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Production process for effectively extracting organic germanium, biological selenium and chalcone from angelica keiskei

A production process, organic germanium technology, applied in the field of Ashitaba extraction, can solve problems such as ineffective extraction and separation, failure of enrichment of selenium and germanium, waste of resources, etc.

Pending Publication Date: 2021-08-31
潘惟谦
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Moreover, the ashitaba grown in selenium-enriched and germanium-enriched cultures contains more organic germanium and biological selenium, but the existing process is extracting chalcones, which cannot effectively extract and separate organic germanium and biological selenium, resulting in a waste of resources and rich selenium and germanium failed, so it is of great significance to separate and purify organic germanium, biological selenium and chalcone from Ashitaba

Method used

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  • Production process for effectively extracting organic germanium, biological selenium and chalcone from angelica keiskei
  • Production process for effectively extracting organic germanium, biological selenium and chalcone from angelica keiskei

Examples

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Embodiment 1

[0032] A production process for effectively extracting biological organic germanium, biological selenium and chalcone from Ashitaba, comprising the following steps:

[0033] Step 1. Ultrasonic extraction of ashitaba once

[0034] Cut the freshly picked Ashitaba leaves into chunks with a length of 0.5-1cm, extract once with chloroform that is 3 times the weight of the freshly picked Ashitaba leaves, and use ultrasonic conditions at a temperature of 30-40°C and a power of 80 Extract at -100W for 3min, filter out the insoluble matter, and separate the filtrate to obtain a water layer and an oil layer;

[0035] Step 2, Ultrasonic extraction of insoluble matter once

[0036] Put the insoluble matter in step 1 into a chloroform solution that is 3 times the weight of the freshly picked Ashitaba leaves and extract it once. Under the ultrasonic conditions, the temperature is 40-45°C, the power is 100-150W, and the extraction time is 10 minutes, and the insoluble matter is filtered out...

Embodiment 2

[0044] A production process for effectively extracting biological organic germanium, biological selenium and chalcone from Ashitaba, comprising the following steps:

[0045] Step 1. Ultrasonic extraction of ashitaba once

[0046] Cut the freshly picked Ashitaba leaves into chunks with a length of 0.5-1cm, extract once with chloroform that is 3 times the weight of the freshly picked Ashitaba leaves, and use ultrasonic conditions at a temperature of 30-40°C and a power of 80 Extract at -100W for 3min, filter out the insoluble matter, and separate the filtrate to obtain a water layer and an oil layer;

[0047] Step 2, Ultrasonic extraction of insoluble matter once

[0048] Put the insoluble matter in step 1 into a chloroform solution that is 3 times the weight of the freshly picked Ashitaba leaves and extract it once. Under the ultrasonic conditions, the temperature is 40-45°C, the power is 100-150W, and the extraction time is 10 minutes, and the insoluble matter is filtered out...

Embodiment 3

[0056] A production process for effectively extracting biological organic germanium, biological selenium and chalcone from Ashitaba, comprising the following steps:

[0057] Step 1, Ultrasonic Extraction of Ashitaba once Cut the freshly picked Ashitaba leaves into chunks with a length of 0.5-1cm, and use 3 times the weight of freshly picked Ashitaba leaves to extract once with chloroform, under ultrasonic conditions Extract at a temperature of 30-40°C and a power of 80-100W for 3 minutes, filter out the insoluble matter, and separate the filtrate to obtain a water layer and an oil layer;

[0058] Step 2. Ultrasonic extraction of insoluble matter once. Put the insoluble matter in step 1 into a chloroform solution that is 3 times the weight of freshly picked Ashitaba leaves and extract once. Under the ultrasonic conditions, the temperature is 40-45°C, and the power is 100- 150W, leaching for 10min, filtering out the insoluble matter, separating the filtrate to obtain a water lay...

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Abstract

The invention provides a production process for effectively extracting biological organic germanium, biological selenium and chalcone from Angelica keiskei, which comprises the following steps: step 1, cutting freshly picked Angelica keiskei leaves into blocks with the length of 0.5-1cm, conducting extracting once with chloroform under an ultrasonic condition for 3 minutes, filtering out insoluble substances, and layering filtrate to obtain a water layer and an oil layer; step 2, conducting extracting with chloroform twice; step 3, putting the insoluble substances in the step 2 into a chloroform solution for once extraction for 30 min under the ultrasonic condition, filtering out insoluble substances, and layering filtrate to obtain a water layer and an oil layer; step 4, conducting recycling; and step 5, carrying out enzymolysis, sterilizing and filtering, and carrying out reduced pressure distillation on filtrate until the filtrate is dry, so as to obtain a crude product B. According to the production process disclosed by the invention, organic germanium, biological selenium and chalcone in the angelica keiskei can be effectively separated out.

Description

technical field [0001] The invention belongs to the technical field of Ashitaba extraction, and in particular relates to a production process for effectively extracting biological organic germanium, biological selenium and chalcone from Ashitaba. Background technique [0002] Ashitaba is also a longevity vegetable, a perennial herb of the native Celery family, originally from Hachijo Island, Japan. It is a kind of plant with both medicine and food, and it is often used clinically to treat constipation and constipation. Studies have shown that Ashitaba is rich in various active ingredients such as chalcone, yellow vinegar, coumarin, organic germanium, organic selenium, and vitamin B J2. Chalcones have anti-cancer, anti-diabetes, blood lipid-lowering, anti-vascular diseases and other effects, and chalcones are clear [0003] The active ingredients with the highest content in Japanese leaves mainly include yellow angelica alcohol, yellow angelica alcohol F, yellow angelica al...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C07F7/30C07C45/78C07C45/82C07C49/796C08B37/00
CPCC07F7/30C07C45/78C07C45/82C08B37/0003C07C49/796
Inventor 于中玉葛卫桥潘惟谦
Owner 潘惟谦
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