by weight of SBS, heat and stir at 170°C until there are no solid particles, add 0.017 parts by weight of sulfur, and stir at 170°C for a total of 3 hours.

[0058] The performance test was carried out on the construction petroleum asphalt No. 10 prepared in Example 2 of the present invention, and the test results are shown in Table 2.

[0059] Table 2 No. 10 performance test results of construction petroleum asphalt prepared by Example 2 of the present invention

[0060]

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Abstract

The invention provides building petroleum asphalt No.10. The building petroleum asphalt No.10 is prepared from deoiled asphalt, hydrogenated tail oil and / or recycle oil, SBS and sulfur. Compared with the prior art, the method has the advantages that the deoiled asphalt which cannot meet the requirements of asphalt indexes (GBT494-2010 building petroleum asphalt), the hydrogenated tail oil / recycle oil, the SBS and the sulfur are prepared into the qualified building petroleum asphalt No.10, on one hand, the source of asphalt production raw materials is widened, wax-containing crude oil can also serve as the asphalt production raw materials, and the obtained deoiled asphalt serves as the raw material of the asphalt No.10; and on the other hand, the asphalt production process is enriched, and the production limitation on the No.10 asphalt caused by the environmental protection problem is solved. The invention also provides a preparation method of the building petroleum asphalt No.10.

Description

technical field [0001] The invention belongs to the technical field of petroleum asphalt, in particular to No. 10 construction petroleum asphalt and a preparation method thereof. Background technique [0002] With the rapid development of my country's economic construction, especially infrastructure, the demand for waterproof materials is increasing, and the scope of application is also expanding rapidly. There are many types of waterproof materials, especially environmental protection and multi-functionality have become the development direction of waterproof materials in the future. [0003] Petroleum asphalt is a product of crude oil processing. It is a black or dark brown viscous liquid, semi-solid or solid at room temperature. It mainly contains hydrocarbons and non-hydrocarbon derivatives soluble in trichlorethylene. Its properties The composition and composition vary with crude oil sources and production methods. At present, the main production methods of petroleum ...

Claims

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Application Information

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IPC IPC(8): C08L95/00C08L91/00C08L53/02C08K3/06
CPCC08L95/00C08L2205/03C08L91/00C08L53/02C08K3/06
Inventor 张红娟祁聪栾波王耀伟刘建伟孙美丽谢强
Owner SHANDONG JINGBO PETROCHEM