Synthesis method of O-quaternized vanilla-based carbon residue particles based on amphiphilic biological carbon material
A technology of bio-carbon material and synthesis method, which is applied in the field of synthesis of O-quaternized vanillyl chitosan carbon slag particles, can solve the problems of few biocompatible antibacterial materials, and achieve excellent broad-spectrum antibacterial properties, The effect of expanding the application range and uniform and stable dispersion
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[0038] refer to Figure 1-4 As shown, the synthesis of O-quaternized vanillyl chitosan carbon residue particles based on amphiphilic biochar materials:
[0039](1) Preparation of amphiphilic bio-carbon material: Weigh 10 g of beer yeast cells (provided by Henan Aoke Brewery), add 80-100 ml of deionized water and stir to disperse evenly. In this embodiment, the amount of deionization added can be selected 90ml, 87ml or 96ml, the dispersion liquid is centrifuged at 8000r / min for 2min, the supernatant is discarded, the precipitate is added with an appropriate amount of acetone, the glass is stirred to mix, and placed on a shaker at 180r / min for 15-20min. In the embodiment, the glass cup is placed on a shaker and oscillated at 180r / min for 16min, 18min or 19min, centrifuged, and the supernatant liquid is poured off to obtain the yeast cell wall, and the above operation is repeated 3 to 5 times in the same way. Choose to repeat 4 or 5 times. Centrifugal wash with deionized water ...
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