Production process for effectively extracting organic germanium, biological selenium and chalcone from angelica keiskei
A production process, organic germanium technology, applied in the field of Ashitaba extraction, can solve problems such as ineffective extraction and separation, failure of enrichment of selenium and germanium, waste of resources, etc.
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Embodiment 1
[0032] A production process for effectively extracting biological organic germanium, biological selenium and chalcone from Ashitaba, comprising the following steps:
[0033] Step 1. Ultrasonic extraction of ashitaba once
[0034] Cut the freshly picked Ashitaba leaves into chunks with a length of 0.5-1cm, extract once with chloroform that is 3 times the weight of the freshly picked Ashitaba leaves, and use ultrasonic conditions at a temperature of 30-40°C and a power of 80 Extract at -100W for 3min, filter out the insoluble matter, and separate the filtrate to obtain a water layer and an oil layer;
[0035] Step 2, Ultrasonic extraction of insoluble matter once
[0036] Put the insoluble matter in step 1 into a chloroform solution that is 3 times the weight of the freshly picked Ashitaba leaves and extract it once. Under the ultrasonic conditions, the temperature is 40-45°C, the power is 100-150W, and the extraction time is 10 minutes, and the insoluble matter is filtered out...
Embodiment 2
[0044] A production process for effectively extracting biological organic germanium, biological selenium and chalcone from Ashitaba, comprising the following steps:
[0045] Step 1. Ultrasonic extraction of ashitaba once
[0046] Cut the freshly picked Ashitaba leaves into chunks with a length of 0.5-1cm, extract once with chloroform that is 3 times the weight of the freshly picked Ashitaba leaves, and use ultrasonic conditions at a temperature of 30-40°C and a power of 80 Extract at -100W for 3min, filter out the insoluble matter, and separate the filtrate to obtain a water layer and an oil layer;
[0047] Step 2, Ultrasonic extraction of insoluble matter once
[0048] Put the insoluble matter in step 1 into a chloroform solution that is 3 times the weight of the freshly picked Ashitaba leaves and extract it once. Under the ultrasonic conditions, the temperature is 40-45°C, the power is 100-150W, and the extraction time is 10 minutes, and the insoluble matter is filtered out...
Embodiment 3
[0056] A production process for effectively extracting biological organic germanium, biological selenium and chalcone from Ashitaba, comprising the following steps:
[0057] Step 1, Ultrasonic Extraction of Ashitaba once Cut the freshly picked Ashitaba leaves into chunks with a length of 0.5-1cm, and use 3 times the weight of freshly picked Ashitaba leaves to extract once with chloroform, under ultrasonic conditions Extract at a temperature of 30-40°C and a power of 80-100W for 3 minutes, filter out the insoluble matter, and separate the filtrate to obtain a water layer and an oil layer;
[0058] Step 2. Ultrasonic extraction of insoluble matter once. Put the insoluble matter in step 1 into a chloroform solution that is 3 times the weight of freshly picked Ashitaba leaves and extract once. Under the ultrasonic conditions, the temperature is 40-45°C, and the power is 100- 150W, leaching for 10min, filtering out the insoluble matter, separating the filtrate to obtain a water lay...
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