All-solid secondary battery, and method of manufacturing all-solid secondary battery
A secondary battery, all-solid technology, applied in secondary battery, electrolyte storage battery manufacturing, battery electrodes, etc., can solve problems such as fire and overheating
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[0144] (Preparation of laminate of solid electrolyte layer / negative electrode layer)
[0145]At least one of materials constituting the first negative electrode active material layer 22, such as a first carbonaceous negative electrode active material, optionally a metal or metalloid negative electrode active material, and optionally a binder or an additive, may be added to the polar solvent Or a non-polar solvent to prepare slurry (the first negative electrode active material composition). The prepared slurry may be coated on the surface of the solid electrolyte layer 30 and dried to prepare a first laminate in which the first negative active material composition is disposed on the first surface of the solid electrolyte layer 30 . The first laminate may be heat-treated to prepare a second laminate in which the first negative electrode active material layer 22 which is a sintered product is provided on the solid electrolyte layer 30 . The heat treatment temperature may be, for...
Embodiment 1
[0163] Example 1: First layer (Ag+CB, 5 μm) / second layer (Ag+CB, 25 μm), and 450°C heat treatment of the first layer
[0164] (Preparation of laminate of solid electrolyte layer / negative electrode layer)
[0165]Carbon black (CB) having a primary particle diameter of about 38 nm and silver (Ag) particles having an average particle diameter of about 100 nm were prepared as negative electrode active materials.
[0166] 3 grams (g) of the carbon black (CB) and 1 g of the silver particles were placed in a container. 2.692 g of polyvinyl alcohol-polyacrylic acid (PVA-PAA) binder solution (SUMITOMO SEIKACHEMICALS CO., LTD; AG binder) was mixed with 7 g of distilled water, then added to the container, and the contents were distilled at about Stir at 1,000 rpm for about 30 minutes to prepare the first slurry. 4 g of zirconia balls and 20 g of distilled water were added to the first slurry, and stirred at about 1,000 revolutions per minute (rpm) for about 30 minutes (secondary stirri...
Embodiment 2
[0176] Example 2: First layer (Ag+CB, 5 μm) / second layer (Ag+CB, 25 μm), 600°C heat treatment of the first layer
[0177] An all-solid secondary battery was manufactured in the same manner as in Example 1 except that the heat treatment temperature was changed to 600° C. in the preparation of the first negative electrode active material layer.
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