A kind of 5g application low-loss soft ferrite material and preparation method thereof
A soft ferrite, low-loss technology, used in magnetic materials, inductance/transformer/magnet manufacturing, magnetic objects, etc., can solve problems such as power loss not reflected, achieve adjustable microwave electromagnetic performance, reduce conductivity loss, The effect of enhanced absorption capacity
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Embodiment 1
[0030] A 5g application low-loss soft ferrite material and a preparation method thereof, comprising the following steps:
[0031] (1) Take modified 36.8mol% modified Fe 2 o 3 , 36.8mol% Mn 3 o 4 , 26.4mol% ZnO mixture, add zirconium balls and liquid forming material: after the ball: liquid ratio is 1:3:2 ball milling medium, put it into the ball mill pot for mixing and ball milling to form powder, the ball milling time is 80min, the slurry is average The particle size is around 1.1 μm.
[0032] (2) Pre-burn the powder obtained in step (1) using a natural gas rotary kiln at 960°C under air conditions for 4 hours, with a feed rate of 2kg / h and a rotation speed of 2N / min, to obtain a spinel synthesis degree of 12 % ferrite powder.
[0033] (3) Add 300ppmCaCO3, 100ppmNb to the ferrite powder obtained in step (2) 2 o 5 , 50ppmBi2O3, 100ppmCo2O3, mix evenly, and put the mixed material into the ball mill tank for secondary ball milling, wherein: material: ball: liquid ratio is...
Embodiment 2
[0037] A 5g application low-loss soft ferrite material and a preparation method thereof, comprising the following steps:
[0038] (1) Take modified 38.5mol% modified Fe 2 o 3 , 33.3mol% Mn 3 o 4 , 28.2mol% ZnO mixture, add zirconium balls and liquid forming material: after the ball: liquid ratio is 1:3:2 ball milling medium, put it into the ball mill tank for mixing and ball milling to form powder, the ball milling time is 80min, the slurry is average The particle size is around 1.1 μm.
[0039] (2) The powder obtained in step (1) is pre-fired at a temperature of 960°C for 4 hours in a natural gas rotary kiln under air conditions, the feed rate is 2.5kg / h, and the rotation speed is 2N / min to obtain a spinel synthesis degree of 15% ferrite powder.
[0040] (3) Add 300ppm CaCO to the ferrite powder obtained in step (2) 3 , 100ppmV 2 o 5 、50ppm Bi 2 o 3 , 100ppm Co 2 O3, 300Ce 2 SnO 5 Finally, mix evenly, and put the mixed material into the ball mill tank for seconda...
Embodiment 3
[0044] A 5g application low-loss soft ferrite material and a preparation method thereof, comprising the following steps:
[0045] (1) Take modified 37.6mol% modified Fe 2 o 3 , 34.9mol% Mn 3 o 4 , 27.5mol% ZnO mixture, add zirconium balls and liquid forming material: after the ball: liquid ratio is 1:3:2 ball milling medium, put it into the ball mill pot for mixing and ball milling to form powder, the ball milling time is 80min, the slurry is average The particle size is around 1.1 μm.
[0046] (2) The powder obtained in step (1) is pre-fired at a temperature of 960°C for 4 hours in a natural gas rotary kiln under air conditions, the feed rate is 2.7kg / h, and the rotation speed is 2N / min to obtain a spinel synthesis degree of 18% ferrite powder.
[0047] (3) Add 200ppm CaCO to the ferrite powder obtained in step (2) 3 , 100ppmV 2 o 5 、50ppm Bi 2 o 3 , 100ppmMoO 3 、300Pr 2 SnO 5 After mixing evenly, put the mixed material into the ball mill tank for secondary ball ...
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